公开(公告)号：CA2468042A1

公开(公告)日：2003-06-12

申请号：CA2468042

申请日：2002-12-03

Applicant: BASF AG

Inventor： FRANKE DIRK ,  BOGENSTATTER THOMAS ,  KLOPP INGO

IPC: C07C51/41 ,  C07C20060101 ,  C07C63/00 ,  C07C63/04 ,  C07C63/08

Abstract: A method for the production of ammonium salts of aromatic carboxylic acids b y reaction of an aromatic carboxylic acid with ammonia in an aprotic solvent i s disclosed. Said reaction is carried out in a closed vessel and a solution of the aromatic carboxylic acid in an aprotic solvent and gaseous ammonia are continuously introduced into the vessel, such that a partial pressure of ammonia of 0.1 to 3 bars is maintained in the gas chamber of the vessel and a suspension of the ammonium salt separates out in the aprotic solvent. The method permits the production of ammonium salts with defined crystal size an d a narrow size distribution.

公开(公告)号：AU2002356773B2

公开(公告)日：2008-09-04

申请号：AU2002356773

申请日：2002-12-03

Applicant: BASF AG

Inventor： KLOPP INGO ,  FRANKE DIRK ,  BOGENSTATTER THOMAS

IPC: C07C51/41 ,  C07C20060101 ,  C07C63/00 ,  C07C63/04 ,  C07C63/08

Abstract: A process is described for preparing ammonium salts of aromatic carboxylic acids by reacting an aromatic carboxylic acid with ammonia in an aprotic solvent, which comprises carrying out the reaction in a closed vessel by continuously introducing a solution of the aromatic carboxylic acid in the aprotic solvent and passing in gaseous ammonia so that an ammonia partial pressure in the range from 0.1 to 3 bar is maintained in the gas space of the vessel, and discharging a suspension of the ammonium salt in the aprotic solvent. The process allows the preparation of ammonium salts of defined crystal size having a narrow size distribution.

公开(公告)号：DE50309110D1

公开(公告)日：2008-03-20

申请号：DE50309110

申请日：2003-11-28

Applicant: BASF AG

Inventor： KLOPP INGO ,  GONZALEZ GOMEZ JUAN ANTONIO ,  MAUTHE UWE ,  REISACHER HANSULRICH ,  STOHR ANDREAS

IPC: C09B67/20 ,  C08K9/04 ,  C08K9/08 ,  C09B67/00 ,  C09B67/22 ,  C09C3/08 ,  C09D7/12 ,  C09D11/02

Abstract: Solid pigment preparations containing the following ingredients as substantial components: (A) 60-85 wt. % of at least one organic pigment, (B) 0.1-15 wt. % of at least one pigment derivative of general formula I wherein the variables have the following meanings: P is the radical of the parent substance of an organic pigment; T 1 , T 2 independently represent a chemical bond, -CONR 1 - or -SO 2 NR 1 -; B 1 , B 2 independently represent a chemical bond, C1-C8-alkylene or phenylene;X, Y independently represent similar or different groups -SO 3 - Ka + or -COO- Ka + ; m, n represent a rational number from 0 to 3, whereby 1=m+n=4; Ka + H + , Li + , Na + , K + , N + R 2 R 3 R 4 R 5 or a mixture of said cations; R 1 represents hydrogen; C 1 -C 4 -alkyl; phenyl or naphthyl which can be respectively substituted by C 1 -C 18 -alkyl; R 2 , R 3 , R 4 , R 5 independently represent hydrogen; C 1 -C 30 -alkyl; C 3 -C 30 -alkenyl; C 5 -C 6 -cycloalkyl which can be substituted by C 1 -C 24 -alkyl; phenyl or naphthyl which can be respectively substituted by C 1 -C 24 -alkyl or C 2 -C 24 -alkenyl; a radical of formula -[CHR 6 -CHR 7 -O]x-R 8 , wherein the repeating units -[CHR 6 -CHR 7 -O] for x> 1 can vary; R 6 , R 7 , R 8 independently represent hydrogen or C 1 -C 6 -alkyl; x is a whole number= 1 , and (C) 14.9 39.9 wt. % of at least one surface active additive from the group of non-ionic polyethers containing no primary amino groups, the acidic phosphoric acid esters,phosphonic acid esters, sulphuric acid esters and/or sulfonic acid esters thereof, the salts thereof and the condensation produces thereof with formaldehyde.

公开(公告)号：AT372977T

公开(公告)日：2007-09-15

申请号：AT02804219

申请日：2002-12-03

Applicant: BASF AG

Inventor： KLOPP INGO ,  BOGENSTAETTER THOMAS ,  FRANKE DIRK

IPC: C07C51/41 ,  C07C20060101 ,  C07C63/00 ,  C07C63/04 ,  C07C63/08

Abstract: A process is described for preparing ammonium salts of aromatic carboxylic acids by reacting an aromatic carboxylic acid with ammonia in an aprotic solvent, which comprises carrying out the reaction in a closed vessel by continuously introducing a solution of the aromatic carboxylic acid in the aprotic solvent and passing in gaseous ammonia so that an ammonia partial pressure in the range from 0.1 to 3 bar is maintained in the gas space of the vessel, and discharging a suspension of the ammonium salt in the aprotic solvent. The process allows the preparation of ammonium salts of defined crystal size having a narrow size distribution.

公开(公告)号：DE50303970D1

公开(公告)日：2006-08-03

申请号：DE50303970

申请日：2003-06-18

Applicant: BASF AG

Inventor： REISACHER HANSULRICH ,  STOHR ANDREAS ,  KLOPP INGO ,  GONZALEZ GOMEZ JUAN ANTONIO

IPC: C08G18/08 ,  C08K9/04 ,  A61K8/04 ,  A61K8/46 ,  A61K8/55 ,  A61K8/90 ,  A61Q1/02 ,  C08G18/66 ,  C08L101/00 ,  C09B67/00 ,  C09B67/20 ,  C09B67/46 ,  C09D7/12 ,  C09D11/00 ,  C09D17/00 ,  C09D175/06 ,  C09D201/00

Abstract: Solid pigment preparations comprising as essential constituents (A) from 60% to 10% to 40% by weight of at least one anionic surface-active additive based on acid phosphoric, phosphonic, sulfuric and/or sulfonic esters of polyalkylene oxides or of reaction products of alkylene oxides with aliphatic alcohols, with phenol or naphthol, which may each be alkyl substituted if desired, with aliphatic or aromatic amines or with aliphatic carboxylic acids or carboxamides or on salts thereof, the fraction of the phosphorus-containing additive in a mixture of phosphorus- and sulfur-containing additives being not less than 50% by weight, and (C) from 0% to

公开(公告)号：MX238841B

公开(公告)日：2006-07-24

申请号：MXPA04001485

申请日：2002-08-29

Applicant: BASF AG

Inventor： BOGENSTATTER THOMAS ,  FRANKE DIRK ,  KLOPP INGO ,  MUNZINGER MANFRED

IPC: B01J8/08 ,  B01J8/00 ,  B01J8/06 ,  B01J8/20 ,  B01J19/00 ,  B01J19/24 ,  C07F9/141 ,  C07F9/38 ,  C07F9/40

Abstract: A process for carrying out a liquid/solid reaction comprises a) preparing a reaction suspension in which a first reactant is present in suspended form and a second reactant is present in dissolved form in a suspension medium, where one of the reaction products is insoluble in the suspension medium, b) passing the reaction suspension through an elongated reaction zone so that the Reynolds number of the stream is less than 20,000 and c) separating off the insoluble reaction product formed. The process has the advantage that the insoluble reaction product is obtained in a readily filterable form.

公开(公告)号：DE102004025443A1

公开(公告)日：2005-12-08

申请号：DE102004025443

申请日：2004-05-19

Applicant: BASF AG

Inventor： SCHROEDER GUNTER-RUDOLF ,  DECKER JUERGEN ,  REICHELT HELMUT ,  KLOPP INGO ,  DIEFENBACHER ARMIN ,  VOS HARTWIG

IPC: C09B35/38 ,  C09B35/42 ,  C09B35/52 ,  C09B37/00 ,  C09B67/26 ,  C09B67/54 ,  C09B67/36 ,  C09B29/00

Abstract: A process for producing a liquid formulation of salts of sulfonated azo dyes by coupling an at least equimolar amount of diazotized aminoarylsulfonic acids I H2N—Ar—SO3H  (I), where Ar is phenylene (which may be monosubstituted by sulfo) or naphthylene (which may be mono- or disubstituted by sulfo and/or monosubstituted by hydroxyl) onto the coupling product of an unsubstituted or methyl-substituted phenylenediamine with itself comprises dissolving the azo dye in a basic medium and then subjecting the solution to a nanofiltration.

公开(公告)号：MXPA04004852A

公开(公告)日：2004-07-30

申请号：MXPA04004852

申请日：2002-12-03

Applicant: BASF AG

Inventor： KLOPP INGO ,  BOGENSTAETTER THOMAS ,  FRANKE DIRK

IPC: C07C51/41 ,  C07C20060101 ,  C07C63/00 ,  C07C63/04 ,  C07C63/08

Abstract: Se describe un metodo para la produccion de sales de amonio de acidos carboxilicos aromaticos mediante la reaccion de un acido carboxilico aromatico con amoniaco en un solvente aprotico. Dicha reaccion se lleva a cabo en un recipiente cerrado y una solucion del acido carboxilico aromatico en un solvente aprotico y amoniaco gaseoso es introducida de manera continua dentro del recipiente, de manera que se mantiene una presion parcial de amoniaco de 0.1 hasta 3 bars en la camara de gas del recipiente y una suspension de la sal de amonio se separa en el solvente aprotico. El metodo permite la produccion de sales de amonio con tamano de cristal definido y una distribucion de tamano estrecha.

公开(公告)号：AU2003298151A8

公开(公告)日：2004-06-23

申请号：AU2003298151

申请日：2003-11-28

Applicant: BASF AG

Inventor： REISACHER HANSULRICH ,  KLOPP INGO ,  GOMEZ JUAN ANTONIO GONZALEZ ,  STOHR ANDREAS ,  MAUTHE UWE

IPC: C08K9/08 ,  C09B67/00 ,  C09B67/20 ,  C09B67/22 ,  C09D7/12 ,  C09D11/02 ,  C08K9/04 ,  C09C3/08

Abstract: Solid pigment preparations containing the following ingredients as substantial components: (A) 60-85 wt. % of at least one organic pigment, (B) 0.1-15 wt. % of at least one pigment derivative of general formula I wherein the variables have the following meanings: P is the radical of the parent substance of an organic pigment; T 1 , T 2 independently represent a chemical bond, -CONR 1 - or -SO 2 NR 1 -; B 1 , B 2 independently represent a chemical bond, C1-C8-alkylene or phenylene;X, Y independently represent similar or different groups -SO 3 - Ka + or -COO- Ka + ; m, n represent a rational number from 0 to 3, whereby 1=m+n=4; Ka + H + , Li + , Na + , K + , N + R 2 R 3 R 4 R 5 or a mixture of said cations; R 1 represents hydrogen; C 1 -C 4 -alkyl; phenyl or naphthyl which can be respectively substituted by C 1 -C 18 -alkyl; R 2 , R 3 , R 4 , R 5 independently represent hydrogen; C 1 -C 30 -alkyl; C 3 -C 30 -alkenyl; C 5 -C 6 -cycloalkyl which can be substituted by C 1 -C 24 -alkyl; phenyl or naphthyl which can be respectively substituted by C 1 -C 24 -alkyl or C 2 -C 24 -alkenyl; a radical of formula -[CHR 6 -CHR 7 -O]x-R 8 , wherein the repeating units -[CHR 6 -CHR 7 -O] for x> 1 can vary; R 6 , R 7 , R 8 independently represent hydrogen or C 1 -C 6 -alkyl; x is a whole number= 1 , and (C) 14.9 39.9 wt. % of at least one surface active additive from the group of non-ionic polyethers containing no primary amino groups, the acidic phosphoric acid esters,phosphonic acid esters, sulphuric acid esters and/or sulfonic acid esters thereof, the salts thereof and the condensation produces thereof with formaldehyde.

公开(公告)号：AU2003298151A1

公开(公告)日：2004-06-23

申请号：AU2003298151

申请日：2003-11-28

Applicant: BASF AG

Inventor： GOMEZ JUAN ANTONIO GONZALEZ ,  MAUTHE UWE ,  REISACHER HANSULRICH ,  STOHR ANDREAS ,  KLOPP INGO

IPC: C08K9/08 ,  C09B67/00 ,  C09B67/20 ,  C09B67/22 ,  C09D7/12 ,  C09D11/02 ,  C09C3/08 ,  C08K9/04

Abstract: Solid pigment preparations containing the following ingredients as substantial components: (A) 60-85 wt. % of at least one organic pigment, (B) 0.1-15 wt. % of at least one pigment derivative of general formula I wherein the variables have the following meanings: P is the radical of the parent substance of an organic pigment; T 1 , T 2 independently represent a chemical bond, -CONR 1 - or -SO 2 NR 1 -; B 1 , B 2 independently represent a chemical bond, C1-C8-alkylene or phenylene;X, Y independently represent similar or different groups -SO 3 - Ka + or -COO- Ka + ; m, n represent a rational number from 0 to 3, whereby 1=m+n=4; Ka + H + , Li + , Na + , K + , N + R 2 R 3 R 4 R 5 or a mixture of said cations; R 1 represents hydrogen; C 1 -C 4 -alkyl; phenyl or naphthyl which can be respectively substituted by C 1 -C 18 -alkyl; R 2 , R 3 , R 4 , R 5 independently represent hydrogen; C 1 -C 30 -alkyl; C 3 -C 30 -alkenyl; C 5 -C 6 -cycloalkyl which can be substituted by C 1 -C 24 -alkyl; phenyl or naphthyl which can be respectively substituted by C 1 -C 24 -alkyl or C 2 -C 24 -alkenyl; a radical of formula -[CHR 6 -CHR 7 -O]x-R 8 , wherein the repeating units -[CHR 6 -CHR 7 -O] for x> 1 can vary; R 6 , R 7 , R 8 independently represent hydrogen or C 1 -C 6 -alkyl; x is a whole number= 1 , and (C) 14.9 39.9 wt. % of at least one surface active additive from the group of non-ionic polyethers containing no primary amino groups, the acidic phosphoric acid esters,phosphonic acid esters, sulphuric acid esters and/or sulfonic acid esters thereof, the salts thereof and the condensation produces thereof with formaldehyde.