Abstract:
The present invention relates to a method and an apparatus for manufacturing an iodinated aromatic compound and mono-iodinated benzene through sequential catalyst circulation through sequential catalyst circulation using zeolite-based catalysts, alumina-based catalysts and silicon-based catalysts by mixing or ion-exchanging the catalysts in a weight ratio, by adding oxygen or ozone to the inside of a combustion chamber and oxidizing and generating catalytic materials from room temperature to 700°C to prepare mono-iodinated benzene, wherein the mono-iodinated benzene is isolated and selected from di-iodinated benzene and tri-iodinated benzene by transiodination using a difference of melting points. [Reference numerals] (23) Continuous solid-liquid separator; (28) Mixer; (AA) First direction; (BB) Second direction
Abstract:
PURPOSE: An apparatus for processing exhaust gas and a method for preventing environmental contamination are provided to minimize the generation of wastewater by neutralizing the ammonia of a small amount which is discharged without absorbing to sulfuric acid. CONSTITUTION: A unification line(17) merges an exhaust gas line to one line. A absorptive tower(20) receives exhaust gas which comes out through the unification line and reacts the exhaust gas with water or deionized water. The water or a deionized water injection line is installed on the upper side of the absorptive tower. The water or a deionized water injection line injects the water or the deionized water to the inside of the absorptive tower. A neutralizing tank(24) neutralizes ammonia gas which comes out through the exhaust gas line of the upper side of the absorptive tower.
Abstract:
본 발명은 고순도 일산화질소와 고순도 아산화질소의 제조 방법에 관한 것으로, 공업용 저순도 암모니아를 기화시켜 순도를 높여서 원료로 사용하기 위하여 리보일러, 칼럼 및 냉각기로 구성된 증류탑을 사용하여 고순도 암모이나를 제조하는 하는 제1단계 공정을 거쳐서, 상기 제조된 고순도 암모이나를 촉매가 탑재된 촉매반응기에 투입하면서 산소를 주입하여 부분 산화시켜 NO(일산화질소), N 2 O(아산화질소)를 합성하는 제2단계 공정을 거치고, 촉매반응기에서 반응 후 생산된 혼합가스를 리보일러, 칼럼, 냉각기로 이루어진 증류탑을 사용하여 분리 정제하는 제3단계 공정으로 이루어진 고순도 일산화질소와 아산화질소의 제조방법 및 고순도 일산화질소와 아산화질소의 제조공정에 사용된 되는 고순도 일산화질소와 아산화질소의 제조장치를 제공하는 것이다.
Abstract:
PURPOSE: A method and an apparatus for manufacturing high purity ammonia are provided to continuously produce the ammonia and improve the purity of the ammonia based on a simply facility by installing three step distillation towers. CONSTITUTION: Low purity liquefied ammonia is introduced into a second step distillation tower composed of a reboiler(13), a column(14), and a cooler(15). Water and heavy metal from the low purity liquefied ammonia are moved to the column(18) of a first step distillation tower. The water and the heavy metal are eliminated. The ammonia through the first step distillation tower is introduced into the second step distillation tower. The ammonia passes through the second step distillation tower in order to eliminate low volatile materials from the ammonia. The ammonia is discharged through the discharging hole of a third step distillation tower. The ammonia is liquefied by a cooler(25) in the third step distillation tower and is transferred to a storing tank.
Abstract:
본 발명은 삼염화실란(TCS)을 제조함에 있어서 삼염화실란의 생성에 방해가 되지 않는 발열 반응물질을 더 투입하여 내부 반응에 의한 발열량으로 반응기 히터의 용량을 최소화하거나 제거하여 반응기의 부피를 최소화함으로써 설치공간, 설치비용, 생산원가 및 유지비용을 절감하는데 그 목적 및 효과가 있다. 본 발명은 반도체용 특수가스 및 태양전지용 폴리 실리콘의 주원료인 삼염화실란(TCS)을 효율적으로 제조하기 위해 메탈등급의 규소입자의 크기가 50~ 400mesh이고 순도는 90%이상이며. 수소의 순도는 70%이상이고, 사염화규소(STC)의 순도는 75%이상이고, 염소의 순도는 90%이상의 공업용을 사용하며, 사염화규소가 담겨있는 탱크를 기화온도 이상으로 가열하고, 수소를 사염화규소 탱크로 주입하여 버블링시켜 기화된 사염화규소와 수소가 함께 반응기로 공급되며, 염소는 반응기 전단에서 상기 사염화규소 및 수소와 함께 혼합 공급하거나 반응기 내부로 독립적으로 금속촉매가 장입된 반응기로 공급되고, 반응기를 통과한 가스는 리보일러와 컨덴서를 구비한 증류탑으로 이송되며, 증류탑에서 비등점 차이를 이용하여 삼염화실란과 사염화규소를 분리하여 분리 회수된 사염화규소는 사염화규소 탱크로 재순환시키고, 순도 95% 이상인 삼염화실란은 저장탱크로 이송되도록 구성되어 있다. 삼염화실란, 사염화규소, 염소, 수소, 메탈등급 실리콘
Abstract:
PURPOSE: A manufacturing method of trichlorosilane and the trichlorosilane manufactured thereby are provided to reduce costs for managing and maintaining and installation costs by gaining a high conversion rate of trichlorosilane. CONSTITUTION: A Manufacturing method of trichlorosilane and the trichlorosilane manufactured thereby includes a step for gaining trichlorosilane from a reactor(11) by injecting hydrogen chloride into a reaction and mounting metallic silicon and a palladium catalyst in the reactor. The palladium catalyst is manufactured by drying the palladium metal after dipping the palladium metal in PdCl3 or Pd(NO3) liquid by selecting a carrier among active alumina, zeolite, activated charcoal, diatomite, alumina and silica.
Abstract:
The present invention relates to an absorption reaction material for removing PFC and acid gas which obtained by molding: a composition which is produced by mixing Al2O3 powder and MgO powder in a predetermined wt%; a composition which is produced by mixing Al2O3 powder, MgO powder, and SiO2 powder in a predetermined wt%; and a composition which is produced by mixing Al2O3 powder, MgO powder, and SiO2 powder in a predetermined wt%, and adding more than one from CuO powder, NiO powder, and V2O5 powder to the mixture in a predetermined wt%. The absorption reaction material is molded into a particle size of 10-100 um for processing PFC and acid gas.
Abstract translation:本发明涉及一种通过成型获得的去除PFC和酸性气体的吸收反应材料:通过以预定wt%混合Al 2 O 3粉末和MgO粉末而制备的组合物; 通过以预定wt%混合Al 2 O 3粉末,MgO粉末和SiO 2粉末制造的组合物; 和通过以预定wt%混合Al 2 O 3粉末,MgO粉末和SiO 2粉末并以预定wt%的比例将CuO粉末,NiO粉末和V 2 O 5粉末加入到混合物中而制备的组合物。 吸收反应材料被模制成10-100μm的粒度,用于处理PFC和酸性气体。
Abstract:
PURPOSE: A method and an apparatus for producing high-purity chlorine are provided to quickly prepare a large amount of liquid chlorine and to ensure convenient maintenance of the producing apparatus. CONSTITUTION: A method for producing high-purity chlorine from liquid chlorine or low-purity chlorine produced in electrolysis is as follows. Water, carbon dioxide, hydrochloride, and heavy metal having a high volatilization point are discharged through a vent installed in a reboiler and removed using a first-stage distillation tower(22) consisting of the reboiler(14), a column(18), and a cooler(16). Most of the chlorine gas produced through the first-stage distillation tower is liquefied by a cooler of a second-stage distillation tower(23) and carbon dioxide, oxygen, nitrogen, and hydrogen having a low volatilization point are discharged to a vent installed on an upper side of the second-stage distillation tower. The liquid chlorine is collected in the reboiler and the collected liquid chlorine is transferred to a chlorine storage tank(20).