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公开(公告)号：KR1020040002510A
公开(公告)日：2004-01-07
申请号：KR1020030028254
申请日：2003-05-02
Applicant: 한국화학연구원
IPC: C07D263/58
CPC classification number: C07D213/643 , C07B2200/07 , C07C67/31 , C07C253/30 , C07D241/44 , C07D263/58 , C07C69/712 , C07C255/55
Abstract: PURPOSE: Provided is a process for manufacturing (R)-aryloxypropionic acid ester derivatives using substituted phenol derivative and (S)-alkyl O-arylsulfonyl lactate. CONSTITUTION: A process for manufacturing (R)-aryloxypropionic acid ester derivatives of the formula(1) is characterized by reacting a phenol derivative of the formula(2) and (S)-alkyl O-arylsulfonyl lactate of the formula(3) in the presence of alkali metal carbonate, using aliphatic or aromatic hydrocarbon at 60-100 deg.C.
Abstract translation: 目的：提供使用取代的苯酚衍生物和（S） - 烷基O-芳基磺酰基乳酸盐制备（R） - 丙氧基丙酸酯衍生物的方法。 构成：式（1）的（R） - 芳氧基丙酸酯衍生物的制备方法的特征在于使式（2）的苯酚衍生物与（S） - 式（3）的O-芳基磺酰基烷基烷基酯在 在60-100℃下使用脂族或芳族烃的碱金属碳酸盐的存在。
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公开(公告)号：KR1020000026668A
公开(公告)日：2000-05-15
申请号：KR1019980044313
申请日：1998-10-22
Applicant: 한국화학연구원
Abstract: PURPOSE: 2-phenyl alkanoic acid are prepared from 5,6-dihydro-2(4H)-benzofuranone in the presence of organic acid metal salt catalyst. CONSTITUTION: 5,6-Dihydro-2(4H)-benzofuranone of formula 2(R1 is H, C1-C6 alkyl, phenyl, benzoyl, phenoxy, furoyl or thenoyl; R2 is H, C1-C6 alkyl or phenyl; R3 is H, C1-C6 alkyl, phenyl, pyridyl, naphthyl or thiophenyl group) is reacted at 150-250°C in the presence of 0.01-5 equivalent weight of organic metal salt such as R-CO2M(R is H, C1-C13 alkyl, C1-C13 alkene, C1-C13 alkyne, C1-C13 alkoxyalkyl, C3-C6 cycloalkyl or A-(CH2)n; A is aryl group such as phenyl, naphthyl, pyridyl, quinolyl and thiophenyl group; n= 0-4; Mis alkali metal atom or under the structure) to give 2-phenyl alkanoic acid of formula 1.
Abstract translation: 目的：在有机酸金属盐催化剂存在下，从5,6-二氢-2（4H） - 苯并呋喃酮制备2-苯基链烷酸。 构成：式2的5,6-二氢-2（4H） - 苯并呋喃酮（R 1是H，C 1 -C 6烷基，苯基，苯甲酰基，苯氧基，糠基或后酰基; R 2是H，C 1 -C 6烷基或苯基; R 3是 H，C 1 -C 6烷基，苯基，吡啶基，萘基或噻吩基）在0.01-5当量有机金属盐如R-CO 2 M（R为H，C 1 -C 13）的存在下，在150-250℃下反应 烷基，C1-C13烯烃，C1-C13炔烃，C1-C13烷氧基烷基，C3-C6环烷基或A-（CH2）n; A是芳基如苯基，萘基，吡啶基，喹啉基和噻吩基; n = 4;错碱金属原子或结构下），得到式1的2-苯基链烷酸。
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公开(公告)号：KR1019990027763A
公开(公告)日：1999-04-15
申请号：KR1019970050284
申请日：1997-09-30
Applicant: 한국화학연구원
IPC: C07C69/767
Abstract: 본 발명은
o- (클로로메틸)벤조산 에스테르 유도체의 제조방법에 관한 것으로서, 더욱 상세하게는
o- (클로로메틸)벤조산 클로라이드를 출발물질로 하고 알콜화합물을 반응물질 및 반응용매로 사용하여 보다 간편한 조작과 온화한 조건하에서 에스테르화 반응시키므로써 작물보호제를 합성하는 중요한 중간체 화합물인 다음 화학식 1로 표시되는
o- (클로로메틸)벤조산 에스테르 유도체를 제조하는 새로운 방법에 관한 것이다.
상기 화학식 1에서: R
1 은 수소원자, 할로겐원자, C
1 ∼ C
6 의 알킬기, C
1 ∼ C
6 의 할로알킬기, C
1 ∼ C
6 의 알콕시기, C
1 ∼ C
6 의 알콕시카르보닐기, 니트로기 또는 페닐기를 나타내고; R
2 는 C
1 ∼ C
6 의 알킬기, C
1 ∼ C
6 의 할로알킬기 또는 C
3 ∼ C
6 의 사이클로알킬기를 나타낸다.-
公开(公告)号：KR1019960011389B1
公开(公告)日：1996-08-22
申请号：KR1019930006915
申请日：1993-04-24
Applicant: 한국화학연구원
IPC: C07D401/12
Abstract: The sulfonylurea derivatives having an erythro stereoisomer for substituents is described in the following structure of formula (I), wherein P and Q are the same or different, and are each CH or N, the aromatic ring having P and Q is benzene and pyridine ring, R is H or Ra-CO-, Ra-Xa-CO-, wherein Ra is C1-C4 alkyl, C1-C3 haloalkyl, C2-C4 alkenyl or C2-C4 alkinyl, Xa is oxygen or sulfur, NH is NRa, R' is H or CH3, X and Y are independently C1-C2 alkyl, C1-C2 -alkoxy, C1-C2 -haloalkoxy or halogen.
Abstract translation: 具有取代基的赤式立体异构体的磺酰脲衍生物在下列结构式（I）中描述，其中P和Q相同或不同，并且各自为CH或N，具有P和Q的芳环为苯和吡啶环 其中R a为C 1 -C 4烷基，C 1 -C 3卤代烷基，C 2 -C 4烯基或C 2 -C 4炔基，X a为氧或硫，NH为NR a， R'是H或CH 3，X和Y独立地是C 1 -C 2烷基，C 1 -C 2烷氧基，C 1 -C 2卤代烷氧基或卤素。
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公开(公告)号：KR1019930009508B1
公开(公告)日：1993-10-06
申请号：KR1019910004063
申请日：1991-03-14
Applicant: 한국화학연구원
IPC: C07D405/12
CPC classification number: C07D521/00 , A01N47/36
Abstract: Thiophene sulfonylurea derivs. of formula (I) are new. In the formula (I), R1=H, C1-3 alkyl, C1-3 haloalkyl, halogen, CN, C1-3 alkoxy, C1-3 haloalkoxy, NH2, NHCH3, N(Me)2, C1-2 alkyl substd. by C1-2 alkoxy, C1-2 haloalkoxy, SH, SCH3, CN or OH; R3=H or CH3; W=O or S; P= a gp. of formula (II), (III) or (IV). Pref. the cpds. (I) are methyltriazine-2-yl)amino carbonyl)-4-thiophene sulfonamide, aminocarbonyl)-3-(2-fluoromethyl-1,3-dioxyalane-2-yl)-4thiophene sulfonamide, etc. The cpds. (I) have a herbicidal activity.
Abstract translation: 噻吩磺酰脲衍生物。 式（I）的化合物是新的。 在式（I）中，R 1 = H，C 1-3烷基，C 1-3卤代烷基，卤素，CN，C 1-3烷氧基，C 1-3卤代烷氧基，NH 2，NHCH 3，N（Me）2， 。 C 1-2烷氧基，C 1-2卤代烷氧基，SH，SCH 3，CN或OH; R3 = H或CH3; W = O或S; P = gp。 的式（II），（III）或（IV）。 县。 cpds。 （I）是甲基三嗪-2-基）氨基羰基）-4-噻吩磺酰胺，氨基羰基）-3-（2-氟甲基-1,3-二氧戊烷-2-基）-4-噻吩磺酰胺等。 （I）具有除草活性。
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Patent Agency Ranking
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公开(公告)号：KR101201203B1
公开(公告)日：2012-11-15
申请号：KR1020120033835
申请日：2012-04-02
IPC: C07D413/04
CPC classification number: C07D413/04 , B01J31/0271
Abstract: PURPOSE: An industrial method for preparing [5-{(2,6-difluorobenzyloxy)methyl}-4,5-dihydro-5-methyl-3-(3-methylthiophene-2-yl)-isoxazole](methiozolin) is provided to obtain a large amount of the methiozolin of high purity and to cultivate agricultural crops. CONSTITUTION: A method for preparing thiozolin(chemical formula 1) comprises: a step of reacting 4,5-dihydro-5-methyl-3-{(3-methylthiophene-2-yl)-isoxazole-5-yl}methanol of chemical formula 2 with 2,6-difluorobenzyl(chloride or bromide) of chemical formula 3 using an alkali metal base and a phase converting catalyst in a mixture of water and organic solvent at 50-100 Deg. C. to prepare the concentrate of an organic layer; and a step of crystallizing the concentrate in a mixture solvent of water/ethanol, water/isopropanol, or C1-C3 alcohol/n-heptane. The organic solvent is benzene, toluene, xylene, chlorobenzene, or 1,2-dichloroethane. The alkali metal base is sodium hydroxide, potassium hydroxide, or lithium hydroxide.
Abstract translation: 目的：提供制备[5 - {（2,6-二氟苄氧基）甲基} -4,5-二氢-5-甲基-3-（3-甲基噻吩-2-基） - 异恶唑]（甲氧基）唑的工业方法） 获得大量高纯度的甲氧唑啉并培育农作物。 构成：制备噻唑啉（化学式1）的方法包括：将化合物的4,5-二氢-5-甲基-3 - {（3-甲基噻吩-2-基） - 异恶唑-5-基}甲醇 式2与化学式3的2,6-二氟苄基（氯化物或溴化物）使用碱金属碱和相转化催化剂在水和有机溶剂的混合物中在50-100℃下反应。 C.制备有机层的浓缩物; 以及将浓缩物在水/乙醇，水/异丙醇或C 1 -C 3醇/正庚烷的混合溶剂中结晶的步骤。 有机溶剂为苯，甲苯，二甲苯，氯苯或1,2-二氯乙烷。 碱金属碱是氢氧化钠，氢氧化钾或氢氧化锂。
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公开(公告)号：KR101103840B1
公开(公告)日：2012-01-06
申请号：KR1020090090692
申请日：2009-09-24
IPC: C07D239/54 , A01N43/54 , A01N41/06
CPC classification number: C07D239/54 , A01N43/54
Abstract: 본 발명은 하기 화학식 1로 표시되는 우라실계 화합물과 이 화합물의 제조방법, 및 이 화합물을 활성성분으로 포함하는 제초제에 관한 것이다.
상기 화학식 1에서, R
1 , R
2 , R
3 , R
4 , R
5 , X, Y, Z, 및 W는 각각 발명의 상세한 설명에서 정의한 바와 같다.
우라실, 제초제, 피리미딘다이온-
公开(公告)号：KR1020100121890A
公开(公告)日：2010-11-19
申请号：KR1020090040809
申请日：2009-05-11
Applicant: 한국화학연구원
Abstract: PURPOSE: A nematocidal composition containing N-3,4-dichlorophenyl-1-pyrrolidine carboxamide is provided to ensure strong nematocidal effect. CONSTITUTION: A nematocidal composition contains N-3,4-dichlorophenyl-1-pyrolidine carboxamide compound or pharmaceutically acceptable salt thereof as an active ingredient. The composition has nematocidal effect to Bursaphelenchus xylophilus.
Abstract translation: 目的：提供含有N-3,4-二氯苯基-1-吡咯烷甲酰胺的杀线虫组合物，以确保杀线虫效果。 构成：杀虫剂组合物含有作为活性成分的N-3,4-二氯苯基-1-吡咯烷羧酰胺化合物或其药学上可接受的盐。 该组合物对松节虫具有杀线虫作用。
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公开(公告)号：KR1020100121889A
公开(公告)日：2010-11-19
申请号：KR1020090040808
申请日：2009-05-11
Applicant: 한국화학연구원
Abstract: PURPOSE: A nematocide composition containing N-3,4-dichlorophenyl carbamic acid alkyl ester is provided to ensure strong nematicidal effect. CONSTITUTION: A nematocide composition contains N-3,4-dichlorophenyl carbamic acid alkyl ester compound of chemical formula 1 or pharmaceutically acceptable salt as an active ingredient. The composition has nematocidal effect against Bursaphelenchus xylophilus.
Abstract translation: 目的：提供含有N-3,4-二氯苯基氨基甲酸烷基酯的杀线虫剂，以确保强的杀线虫效果。 构成：杀线虫剂组合物含有化学式1的N-3,4-二氯苯基氨基甲酸烷基酯化合物或其药学上可接受的盐作为活性成分。 该组合物具有杀虫效果，适用于松节虫（Bursaphelenchus xylophilus）。
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