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    Amino-substd. alkyl nitriles prodn. - from amines, carbonyl cpds. and hydrogen cyanide, useful e.g. as pharmaceutical and agrochemical intermediates
    83.
    发明专利
    Amino-substd. alkyl nitriles prodn. - from amines, carbonyl cpds. and hydrogen cyanide, useful e.g. as pharmaceutical and agrochemical intermediates 未知

    公开(公告)号：DE2621728A1

    公开(公告)日：1977-11-24

    申请号：DE2621728

    申请日：1976-05-15

    Applicant: BASF AG

    Inventor： DISTLER HARRY DR ,  TOLKSDORF ERICH DR ,  HARTERT ERWIN DR ,  SCHLECHT HELMUT DR

    IPC: C07C255/24 ,  C07D295/145 ,  C07D295/15 ,  C07C121/43 ,  C07C120/00

    Abstract: Prepn. of glycine nitriles of formula R3R4N.CR5R6.CN (I) comprises reacting amnes R3R4NH (III) with carbonyl cpds R5COR6 (IV) and HCN in presence of water for 0.1-4 hrs. at 0-80 degrees C. The condn. of HCN never exceeds 0.9 wt. % of the reaction mixt. In the formulae, R3-6 are aromatic, cycloaliphatic or araliphatic gps.; R3 and R4 may together complete a heterocycle; R4-6 may also be H, and R5 and R6 may also be aliphatic, and when R5 and/or R6 is aliphatic aromatic, cycloaliphatic or araliphatic, then R3 and R4 can also be aliphatic. Pref. the products where R3-6 are aromatic gps., R5 and R6 may also be H, aliphatic, cycloaliphatic or araliphatic, and R4 may be H, are subsequently treated with an acid at pH 1-7. (I) are stabilisers; intermediates for dyes (e.g. indigo) fungicides, bactericides, textile auxiliaries and antigelling agents; and by saponification give glycine salts useful as selective adsorbents for CO2, SO2 and H2S, and by hydrogenation give assymetric diamines useful for making pharmaceuticals and plant protection agents. Cf. the process of DT 1543342. This method is simpler and more economic giving better yields of purer products. Water pollution and formation of resinous by-products are minimised, and subsequent acid treatment obviates expensive purification steps and avoids losses of solvent.

    Amino-substd. alkyl nitriles prodn. - from amines, carbonyl cpds. and hydrogen cyanide, useful e.g. as pharmaceutical and agrochemical intermediates
    84.
    发明专利
    Amino-substd. alkyl nitriles prodn. - from amines, carbonyl cpds. and hydrogen cyanide, useful e.g. as pharmaceutical and agrochemical intermediates 未知

    公开(公告)号：DE2621450A1

    公开(公告)日：1977-11-24

    申请号：DE2621450

    申请日：1976-05-14

    Applicant: BASF AG

    Inventor： DISTLER HARRY DR ,  TOLKSDORF ERICH DR ,  HARTERT ERWIN DR ,  SCHLECHT HELMUT DR

    IPC: C07C255/24 ,  C07D295/145 ,  C07D295/15 ,  C07C121/43 ,  C07C120/00

    Abstract: Prepn. of glycine nitriles of formula R3R4N.CR5R6.CN (I) comprises reacting amnes R3R4NH (III) with carbonyl cpds R5COR6 (IV) and HCN in presence of water for 0.1-4 hrs. at 0-80 degrees C. The condn. of HCN never exceeds 0.9 wt. % of the reaction mixt. In the formulae, R3-6 are aromatic, cycloaliphatic or araliphatic gps.; R3 and R4 may together complete a heterocycle; R4-6 may also be H, and R5 and R6 may also be aliphatic, and when R5 and/or R6 is aliphatic aromatic, cycloaliphatic or araliphatic, then R3 and R4 can also be aliphatic. Pref. the products where R3-6 are aromatic gps., R5 and R6 may also be H, aliphatic, cycloaliphatic or araliphatic, and R4 may be H, are subsequently treated with an acid at pH 1-7. (I) are stabilisers; intermediates for dyes (e.g. indigo) fungicides, bactericides, textile auxiliaries and antigelling agents; and by saponification give glycine salts useful as selective adsorbents for CO2, SO2 and H2S, and by hydrogenation give assymetric diamines useful for making pharmaceuticals and plant protection agents. Cf. the process of DT 1543342. This method is simpler and more economic giving better yields of purer products. Water pollution and formation of resinous by-products are minimised, and subsequent acid treatment obviates expensive purification steps and avoids losses of solvent.

    86.
    发明专利
    未知

    公开(公告)号：DE2354714A1

    公开(公告)日：1975-05-28

    申请号：DE2354714

    申请日：1973-11-02

    Applicant: BASF AG

    Inventor： BECHERT BERTHOLD ,  DISTLER HARRY DR ,  PETRI ROLF

    IPC: C04B24/00 ,  C04B13/24

    Abstract: Mono- or di-alkyl phosphate or their alkali metal salts or optionally substituted ammonium salts for use as antifoaming and hydrophobizing additives for hydraulic binders.

    90.
    发明专利
    未知

    公开(公告)号：DE1768407A1

    公开(公告)日：1971-08-05

    申请号：DE1768407

    申请日：1968-05-10

    Applicant: BASF AG

    Inventor： DISTLER HARRY DR ,  WIDDER RUDI DR

    IPC: C07D233/54 ,  D06M13/248 ,  C07C149/24

    Abstract: 1,257,851. Treating textiles. BADISCHEANILIN- & SODA-FABRIK A.G. 9 May, 1969 [10 May, 1968; 14 Aug., 1968], No. 23670/69. Heading D1P. [Also in Division C2] N,N - bis(# - stearamidoethyl) - # - sulphitoethylbetaine (prepared from N,N - bis(# - stearamidoethyl)amine and polyglycol sulphite) is used in an amount of 10-40 g./l. of aqueous finishing liquor for impregnating cotton, rayon staple fibre, viscose cloth or appropriate yarns, which are then dried to give a soft smooth and full handle.

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