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    54.
    发明专利
    未知

    公开(公告)号：BRPI0718526A2

    公开(公告)日：2013-11-12

    申请号：BRPI0718526

    申请日：2007-12-17

    Applicant: BASF SE

    Inventor： OLBERT GERHARD ,  CORR FRANZ ,  CRONE SVEN

    IPC: B01F5/04 ,  B01J8/08 ,  B01J8/12 ,  C07C5/32

    Abstract: The reactor (1) for continuous oxide hydrogenation of a feed gas flow (2) of saturated hydrocarbons, which are previously mixed with a gas flow (3) containing oxygen, on a moving catalyst bed (4) arranged between two concentric cylindrical holding devices (5, 6) in the longitudinal direction of the reactor by leaving a central inner space and an intermediate space, comprises four reactor sections, which are separated from each other and split into sub-sections by alternating disk-type deflector plates arranged in the central inner space. The reactor (1) for a continuous oxide hydrogenation of a feed gas flow (2) of saturated hydrocarbons, which are previously mixed with a gas flow (3) containing oxygen, on a moving catalyst bed (4) arranged between two concentric cylindrical holding devices (5, 6) in the longitudinal direction of the reactor by leaving a central inner space and an intermediate space between the moving catalyst bed and an inner envelope of the reactor to obtain a reaction gas mixture, comprises four reactor sections, which are separated from each other and split into sub-sections by alternating disk-type deflector plates arranged in the central inner space, and annular deflector plates arranged in the intermediate space between the moving catalyst bed and the inner envelope of the reactor. Each reactor sections comprise a mixing device, which is arranged in the direction of flow of the reaction gas mixture upstream of the moving catalyst bed. The mixing device is formed from two or three successively arranged rows of tubes having turbulence generators on the outer side of the tubes, which narrow the cross-section for the passage of the feed gas flow to 1/3-1/6 of the free cross-section. The oxygen-containing gas flow is guided through the tubes and sprayed into the feed gas flow through holes in the tubes in addition to a perforated plate mounted upstream of the tubes and a further perforated plate mounted downstream of the tubes. The tubes are ribbed tubes with the turbulence generators. The holes in rib gears are arranged between the ribs of the ribbed tubes. The ribbed tubes have 100-300 circulations of the ribs per meter length of the ribbed tubes, are formed from tubes with cylindrical outer circumference and are welded in spiral-shaped manner on the outer circumference along a strip longitudinal edge from a longitudinal strip containing ribs, which are notched under the formation of segments with exception of a rib base. An outer diameter of the tubes is 20-50 mm. A ratio of the height of the ribs to the outer diameter of the tubes is 1/10:1/2. The segments are distorted against the rib base in an angle. A thickness of the ribs is 0.3-1.5 mm and a width of the segments is 4-8 mm. The second row of the ribbed tubes is arranged in a gap to the first row of the ribbed tubes. The third row of the ribbed tubes is arranged in a gap to the second row of the ribbed tubes. The diameter of the holes in the upstream perforated plate is smaller than the half of the small distance of the ribs between two sequential circulations on each other. A ratio of the perforated plate thickness to the diameter of the holes in the perforated plate is 0.75:2.0. The diameter of the holes in the downstream perforated plate is larger or same to the diameter of the holes in the upstream perforated plate. The upstream perforated plate is arranged in a distance to flowing level of the first row of the ribbed tubes through the feed gas flow according to 7-20 times of the diameter of the holes in the upstream perforated plate. Two holes per rib gear are arranged between the ribs at diametrically opposite positions of the rib gears with small distance to the adjacent ribbed tubes in the row of the ribbed tubes. A ratio of the holes in the upstream perforated plate is defined as sum of the free surfaces of the holes in the upstream perforated plate related to the entire cross-section area vertical to the supply direction of the feed gas flow to the mixing device of = 0.3. The downstream perforated plate is spaced from the flowing level of the ribbed tubes around 0.5-2 times of the diameter of the ribbed tubes to the last row of the ribbed tubes. A distance of the downstream perforated plate for entering the reaction mixture into the catalyst bed is 5-20 times of the diameter of the holes in the downstream perforated plate. An independent claim is included for a procedure for continuous oxide hydrogenation of a feed gas flow of saturated hydrocarbons.

    METODO PARA LA PRODUCCION DE CLORO MEDIANTE OXIDACION DE CLORURO DE HIDROGENO EN FASE GASEOSA.
    55.
    发明专利
    METODO PARA LA PRODUCCION DE CLORO MEDIANTE OXIDACION DE CLORURO DE HIDROGENO EN FASE GASEOSA. 未知

    公开(公告)号：ES2362093T3

    公开(公告)日：2011-06-28

    申请号：ES03789225

    申请日：2003-12-11

    Applicant: BASF SE

    Inventor： OLBERT GERHARD ,  WALSDORFF CHRISTIAN ,  HARTH KLAUS ,  STROEFER ECKHARD ,  FIENE MARTIN

    IPC: B01J8/00 ,  C01B7/04 ,  B01J8/06

    Abstract: Metodo para producir cloro mediante oxidacion en fase gaseosa de cloruro de hidrogeno con una corriente de gas que contiene oxigeno molecular en presencia de un catalizador de lecho solido, caracterizado porque el metodo se realiza en un reactor (1) con un haz de tubos del catalizador (2) dispuestos en direccion longitudinal al reactor de manera paralela unos a otros, los cuales estan sujetados en sus extremos en los fondos de tubo (3), que tiene de a una cubierta (4) en ambos extremos del reactor (1), asi como con una o varias laminas deflectoras anulares dispuestas transversalmente a la direccion longitudinal del reactor en el espacio intermedio (5) entre los tubos del catalizador (2), las cuales dejan libres aberturas de paso (8), y una o varias laminas deflectoras (7) en forma de disco que dejan libres aberturas de paso anulares (9) en el borde del reactor, con disposicion alternante de laminas deflectoras anulares (6) y laminas deflectoras en forma de disco (7), en cuyo caso los tubos del catalizador (2) se llenan con el catalizador de lecho solido, el cloruro de hidrogeno y la corriente de gas que contiene oxigeno molecular se conduce desde un extremo de reactor por una cubierta (4) a traves de los tubos del catalizador (2) y la mezcla gaseosa de reaccion se retira del extremo opuesto del reactor por la segunda cubierta (4) y en cuyo caso se conduce un intercambiador liquido de calor a traves del espacio intermedio (5) alrededor de los tubos del catalizador (2), y en cuyo caso el reactor (1) esta sin tubos en la zona de las aberturas de paso (8, 9).

    57.
    发明专利
    未知

    公开(公告)号：DE102006060507A1

    公开(公告)日：2008-06-26

    申请号：DE102006060507

    申请日：2006-12-19

    Applicant: BASF SE

    Inventor： OLBERT GERHARD ,  CORR FRANZ ,  CRONE SVEN

    IPC: B01J8/02

    Abstract: A reactor (1) for carrying out a reaction between two fluid starting materials (2, 3) over a catalyst bed (4) with premixing of the fluid starting materials before introduction into the catalyst bed within a delay time of less than 150 minutes comprises a mixing-in device (5) containing transversally arranged to the inflow direction of the first fluid starting material stream, two/three rows arranged behind one another of tubes which have turbulence generators on the outside, a perforated plate upstream of the tubes and a perforated plate downstream of the tubes. A reactor (1) for carrying out a reaction between two fluid starting materials (2, 3) over a catalyst bed (4) with premixing of the fluid starting materials before introduction into the catalyst bed within a delay time of less than 150 minutes comprises a mixing-in device (5) containing transversally arranged to the inflow direction of the first fluid stream, two/three rows of tubes arranged behind one another and having turbulence generators on the outside, and constrict the flow cross section for the first fluid starting material stream to from 1/2 to 1/10, with the second fluid starting material stream being passed through the interiors of the tubes and injected via openings in the tubes into the first fluid starting material stream; a perforated plate upstream of the tubes; and a perforated plate downstream of the tubes. Independent claims are included for the following (1) mixing-in device for the reactor; and (2) static mixer for at least two fluid composed of the elements of the mixing-in device.

    Monolitos modulares de catalizador
    59.
    发明专利
    Monolitos modulares de catalizador 未知

    公开(公告)号：ES2929028T3

    公开(公告)日：2022-11-24

    申请号：ES16802003

    申请日：2016-11-18

    Applicant: BASF SE

    Inventor： OLBERT GERHARD ,  GAUER JOCHEN ,  FRIEDRICH HOLGER ,  SPIEGEL ANDREAS ,  WOELFERT ANDREAS ,  GMEINER WOLFGANG ,  LORENZ MICHAEL

    IPC: C01B21/26 ,  B01J8/00 ,  B01J19/24 ,  C01B21/28 ,  C01B21/38

    Abstract: La invención se refiere a un reactor (R) con un dispositivo (D) que contiene una base permeable a gases y/o líquidos (B) en cuya zona de borde está dispuesta una barrera lateral (W) que rodea completamente la base (B) y forma un volumen (V), conteniendo dicho volumen cuerpos moldeados catalíticos y/o no catalíticos (F), en el que al menos una malla de metal noble y/o de metal no noble está situada en el lado opuesto a la base (B) en aguas arriba, y los cuerpos moldeados (F) catalíticos y/o no catalíticos se seleccionan entre (i) cuerpos moldeados (F1) en forma de prismas rectos cuya superficie base se selecciona de un triángulo, rectángulo, hexágono o fragmentos de estos polígonos, o (ii) una combinación de cuerpos moldeados (F1) con cuerpos moldeados (F2) de menor tamaño que los cuerpos moldeados (F1), caracterizada porque grupos de m a n cuerpos moldeados (F1), donde m/ n es un número entero entre 3-30 y n > m, están obligados a formar módulos (M) en un casete de metal que se abre aguas arriba y se cierra con un gas-per base móvil en sentido aguas abajo, con sus caras laterales adosadas prácticamente sin intersticio y con su eje longitudinal orientado en dirección vertical, de manera que la sección transversal de la base quede prácticamente cubierta en su totalidad, y cuyos módulos (M) son unidos entre sí a modo de mosaico prácticamente sin separación, con la orientación vertical del eje longitudinal de los cuerpos moldeados (F1), opcionalmente con la cooperación de un material de relleno de juntas. (Traducción automática con Google Translate, sin valor legal)

    Procedimiento para la preparación de isocianatos
    60.
    发明专利
    Procedimiento para la preparación de isocianatos 未知

    公开(公告)号：ES2908060T3

    公开(公告)日：2022-04-27

    申请号：ES11767258

    申请日：2011-10-11

    Applicant: BASF SE

    Inventor： MATTKE TORSTEN ,  OLBERT GERHARD

    IPC: B01J19/18 ,  C07C263/10 ,  C07C265/14

    Abstract: Procedimiento para la preparación de isocianatos mediante reacción de las aminas correspondientes con fosgeno que comprende las etapas (a) suministrar al menos una corriente de reactivos que contenga amina y al menos una corriente de reactivos que contenga fosgeno, (b) mezclar las corrientes de reactivos con al menos una mezcla de reacción en una zona de mezcla, (c) hacer reaccionar la al menos una mezcla de reacción en una zona de reacción, y (d) tratar la al menos una mezcla de productos obtenida a partir de (c), en cuyo caso (iii) la zona de mezcla y la zona de reacción se componen de al menos dos ramas conectadas en paralelo y controlables por separado una de otra que comprenden respectivamente al menos una unidad de mezcla y al menos una unidad de reacción, en cuyo caso, controlables por separado una de otra significa que las ramas individuales conectadas en paralelo están separadas una de otra de manera bloqueable y pueden funcionar respectivamente de modo independiente una de la otra.

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