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    A process for the production of high energy material
    86.
    发明公开
    A process for the production of high energy material 失效
    Verfahren zur Herstellung energiereichen材料。

    公开(公告)号：EP0223440A1

    公开(公告)日：1987-05-27

    申请号：EP86308290.5

    申请日：1986-10-24

    Applicant: Secretary of State for Defence in Her Britannic Majesty's Gov. of the United Kingdom of Great Britain and Northern Ireland

    Inventor： Millar, Ross Wood ,  Paul, Norman Charles ,  Richards, David Hugh

    IPC: C07C201/02 ,  C07C201/04 ,  C07C203/02 ,  C08C19/22 ,  C07D251/00 ,  C06B49/00

    CPC classification number: C07F9/65815 ,  C06B25/00 ,  C07C201/02 ,  C07C203/04 ,  C07C203/06 ,  C07C203/08 ,  C07D251/66

    Abstract: A process for the production of a high energy nitrate ester involves reacting, in an inert organic solvent, a heterocyclic compound, selected from oxiranes, oxetanes, N-substituted aziridines and N-substituted azetidines, with either N 2 0 4 or N 2 0 5 , and when the compound is reacted with N 2 0 4 , oxidising the 0- or N-nitrate substituents or substituent in the product to O-or N - nitrate substituent or substituents. The remaining ring carbon atoms on the heterocyclic compound may be substituted or unsubstituted. Preferred substituent groups for the C and/or N ring atoms on the compound include alkyl, cyanoalkyl, haloalkyl, nitroalkyl, and substituted aryl.
    Several novel nitrate ester are also provided, including nitrated derivatives of polybutadiene, in which between 1 % and 25% of the carbon atoms in the polymer are substituted by vicinal nitrate ester (-ON0 2 ) groups.

    Abstract translation: 制备高能硝酸酯的方法包括在惰性有机溶剂中使选自环氧乙烷，氧杂环丁烷，N-取代的氮丙啶和N-取代的氮杂环丁烷与杂环化合物与N 2 O 4或N 2 O 5反应，当化合物 与N2O4反应，将产物中的O-或N-硝酸盐取代基或取代基氧化成O-或N-硝酸盐取代基。 杂环化合物上的剩余环碳原子可以是取代或未取代的。 化合物上C和/或N环原子的优选取代基包括烷基，氰基烷基，卤代烷基，硝基烷基和取代的芳基。 还提供了几种新的硝酸酯，包括聚丁二烯的硝化衍生物，其中聚合物中1％至25％的碳原子被连位硝酸酯（-ONO 2）基团取代。

    CONTINUOUS SYNTHESIS OF ISOOCTYL NITRATE IN A FLOW REACTOR
    89.
    发明申请
    CONTINUOUS SYNTHESIS OF ISOOCTYL NITRATE IN A FLOW REACTOR 审中-公开
    在流动反应器中连续合成硝酸异氰酸酯

    公开(公告)号：WO2015134703A1

    公开(公告)日：2015-09-11

    申请号：PCT/US2015/018876

    申请日：2015-03-05

    Applicant: CORNING INCORPORATED

    Inventor： MA, Bing ,  SHEN, Wei ,  WANG, Yanhua ,  ZHANG, Mo

    IPC: C07C201/02 ,  C07C203/04

    CPC classification number: C07C201/02 ,  C07C203/04

    Abstract: A process for synthesizing isooctyl nitrate in a continuous flow reactor comprises flowing a H2SO4-HNO3 mixture within a flow reactor, flowing isooctyl alcohol into said flow reactor so as to mix the isooctyl alcohol with the H2SO4-HNO3 mixture and produce a reaction mixture stream flowing in said reactor, maintaining the reaction mixture stream flowing in said flow reactor at a reaction temperature within in the range -10° to 35°C inclusive, and wherein the residence time of the reaction mixture stream in the flow reactor is greater than or equal to 5 seconds and less than or equal to 40 seconds, and wherein the H2SO4 of the H2SO4-HNO3 mixture is H2SO4 having a concentration of in the range of 85 to 95% inclusive, more desirably 88 to 92% inclusive, most desirably of 90%.

    Abstract translation: 在连续流动反应器中合成硝酸异辛酯的方法包括使流动反应器内的H 2 SO 4 -HNO 3混合物流动，将异辛醇流入所述流动反应器中，以将异辛醇与H 2 SO 4 -HNO 3混合物混合并产生流动的反应混合物流 在所述反应器中，保持反应混合物流在所述流动反应器中流动的反应温度在-10℃至35℃的范围内，并且其中反应混合物流在流动反应器中的停留时间大于或等于 至5秒且小于或等于40秒，并且其中H 2 SO 4 -HNO 3混合物的H 2 SO 4为浓度为85-95％（含）的H 2 SO 4，更优选为88-92％，最优选为90 ％。

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