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1.发明授权가시박으로부터 분리된 신규의 제초활성물질 3-히드록시-9에이치-크산텐-9-원 및 그 분리방법 有权新型天然除草复合物3-羟基-9H-呫吨-9-酮（Sicyos angulatus L.）及其制备方法
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公开(公告)号：KR1020110005043A
公开(公告)日：2011-01-17
申请号：KR1020090062536
申请日：2009-07-09
Applicant: 강원대학교산학협력단
CPC classification number: A01N43/90 , A01N65/30 , B01D11/02 , C07D493/04
Abstract: PURPOSE: A novel herbicidal material, angelicin, isolated from Rumex crispus L. and a method for isolating the same are provided to ensure unique chemical structure and to develop novel herbicide. CONSTITUTION: An herbicide composition contains angelicin or agriculturally acceptable salt thereof as an active ingredient. Angelicin is isolated from Rumex crispus L. A method for isolating angelicin from Rumex crispus L. comprises: a step of extracting Rumex crispus L. with methanol; a step of dissolving methanol extract with ethyl acetate to obtain an ethyl acetate fraction; a step of obtaining a fraction(EC) of herbicidal activity from ethyl acetate fraction using dichloromethane-methanol solution; a step of obtaining a fraction(ECD) from the fraction(EC) using ethylacetate-dichloromethane-methanol solution; a step of obtaining a fraction(ECDA) from the fraction(ECD) using hexane-ethyl acetate-dichloromethane-methanol solution; and a step of identifying the structure of the fraction(ECDA).
Abstract translation: 目的：提供从Rumex crispus L.分离的一种新型除草剂，天竺葵素及其分离方法，以确保独特的化学结构和开发新型除草剂。 构成：除草剂组合物含有作为活性成分的天angel素或其农业上可接受的盐。 天竺葵素是从罗姆氏菌中分离出来的一种方法，用于从罗姆氏菌中分离天angel素，包括：用甲醇萃取芦荟; 用乙酸乙酯溶解甲醇提取物以获得乙酸乙酯级分的步骤; 使用二氯甲烷 - 甲醇溶液从乙酸乙酯部分获得除草活性的级分（EC）的步骤; 使用乙酸乙酯 - 二氯甲烷 - 甲醇溶液从级分（EC）获得级分（ECD）的步骤; 使用己烷 - 乙酸乙酯 - 二氯甲烷 - 甲醇溶液从级分（ECD）获得级分（ECDA）的步骤; 以及鉴定分数（ECDA）的结构的步骤。
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3.发明公开가시박으로부터 분리된 신규의 제초활성물질 3-히드록시-9에이치-크산텐-9-원 및 그 분리방법 有权新型天然抗坏血酸化合物3-羟基-9H-十八烷酮（SICYOS ANGULATUS L.）及其制备方法
公开(公告)号：KR1020120055234A
公开(公告)日：2012-05-31
申请号：KR1020100116849
申请日：2010-11-23
Applicant: 강원대학교산학협력단
CPC classification number: A01N43/16 , A01N65/08 , B01D11/02 , C07D311/80
Abstract: PURPOSE: A new weeding active material 3-hydroxy-9H-xanthene-9-circle which is separated from sicyos angulatus and a separation method thereof are provided to be used as parent compound for herbicide which attacks new mode of action by having different structure from conventional herbicides. CONSTITUTION: A new weeding active material 3-hydroxy-9H-xanthene-9-circle which is separated from sicyos angulatus is separated from Sicyos angulatus L. The herbicide composition contains new compound having herbicidal activity. A separating method of new compound having herbicidal efficacy which is separated from the Sicyos angulatus comprises next steps: a step of extracting leaves or stems of the Sicyos angulatus; a step of obtaining dichloromethane fractions by dissolving methanol extract of the Sicyos angulatus in dichloromethane; a step of obtaining MD fractions which has Rf value of 0.37-0.00; a step of obtaining MDC fractions which has Rf value of 0.17-0.00; and a step of obtaining MDCC fractions which has Rf value of 0.70.
Abstract translation: 目的：提供一种与猕猴桃分离的新的除草活性物质3-羟基-9H-呫吨-9-圆，其分离方法用作除草剂的母体化合物，其通过具有不同的结构从而攻击新的作用模式 常规除草剂。 构成：与水atus atus分离的新的除草活性物质3-羟基-9H-呫吨-9-圆分离出来，除草剂组合物含有具有除草活性的新化合物。 从Sicyos angulatus分离的具有除草效力的新化合物的分离方法包括以下步骤：提取Sicyos angulatus的叶或茎的步骤; 通过将Sicyos angulatus的甲醇提取物溶解在二氯甲烷中获得二氯甲烷馏分的步骤; 获得Rf值为0.37-0.00的MD级分的步骤; 获得具有Rf值为0.17-0.00的MDC级分的步骤; 以及获得Rf值为0.70的MDCC级分的步骤。
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