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    64.
    发明专利
    未知

    公开(公告)号：DE69222753D1

    公开(公告)日：1997-11-20

    申请号：DE69222753

    申请日：1992-03-16

    Applicant: UCB SA

    Inventor： MOENS LUC ,  MAETENS DANIEL ,  LOUTZ JEAN-MARIE ,  BAUDOUR MICHEL

    IPC: C08G63/199 ,  C08G63/553 ,  C09D163/00 ,  C09D167/00 ,  C09D5/03

    Abstract: Polyesters containing terminal carboxyl groups comprising the products of reaction of (a) an aliphatic polyester containing terminal hydroxyl groups, prepared from 1,4-cyclohexanedicarboxylic acid and from an alcoholic constituent comprising (1) from 10 to 100 equivalents % of a cycloaliphatic diol and (2) from 90 to 0 equivalents % of at least one aliphatic polyol containing a straight or branched chain which has from 2 to 12 carbon atoms, with (b) an aliphatic and/or aromatic dicarboxylic acid or the corresponding anhydride, process for their preparation and heat-curable compositions in powder form based on these polyesters and polyepoxy compounds used for the production of varnishes and paints in powder form. These polyesters yield coatings which have an excellent resistance to inclement weather, combined with remarkable mechanical properties, even when the curing is performed at low temperature.

    COMPOSICIONES EN POLVO DE POLIESTERES CRISTALINOS QUE CONTIENEN GRUPOS METACRILILO.
    65.
    发明专利
    COMPOSICIONES EN POLVO DE POLIESTERES CRISTALINOS QUE CONTIENEN GRUPOS METACRILILO. 未知

    公开(公告)号：MX9601513A

    公开(公告)日：1997-07-31

    申请号：MX9601513

    申请日：1996-04-23

    Applicant: UCB SA

    Inventor： MOENS LUC ,  LOUTZ JEAN-MARIE ,  MAETENS DANIEL ,  LOOSEN PATRICK ,  KERCKHOVE MARC VAN

    IPC: C08F290/00 ,  C08F290/06 ,  C08F299/04 ,  C08G63/58 ,  C09D5/03 ,  C09D5/46 ,  C09D167/06 ,  C09D167/07 ,  C09D167/02

    Abstract: Se describen composiciones en polvo, curables con radiacion para utilizarse como barniz o pintura, las cuales comprenden por lo menos un poliéster cristalino que contiene grupos metacrililo en el extremo, que comprenden los productos de la reaccion del metacrilato de glicidilo y de poliéster cristalino que contiene grupos carboxilo en el extremo. El poliéster cristalino que contiene grupos carboxilo en el extremo es, ya sea: (a) un poliéster el cual es el producto de la reaccion de (1) un constituyente ácido, el cual contiene (a.1.1) de 85 a 100 % en moles de ácido tereftálico o del ácido 1,4-ciclohexanodicarboxílico y (a.1.2) de 0 a 15 % en moles de por lo menos otro ácido di- o policarboxílico, alifático, cicloalifático o aromático que tiene de 4 a 14 átomos de carbono; y (2) un constituyente alcohol el cual contiene (a.2.1) de 85 a 100 % en moles de un diol alifático, de cadena lineal, saturado que tiene de 2 a 12 átomos de carbono y (a.2.2) de 0 a 15 % en moles de por lo menos otro di- o poliol alifático o cicloalifático que tiene de 2 a 15 átomos de carbono; y (b) un poliéster el cual es el producto de la reaccion de (1) un constituyente ácido el cual contiene (b.1.1) de 85 a 100 % en moles de un ácido dicarboxílico alifático, de cadena lineal, saturado que tiene de 4 a 14 átomos de carbono y (b.1.2) de 0 a 15 % en moles de por lo menos otro ácido di- o policarboxílico, alifático, cicloalifático o aromático que tiene de 4 a 14 átomos de carbono, y (2) un constituyente alcohol el cual contiene (b.2.1) de 85 a 100 % en moles del 1,4-ciclohexanodiol, del 1,4-ciclohexanodimetanol o del etilenglicol y (b.2.2) de 0 a 15 % en moles de por lo menos otro di- o poliol alifático o cicloalifático, que tiene de 2 a 15 átomos de carbono.

    Powder compositions of crystalline polyesters containing end methacrylyl groups
    66.
    发明专利
    Powder compositions of crystalline polyesters containing end methacrylyl groups 未知

    公开(公告)号：SG38962A1

    公开(公告)日：1997-04-17

    申请号：SG1996009315

    申请日：1996-04-20

    Applicant: UCB SA

    Inventor： MOENS LUC ,  LOUTZ JEAN-MARIE ,  MAETENS DANIEL ,  LOOSEN PATRICK ,  KERCKHOVE VAN MARC

    IPC: C08F290/00 ,  C08F290/06 ,  C08F299/04 ,  C08G63/58 ,  C09D5/03 ,  C09D5/46 ,  C09D167/06 ,  C09D167/07 ,  C08F ,  C08G ,  C08L ,  C09D

    Abstract: Radiation-curable powder coating compsns. contain crystalline polyester(s) with methacrylyl terminal gps. obtd. by reacting glycidyl methacrylate with a carboxy-terminated polyester of: (a) a polyester reaction prod. of: (1) an acid component contg.: (a.1.1) 85-100 mole% terephthalic acid or 1,4-cyclohexanedicarboxylic acid; and (a.1.2) 0-15 mole % of other aliphatic, cycloaliphatic or aromatic di- or polycarboxylic acid(s) with 4-14C, and (2) an alcohol component contg.: (a.2.1) 85-100 mole % of a 2-12C satd. aliphatic linear diol; and (a.2.2) 0-15 mole% of other aliphatic or cycloaliphatic di- or polyol(s) with 2-15C, and (b) a polyester reaction prod. of: (1) an acid component contg.: (b.1.1) 85-100 mole% of a satd. aliphatic linear dicarboxylic acid with 4-14C; and (b.1.2) 0-15 mole% of other aliphatic, cycloaliphatic or aromatic di- or polycarboxylic acid(s) with 4-14C, and (2) an alcohol component contg.: (b.2.1) 85-100 mole% of 1,4-cyclohexanediol, 1,4-cyclohexane-dimethanol or ethylene glycol; and (b.2.2) 0-15 mole % of other aliphatic or cycloaliphatic di- or polyol(s) with 2-15C. Also claimed are: (i) a process for coating an article; (ii) varnish and paint coating cured by exposure to electron beam radiation ; and (ii) varnish or paint coating cured by exposure to ultraviolet radiation.

    Thermosetting powder compositions based on polyesters and acrylic copolymers
    67.
    发明专利
    Thermosetting powder compositions based on polyesters and acrylic copolymers 未知

    公开(公告)号：AU5765194A

    公开(公告)日：1994-09-15

    申请号：AU5765194

    申请日：1994-03-09

    Applicant: UCB SA

    Inventor： MOENS LUC ,  MAETENS DANIEL ,  DALLONS JEAN-LUC ,  LOUTZ JEAN-MARIE

    IPC: B05D1/04 ,  B05D7/24 ,  C08G59/32 ,  C08G59/40 ,  C08G63/181 ,  C08G63/183 ,  C08L33/04 ,  C08L33/14 ,  C08L63/00 ,  C08L67/00 ,  C08L67/02 ,  C09D133/04 ,  C09D133/14 ,  C09D163/00 ,  C09D167/00 ,  C09D167/02

    Abstract: Powdered thermosetting compositions including (a) a specific polyester containing carboxyl end groups and (b) an acrylic copolymer containing glycidyl groups. The polyester (a) containing carboxyl end groups has an acid value of 15 to 70 mg of KOH/g and is necessarily prepared in two stages. In the first stage a polyester containing hydroxyl end groups is prepared from at least one polycarboxylic acid other than 1,4-cyclohexanedicarboxylic acid and from at least one aliphatic or cycloaliphatic polyol and, in the second stage, the polyester containing hydroxyl end groups thus obtained is esterified with 1,4-cyclohexanedicarboxylic acid alone. Moreover, the composition of the polyester (a) is highly specific: it contains at least 75 mol% of terephthalic acid, at least 10 mol% of 1,4-cyclohexanedicarboxylic acid and not more than 14 mol% of at least one other aromatic and/or aliphatic and/or cycloaliphatic polycarboxylic acid, relative to the total of the carboxylic acids forming part of its composition. The powdered thermosetting compositions obtained from polyester (a) and from the acrylic copolymer (b) are particularly useful for the preparation of powdered paints and varnishes. They yield coatings exhibiting high gloss, excellent mechanical properties and, at the same time, good weathering resistance.

    SELF-EXTINGUISHING UNSATURATED POLYESTERS
    68.
    发明专利
    SELF-EXTINGUISHING UNSATURATED POLYESTERS 未知

    公开(公告)号：GB1221330A

    公开(公告)日：1971-02-03

    申请号：GB2714068

    申请日：1968-06-07

    Applicant: UCB SA

    Inventor： LAMBERT POL ,  LOUTZ JEAN-MARIE ,  EYGEN CYRILLE VAN

    IPC: C08G63/688

    Abstract: 1,221,330. Unsaturated polyesters. UCB (UNION CHIMIQUE-CHEMISCHE BEDRIJVEN) S.A. 6 June, 1969 [7 June, 1968], No. 27140/68. Headings C3P and C3R. Copolymerizable unsaturated self-extinguishing polyesters may be prepared by condensing unsaturated polycarboxylic acids with polyhydroxy halogenated thio compounds of the general formula where R is an aliphatic hydrocarbon radical containing at least one hydroxyl group, X is hydrogen or halogen, at least one X being halogen. The halogen atoms are preferably chlorine or bromine. The unsaturated polycarboxylic acid may be maleic, fumaric, itaconic or aconitic acid. The reaction mixture may include saturated polycarboxylic acids such as succinic, adipic, sebacic, phthalic, isophthalic terephthalic and tetrachlorophthalic acids, and the Diels-Alder product of maleic anhydride with hexachlorocyclopentadiene, or ester-forming derivatives thereof, and saturated or unsaturated monocarboxylic acids such as acetic, acrylic, methacrylic and benzoic acids. The thio compound may be partially replaced by other polyhydroxy compounds such as ethylene glycols, propylene glycols, glycerol, trimethylolpropane and pentaerythritol, or by a monohydroxy alcohol such as methanol, ethanol, propanol, 2-ethylhexanol or nonanol. The unsaturated polyesters may be dissolved in vinylic compounds, such as styrene, acrylic esters, methacrylic esters or vinyl esters to produce a resin which may be copolymerized in the presence of free radical catalysts initiated by an organo-metallic compound. Before copolymerization the resin may be mixed with conventional additives (e.g. antimony trioxide). Uses.-Shaped articles such as laminates, coated, painted or varnished articles.

    69.
    发明专利
    未知

    公开(公告)号：DE69627010T2

    公开(公告)日：2003-12-11

    申请号：DE69627010

    申请日：1996-12-05

    Applicant: UCB SA

    Inventor： MOENS LUC ,  MAETENS DANIEL ,  LOOSEN PATRICK ,  LOUTZ JEAN-MARIE

    IPC: C08L67/02 ,  C09D5/03 ,  C09D167/00 ,  C09D167/02

    Abstract: Thermosetting powder compositions comprising as binder a mixture of polyesters containing carboxyl groups and of a crosslinking agent having functional groups capable of reacting with the carboxyl groups.The polyesters comprise:(a) a semicrystalline polyester containing carboxyl groups, which comprises, with respect to the total amount of alcohols, of from 85 to 100 mol % of 1,4-cyclohexanediol and of from 0 to 15 mol % of at least one other aliphatic and/or cycloaliphatic polyol and, with respect to the total amount of acids, of from 85 to 100 mol % of a straight-chain saturated dicarboxylic aliphatic acid having from 4 to 14 carbon atoms and of from 0 to 15 mol % of at least one other aliphatic and/or cycloaliphatic and/or aromatic polycarboxylic acid; and(b) an amorphous polyester containing carboxyl groups, which comprises, with respect to the total amount of acids, of from 70 to 100 mol % of isophthalic acid and of from 0 to 30 mol % of at least one other aliphatic and/or cycloaliphatic and/or aromatic polycarboxylic acid and, with respect to the total amount of alcohols, of from 70 to 100 mol % of neopentyl glycol and/or of 2-butyl-2-ethyl-1,3-propanediol and of from 0 to 30 mol % of at least one other aliphatic and/or cycloaliphatic polyol.

    70.
    发明专利
    未知

    公开(公告)号：AT235539T

    公开(公告)日：2003-04-15

    申请号：AT96940944

    申请日：1996-12-05

    Applicant: UCB SA

    Inventor： MOENS LUC ,  MAETENS DANIEL ,  LOOSEN PATRICK ,  LOUTZ JEAN-MARIE

    IPC: C08L67/02 ,  C09D5/03 ,  C09D167/00 ,  C09D167/02

    Abstract: Thermosetting powder compositions comprising as binder a mixture of polyesters containing carboxyl groups and of a crosslinking agent having functional groups capable of reacting with the carboxyl groups.The polyesters comprise:(a) a semicrystalline polyester containing carboxyl groups, which comprises, with respect to the total amount of alcohols, of from 85 to 100 mol % of 1,4-cyclohexanediol and of from 0 to 15 mol % of at least one other aliphatic and/or cycloaliphatic polyol and, with respect to the total amount of acids, of from 85 to 100 mol % of a straight-chain saturated dicarboxylic aliphatic acid having from 4 to 14 carbon atoms and of from 0 to 15 mol % of at least one other aliphatic and/or cycloaliphatic and/or aromatic polycarboxylic acid; and(b) an amorphous polyester containing carboxyl groups, which comprises, with respect to the total amount of acids, of from 70 to 100 mol % of isophthalic acid and of from 0 to 30 mol % of at least one other aliphatic and/or cycloaliphatic and/or aromatic polycarboxylic acid and, with respect to the total amount of alcohols, of from 70 to 100 mol % of neopentyl glycol and/or of 2-butyl-2-ethyl-1,3-propanediol and of from 0 to 30 mol % of at least one other aliphatic and/or cycloaliphatic polyol.

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