Apparatus for producing and casting liquid silicon
    54.
    发明授权
    Apparatus for producing and casting liquid silicon 失效
    用于生产和浇铸液态硅的设备

    公开(公告)号:US4272488A

    公开(公告)日:1981-06-09

    申请号:US075644

    申请日:1979-09-14

    Abstract: The method and apparatus for producing liquid silicon of high purity and for casting silicon. Hydrogen and a hydrogenated silane in gaseous state are mixed, preferably with a source of a small amount of oxygen, in a heated chamber producing the liquid silicon, with the exhaust gases bubbling out of the melt under a baffle. The chamber for the melt of liquid silicon preferably is lined with silicon dioxide. The liquid silicon may be used in making high purity vitreous silica and may be used in making castings of silicon. In making castings, the liquid silicon is accumulated in a second chamber and is periodically drawn from the second chamber into a third chamber which contains the mold for the casting.

    Abstract translation: 用于生产高纯度硅和硅铸造液态硅的方法和装置。 氢气和气态的氢化硅烷在产生液体硅的加热室中混合,优选用少量氧气源,废气在挡板下方从熔体中冒出。 用于液体硅熔体的室优选用二氧化硅衬里。 液硅可用于制造高纯度二氧化硅玻璃,可用于制造硅铸件。 在制造铸件时,液态硅积聚在第二腔室中,并且从第二腔室周期性地拉入包含用于铸造的模具的第三腔室。

    Process for producing liquid silicon
    55.
    发明授权
    Process for producing liquid silicon 失效
    液硅生产工艺

    公开(公告)号:US4176166A

    公开(公告)日:1979-11-27

    申请号:US800191

    申请日:1977-05-25

    Abstract: The method and apparatus for producing liquid silicon of high purity and for casting silicon. Hydrogen and a hydrogenated silane in gaseous state are mixed, preferably with a source of a small amount of oxygen, in a heated chamber producing the liquid silicon, with the exhaust gases bubbling out of the melt under a baffle. The chamber for the melt of liquid silicon preferably is lined with silicon dioxide. The liquid silicon may be used in making high purity vitreous silica and may be used in making castings of silicon. In making castings, the liquid silicon is accumulated in a second chamber and is periodically drawn from the second chamber into a third chamber which contains the mold for the casting.

    Abstract translation: 用于生产高纯度硅和硅铸造液态硅的方法和装置。 氢气和气态的氢化硅烷在产生液体硅的加热室中混合,优选用少量氧气源,废气在挡板下方从熔体中冒出。 用于液体硅熔体的室优选用二氧化硅衬里。 液硅可用于制造高纯度二氧化硅玻璃,可用于制造硅铸件。 在制造铸件时,液态硅积聚在第二腔室中,并且从第二腔室周期性地拉入包含用于铸造的模具的第三腔室。

    METHOD OF PREPARING P{11 O{11 {13 SiO{11 {11 PRODUCTS
    56.
    发明授权
    METHOD OF PREPARING P{11 O{11 {13 SiO{11 {11 PRODUCTS 失效
    制备P {11 O {11 {13 SiO {11}

    公开(公告)号:US3767434A

    公开(公告)日:1973-10-23

    申请号:US3767434D

    申请日:1971-04-08

    Inventor: THOMAS I

    Abstract: A method is provided for producing high purity oxide products of phosphorus and silicon such as, for example, a P2O5 and SiO2 glass wherein a silicon alkoxide is directly reacted with phosphorous acid, phosphoric acid, phosphorus pentoxide, or mixtures thereof, in the absence of any addition of a separate hydrolysis catalyst to produce a single phase solution reaction product and this reaction product with water is converted to a two-phase system, which two-phase system is removed of its free liquid components and the residue is then thermally decomposed to produce a product of phosphorus and silicon. This oxide product may be converted to a substantially unitary shape by conventional melting techniques or by conventional sintering techniques. The product may be used as an additive in conventional glass melting operations to supply at least a portion, and preferably all, of the P2O5 and/or silica requirements of the batch or the product may be compacted and suitably fired into a substantially unitary body, which body is an excellent target in sputtering applications for forming films on semiconductive materials such as, for example, silicon chips.

    Abstract translation: 提供了一种用于生产磷和硅的高纯度氧化物产物的方法,例如P2O5和SiO2玻璃,其中硅烷氧化物直接与亚磷酸,磷酸,五氧化二磷或其混合物反应,在不存在 任何添加单独的水解催化剂以产生单相溶液反应产物,并且该反应产物与水反应转化为两相体系,其两相体系除去其游离液体组分,然后将残余物热分解成 产生磷和硅的产物。 该氧化物产物可以通过常规熔融技术或通过常规烧结技术转化为基本上单一的形状。 该产品可以用作常规玻璃熔融操作中的添加剂,以供应批料或产物的至少一部分,优选全部P 2 O 5和/或二氧化硅的要求或可以压实并适当地烧制成基本上单一的主体, 该体是用于在半导体材料(例如硅芯片)上形成薄膜的溅射应用中的优异靶标。

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