公开(公告)号：KR100728642B1

公开(公告)日：2007-06-14

申请号：KR1020060025203

申请日：2006-03-20

Applicant: 인하대학교 산학협력단

Inventor： 진형준 ,  명승준 ,  강민성

IPC: B82B3/00 ,  B82Y30/00

Abstract: A process of fabricating a composite of nylon 610 and multi-walled carbon nano-tubes(MWCNT) is provided, by which MWCNT is dispersed uniformly and stably using nonionic surfactant. The process includes the steps of: removing impurities of MWCNT and purifying MWCNT; preparing a dispersant by dispersing the purified MWCNT in distilled water containing surfactant; preparing an organic phase containing carbon tetrachloride and sebacoyl chloride; preparing aqueous composite solution containing hexamethylenediamine and sodium hydroxide; and adding the composite solution to the organic phase to form two separate phases and deriving polymerization at interface of the two phases. The purification provides the carbon nano-tube with purity more than 99% by treating the nano-tube with nitric acid solution and sulfuric acid solution, respectively.

Abstract translation: 提供了一种制备尼龙610和多壁碳纳米管（MWCNT）的复合材料的方法，其中使用非离子表面活性剂使MWCNT均匀且稳定地分散。 该方法包括以下步骤：去除多壁碳纳米管杂质并净化多壁碳纳米管; 通过将纯化的MWCNT分散在含有表面活性剂的蒸馏水中来制备分散剂; 制备含有四氯化碳和癸二酰氯的有机相; 制备含有六亚甲基二胺和氢氧化钠的含水复合溶液; 并将该复合溶液加入到有机相中以形成两个分离相并在两相的界面处导出聚合。 通过用硝酸溶液和硫酸溶液分别处理纳米管，纯化提供纯度超过99％的碳纳米管。

公开(公告)号：KR100746643B1

公开(公告)日：2007-08-06

申请号：KR1020060018094

申请日：2006-02-24

Applicant: 인하대학교 산학협력단

Inventor： 진형준 ,  윤석호 ,  강민성

IPC: B01D71/40 ,  B01D71/00

Abstract: A method for producing a polymeric fibrous membrane from a polymer material by using a simple electrospinning apparatus, and a superhydrophobic fibrous membrane having a contact angle to water of 150 degrees or more by using inherent properties and surface characteristics of fiber and membrane are provided. A method for producing a polystyrene fiber comprises the steps of: preparing a mixed solution of polystyrene and dimethylformamide containing 30 to 40 wt.% of a polystyrene polymer; and electrospinning the mixed solution, wherein the mixed solution is electrospun at a fluid rate of 50 to 150 mul/min, and the electrospinning has an electric field intensity of 16 to 19.6 kV. An apparatus for producing a polystyrene fiber comprises: a syringe pump(14) for applying a predetermined pressure to a polystyrene solution; a capillary tube(12) for spinning a polystyrene solution provided from the syringe pump; a stainless steel needle(13) extending to a lower side of the capillary tube; a high voltage power supply(11) for applying a voltage to the tip of the needle; and a stainless steel rotating drum(15) installed below the needle.

Abstract translation: 本发明提供一种利用简单的静电纺丝装置由高分子材料制造高分子纤维膜的方法以及利用纤维和膜的固有性质和表面特性对水的接触角为150度以上的超疏水性纤维膜。 一种生产聚苯乙烯纤维的方法包括以下步骤：制备含有30至40重量％的聚苯乙烯聚合物的聚苯乙烯和二甲基甲酰胺的混合溶液; 并静电纺丝所述混合溶液，其中所述混合溶液以50至150mul / min的流体速率静电纺丝，并且所述静电纺丝具有16至19.6kV的电场强度。 一种用于生产聚苯乙烯纤维的设备，包括：注射泵（14），用于向聚苯乙烯溶液施加预定压力; 用于旋转从注射器泵提供的聚苯乙烯溶液的毛细管（12） 不锈钢针（13），其延伸到毛细管的下侧; 高压电源（11），用于向针的尖端施加电压; 和安装在针下方的不锈钢旋转鼓（15）。