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公开(公告)号：DE3784146D1
公开(公告)日：1993-03-25
申请号：DE3784146
申请日：1987-12-04
Applicant: BASF AG
Inventor： DE DECKER EMILE , OOSTVOGELS JOZEF , VAN WAUWE GERARD , NEUBAUER GERALD DR
IPC: C07D201/04
Abstract: In prepn. of caprolactam by Beckmann conversion of cyclohexanone oxime with oleum at 70-130 deg.C, in at least 1 stage, the reaction mixt. is held for 10-600 mins. at 70-110 deg.C in a post-residence zone. Conversion is at 108-118 deg.C in 2 or 3 stages, with addn. to the 1st stage of all the oleum and 60-95 pts. of cyclohexanone oxime, and addn. of 40-5 pts. of the oxime to the latter stages. The mixt. is held in the post-residence zone for 15-180 mins., at 90-100 deg.C.
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公开(公告)号：DE58900134D1
公开(公告)日：1991-07-04
申请号：DE58900134
申请日：1989-11-10
Applicant: BASF AG
Inventor： FUCHS HUGO DR , AGAR DAVID DR , NEUBAUER GERALD DR , RITZ JOSEF DR
IPC: C07C249/14 , C07C251/44
Abstract: The storability of molten cyclohexanone oxime containing 0.5-15% by weight of cyclohexanone and 1-8% by weight of aqueous ammonium bisulfate solution is improved by washing the molten cyclohexanone oxime with a 10-42% strength by weight aqueous ammonium sulfate solution and maintaining a pH of 4.5-5.8.
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公开(公告)号：DE3761760D1
公开(公告)日：1990-04-05
申请号：DE3761760
申请日：1987-10-21
Applicant: BASF AG
Inventor： NEUBAUER GERALD DR , SCHNABEL ROLF DR , HARTIG JUERGEN DR , RITZ JOSEF DR
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公开(公告)号：DE3636056A1
公开(公告)日：1988-04-28
申请号：DE3636056
申请日：1986-10-23
Applicant: BASF AG
Inventor： NEUBAUER GERALD DR , SCHNABEL ROLF DR , HARTIG JUERGEN DR , RITZ JOSEF DR
IPC: C07C29/132 , C07C29/88 , C07C35/08 , C07C29/50 , C07C49/403
Abstract: A process for working up reaction mixtures containing cyclohexyl hydroperoxide, which have been obtained by oxidation of cyclohexane with molecular oxygen or gases containing such in the liquid phase at a temperature of 130 to 200@C and under a pressure of 5 to 125 bar, by reaction with cycloolefins at elevated temperature in the presence of catalysts, characterised in that cyclohexyl hydroperoxide is reacted with cyclohexene at elevated temperature in the presence of cyclohexane-soluble compounds of transition metals of the 4th to 6th group of the Periodic Table and the resulting cyclohexene oxide is then hydrogenated at elevated temperature in the presence of hydrogenation catalysts to give cyclohexanol.
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公开(公告)号：DE3375978D1
公开(公告)日：1988-04-21
申请号：DE3375978
申请日：1983-08-04
Applicant: BASF AG
Inventor： FRANK GERHARD DR , RUDOLF PETER DR , NEUBAUER GERALD DR , OHLINGER MANFRED DR , WILFINGER HANS JOERG DR , PFANNEBECKER EMIL , DUFFNER PAUL DR
IPC: B01J23/74 , B01J23/745 , B01J37/00 , C07B61/00 , C07C67/00 , C07C209/00 , C07C209/48 , C07C211/09 , C07C85/12
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Patent Agency Ranking
公开(公告)号：DE3528760A1
公开(公告)日：1987-02-19
申请号：DE3528760
申请日：1985-08-10
Applicant: BASF AG
Inventor： FUCHS HUGO DR , WEISS FRANZ-JOSEF DR , THOMAS ERWIN , NEUBAUER GERALD DR , RITZ JOSEF DR
IPC: C01B21/14
Abstract: Process for the preparation of hydroxylammonium nitrate, in which hydroxylammonium sulphate having a content of ammonium ions less than 500 ppm is reacted at elevated temperature with an equivalent amount of barium, strontium and/or calcium nitrate in aqueous solution, and calcium, strontium and/or barium sulphate is/are removed.
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公开(公告)号：DE3528463A1
公开(公告)日：1987-02-19
申请号：DE3528463
申请日：1985-08-08
Applicant: BASF AG
Inventor： FUCHS HUGO DR , WEISS FRANZ-JOSEF DR , THOMAS ERWIN , NEUBAUER GERALD DR , RITZ JOSEF DR
IPC: C01B21/14
Abstract: Process for the preparation of aqueous solutions of free hydroxylamine characterised in that hydroxylammonium sulphate having an ammonium ion content less than 500 ppm is reacted with equivalent amounts of oxides and/or hydroxides of calcium, strontium and/or barium in aqueous solution at a temperature below 20 DEG C and the insoluble sulphates are removed.
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公开(公告)号：DE3460627D1
公开(公告)日：1986-10-09
申请号：DE3460627
申请日：1984-12-18
Applicant: BASF AG
Inventor： FRANK GERHARD DR , NEUBAUER GERALD DR
IPC: B01J23/74 , B01J23/745 , B01J33/00 , B01J37/00 , B01J37/14 , B01J37/18 , C07B61/00 , C07C67/00 , C07C209/00 , C07C209/48 , C07C211/02 , C07C85/12
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公开(公告)号：DE3361565D1
公开(公告)日：1986-01-30
申请号：DE3361565
申请日：1983-08-04
Applicant: BASF AG
Inventor： FRANK GERHARD DR , RUDOLF PETER DR , NEUBAUER GERALD DR , DUFFNER PAUL DR , OHLINGER MANFRED DR , WILFINGER HANS JEORG DR , PFANNEBECKER EMIL
IPC: C07B61/00 , B01J23/00 , B01J23/74 , B01J23/745 , C07C67/00 , C07C209/00 , C07C209/48 , C07C211/03 , C07C211/09 , C07C85/12 , C07C87/14
Abstract: Saturated primary amines are prepared by reacting a nitrile with hydrogen at elevated temperature under superatmospheric pressure in the presence of ammonia and a metallic iron catalyst which has been obtained by reducing anisometric iron oxide particles with hydrogen at not more than 500 DEG C.
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公开(公告)号：AT232002B
公开(公告)日：1964-02-25
申请号：AT155362
申请日：1962-02-23
Applicant: BASF AG
Inventor： AMANN AUGUST DR , JENTZSCH WOLFGANG DR , NEUBAUER GERALD DR
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