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公开(公告)号：KR101166365B1
公开(公告)日：2012-07-23
申请号：KR1020090115867
申请日：2009-11-27
Applicant: 한국과학기술연구원
Abstract: 본 발명은 금속 나노 입자의 제조 방법에 관한 것으로서, (a) 알코올에 금속 전구체를 용해시킨 금속 전구체 용액을 준비하는 단계; (b) 상기 금속 전구체 용액을 초임계 조건의 반응기에 연속적으로 도입하여 금속 나노 입자를 생성시키는 단계; (c) 상기 단계 (b)에서 얻어지는 용액을 냉각시키는 단계; 및 (d) 상기 단계 (c)에서 얻어지는 용액으로부터 금속 나노 입자를 분리 및 회수하는 단계;를 포함하는 금속 나노 입자의 연속 제조 방법과, 이에 의하여 제조되는 금속 나노 입자에 관한 것이다.
금속 나노 입자, 알코올 용매, 초임계 조건, 연속공정-
42.发明授权
公开(公告)号：KR101075876B1
公开(公告)日：2011-10-25
申请号：KR1020100026294
申请日：2010-03-24
Applicant: 한국과학기술연구원
IPC: H01L31/04 , H01L21/208
CPC classification number: Y02E10/50
Abstract: 본발명은광전기화학전지용산화전극촉매막의제조방법, 이에따라제조되는촉매막및 이를이용한광전기화학전지에관한것으로, 더욱상세하게는상기목적을달성하기위해, 본발명은산화물나노입자를분산시킨후 페이스트또는잉크로제조하는단계(단계 1); 상기단계 1에서제조된산화물나노입자페이스트또는잉크로일면이광전극으로구성된전도성기판의또 다른일면에코팅막을형성시키는단계(단계 2); 및상기단계 3에서형성된코팅막을저온열처리하는단계(단계 3)를포함하는광전기화학전지용산화전극촉매막의제조방법, 산화물나노입자를분산시킨후 페이스트또는잉크로제조하여일면이광전극으로구성된전도성기판의또 다른일면에상기페이스트또는잉크로코팅막을형성시킨후 열처리하여제조되는, 광전기화학전지용산화전극촉매막및 광전셀/산화전극/이온분리막/환원전극으로이루어진광전기화학전지에있어서, 상기산화전극은일면이광전극으로구성된전도성기판의또 다른일면에산화물나노입자페이스트또는잉크로코팅막을형성시킨후 열처리하여제조되는촉매막으로이루어진것을특징으로하는광전기화학전지에관한것이다.
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公开(公告)号：KR101068691B1
公开(公告)日：2011-09-29
申请号：KR1020100010954
申请日：2010-02-05
Applicant: 한국과학기술연구원
IPC: C08B15/05
Abstract: 본 발명은 셀룰로오즈 포스파이트 화합물의 제조방법에 관한 것으로, 더욱 상세하게는 셀룰로오즈를 아민계 양이온과 포스파이트계 음이온으로 이루어진 이온성 액체를 사용한 포스포릴화 반응을 통해 제조하는 셀룰로오즈 포스파이트 화합물의 제조방법에 관한 것이다.
본 발명의 제조방법으로 제조된 셀룰로오즈 포스파이트 화합물은 물에 대한 용해도가 우수하여 농도 조절제, 의약품, 생체용 멤브레인 등의 소재로서 이용가치가 매우 크다.Abstract translation: 用于生产本发明所制备的磷酸纤维素化合物的本发明方法使用由基于胺的阳离子和阴离子磷酸酯组成的纤维素的离子液体涉及纤维素亚磷酸酯化合物的制造方法，并且更具体地，涉及磷酸化反应 Lt。
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公开(公告)号：KR1020110055163A
公开(公告)日：2011-05-25
申请号：KR1020090112074
申请日：2009-11-19
Applicant: 한국과학기술연구원
CPC classification number: H01M12/065 , H01M2/162 , H01M2/1673 , H01M4/12 , H01M4/661 , H01M4/742 , H01M4/8652 , H01M4/8657 , H01M4/886 , H01M4/8882 , H01M4/9016
Abstract: PURPOSE: A zinc-air fuel cell is provided to minimize the distance where hydroxide ions generated in a positive electrode collector moves to a negative electrode collector and to improve the performance of the fuel cell by accelerating a speed losing electrons from zinc. CONSTITUTION: A zinc-air fuel cell comprises: an integrated separator-electrode assembly including a metal porous plate as a positive electrode collector, carbon paper on which a catalyst is coated, separation film, and metal porous plate as a negative electrode collector; and an inclined non-conductive supporter. The metal porous plates as the positive and negative electrode collectors are stainless steel, nickel, iron, copper, gold or platinum.
Abstract translation: 目的：提供一种锌空气燃料电池，以使在正极集电体中产生的氢氧根离子移动到负极集电体的距离最小化，并且通过加速从锌损失电子的速度来提高燃料电池的性能。 构成：锌空气燃料电池包括：集成分离器电极组件，其包括作为正极集电体的金属多孔板，其上涂覆有催化剂的碳纸，分离膜和作为负极集电体的金属多孔板; 和倾斜的非导电支撑物。 作为正极和负极集电体的金属多孔板是不锈钢，镍，铁，铜，金或铂。
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公开(公告)号：KR1020100114395A
公开(公告)日：2010-10-25
申请号：KR1020090032906
申请日：2009-04-15
Applicant: 한국과학기술연구원
CPC classification number: B22F9/24 , B22F2202/03 , B22F2304/054 , B82Y30/00 , B82Y40/00
Abstract: PURPOSE: A method for quickly preparing metal nanoparticles of high yield using supercritical fluid without toxic reductant and storng acid is provided. CONSTITUTION: A method for preparing metal nanoparticles comprises: a step of dissolving metal precursors in alcohol to obtain a metal precursor solution; a step of introducing the metal precursor solution to a reactor to generate metal nanoparticles under supercritical condition; a step of cooling the metal nanoparticles; and a step of isolating and collecting metal particles from the cooled solution. The reaction temperature is 200-600°C. The metal nanoparticle is selected from a group consisting of Cu, Ni, Ag, Au, Ru, Rh, Pd and Pt.
Abstract translation: 目的：提供使用无毒还原剂和储存酸的超临界流体快速制备高产率金属纳米粒子的方法。 构成：制备金属纳米颗粒的方法包括：将金属前体溶解在醇中以获得金属前体溶液的步骤; 将金属前体溶液引入反应器以在超临界条件下生成金属纳米颗粒的步骤; 冷却金属纳米粒子的步骤; 以及从冷却的溶液中分离和收集金属颗粒的步骤。 反应温度为200-600℃。 金属纳米颗粒选自由Cu，Ni，Ag，Au，Ru，Rh，Pd和Pt组成的组。
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Patent Agency Ranking
公开(公告)号：KR1020100100465A
公开(公告)日：2010-09-15
申请号：KR1020090019374
申请日：2009-03-06
Applicant: 한국과학기술연구원
IPC: B22F9/16 , C07F1/08 , B82B3/00 , H01L31/0445
CPC classification number: Y02E10/50 , B22F9/24 , B22F1/0003 , C09D11/52 , H01B1/02
Abstract: PURPOSE: CIGS(CuInxGa1-xSe2) particles and a method for preparing the same are provided to prepare CIGS particles at relatively low temperature by using an alcohol mixed solvent with high volatility. CONSTITUTION: A method for preparing CIGS particles comprises steps of: preparing a CIG precursor compound(101) or oxide from the precursors of Cu, In, and Ga(100), dissolving the CIG precursor compound or oxide and Se precursor in a mixed organic solvent, synthesizing CIGS particles by making the solution react at a temperature lower than to the boiling temperature of the organic solvent and higher than the boiling temperature of alcohol, separating the precipitate from the solution and washing and drying it, and obtaining nano-sized CIGS particles through the centrifugal separation, washing and drying of the remaining solution.
Abstract translation: 目的：提供CIGS（CuInxGa1-xSe2）颗粒及其制备方法，以通过使用具有高挥发性的醇混合溶剂在较低温度下制备CIGS颗粒。 构成：制备CIGS颗粒的方法包括以下步骤：从Cu，In和Ga（100）的前体制备CIG前体化合物（101）或氧化物，将CIG前体化合物或氧化物和Se前体溶解在混合有机 溶剂，通过使溶液在低于有机溶剂的沸点温度的温度下反应并高于醇的沸点来合成CIGS颗粒，将沉淀物与溶液分离并洗涤和干燥，并获得纳米尺寸的CIGS 颗粒通过离心分离，洗涤和干燥剩余溶液。
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公开(公告)号：KR1020090131049A
公开(公告)日：2009-12-28
申请号：KR1020080056824
申请日：2008-06-17
Applicant: 한국과학기술연구원
Abstract: PURPOSE: A process for preparing hydrofluoroethers is provided to prepare hydrofluoroethers at a high yield while dramatically reducing a double bond product as a by-product by using alkali metal phosphate and halide-based amine salt. CONSTITUTION: A process for preparing hydrofluoroethers is prepared by reacting an alcohol compound and a fluorine-containing olefin compound. The reaction is performed in a condition that alkali metal phosphate and halide-based amine salt are present. The alcohol compound is selected from C1-8 alcohol, perfluorinated phenol containing 1-5 fluorine atoms, and C1-8 fluorinated alcohol containing 1-15 fluorine atoms. The fluorine-containing olefin is selected from C2-4 olefin compound containing 1-8 fluorine atoms.
Abstract translation: 目的：提供制备氢氟醚的方法以高产率制备氢氟醚，同时通过使用碱金属磷酸盐和卤化物基胺盐显着减少副产物作为副产物。 构成：通过醇化合物和含氟烯烃化合物反应制备氢氟醚的方法。 反应在存在碱金属磷酸盐和卤化物基胺盐的条件下进行。 醇化合物选自C1-8醇，含有1-5个氟原子的全氟化苯酚和含有1-15个氟原子的C1-8氟化醇。 含氟烯烃选自含有1-8个氟原子的C2-4烯烃化合物。
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公开(公告)号：KR1020090058375A
公开(公告)日：2009-06-09
申请号：KR1020070125122
申请日：2007-12-04
Abstract: A preparation method of 5-vinyl-2-norbornene is provided to improve a conversion ratio of cyclo pentadiene and to suppress by-products by using an aprotic polar compound. A preparation method of 5-vinyl-2-norbornene through Diels-alder reaction of cyclopentadiene and 1,3-butadiene uses a reaction catalyst and an aprotic polar compound as solvent. The aprotic polar compound is single or a mixture of at least two selected from dimethylformamide, monomethylformamide, monomethylacetamide, dimethylacetamide, dimethylsulfoxide and methylpyrrolidone.
Abstract translation: 提供5-乙烯基-2-降冰片烯的制备方法以提高环戊二烯的转化率，并通过使用非质子极性化合物抑制副产物。 通过环戊二烯和1,3-丁二烯的狄尔斯al反应制备5-乙烯基-2-降冰片烯的制备方法使用反应催化剂和非质子极性化合物作为溶剂。 非质子极性化合物是单一的或选自二甲基甲酰胺，单甲基甲酰胺，单甲基乙酰胺，二甲基乙酰胺，二甲基亚砜和甲基吡咯烷酮中的至少两种的混合物。
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公开(公告)号：KR102203806B1
公开(公告)日：2021-01-15
申请号：KR1020180107890
申请日：2018-09-10
Applicant: 한국과학기술연구원
IPC: G01N23/083
Abstract: 전기화학적흐름전지, 이를이용한실시간 X-선흡수법측정시스템, 및상기흐름전지에사용되는전극구조체가제공된다. 상기전기화학적흐름전지는전기화학적반응이가능하도록기준전극, 상대전극, 작업전극 3전극을하나의반응전지에포함하여, 작업전극의전극물질을 X-선흡수분광법을활용하여실시간분석가능하고, 전기화학적반응중 발생하는기체의 X-선신호의간섭효과를막을수 있다.
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公开(公告)号：KR102200474B1
公开(公告)日：2021-01-08
申请号：KR1020190041499
申请日：2019-04-09
Applicant: 한국과학기술연구원
Abstract: 양기능성수전해용전극촉매및 그제조방법, 그리고, 상기전극촉매를포함하는수전해전지가제공된다. 상기수전해용전극촉매는산소결핍도가크면서나노다공성구조를가지고, 산소발생성능및 수소발생성능이높아수전해시스템에활용될수 있다. 상기수전해용전극촉매는금속양이온및 할로겐음이온을포함하는용액을이용한전기화학적처리를통하여간단하게대면적으로제조할수 있다.
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