公开(公告)号：KR100761000B1

公开(公告)日：2007-10-04

申请号：KR1020060061064

申请日：2006-06-30

Applicant: 한국과학기술연구원

Inventor： 이중기 ,  조병원 ,  김형선 ,  우주만 ,  김희정 ,  박성용

IPC: C01B33/025 ,  C01B31/00 ,  H01M4/133 ,  B82Y30/00

CPC classification number: C01B32/05 ,  C01B33/021 ,  C01P2004/80 ,  C01P2006/40 ,  H01M4/362 ,  H01M10/052

Abstract: An improved method for preparing a carbon composite by coating the activated silicon precursor on surfaces of graphite-based or coke-based carbon particles by a plasma spray coating method after activating a silicon precursor by plasma is provided. A preparation method of a carbon composite comprises the processes of: injecting an inert gas and graphite-based or coke-based carbon particles into a reactor on which a rotor is mounted, thereby suspending the carbon particles by a rotary power of the rotor mounted on the reactor; and activating a silicon precursor by plasma, and injecting the activated silicon precursor into the reactor, thereby forming a nano-sized coating layer with a cluster shape on surfaces of the carbon particles. Further, the preparation method comprises a process or spraying the activated silicon precursor by a plasma spray coating method after activating a silicon precursor by plasma. The silicon precursor is a mixture of one or more selected from SiH4, SiH2Cl2, SiH3Cl, SiCl4, Si2Cl6, and Si(OC2H5)4.

Abstract translation: 提供了一种改进的制备碳复合材料的方法，该方法是在通过等离子体激活硅前体之后，通过等离子喷涂法在石墨基或焦炭基碳颗粒的表面上涂覆活性硅前体。 碳复合材料的制备方法包括以下方法：将惰性气体和石墨基或焦炭基碳颗粒注入到其上安装转子的反应器中，从而通过安装在转子上的转子的旋转动力来悬浮碳颗粒 反应堆; 并通过等离子体活化硅前体，并将活化的硅前体注入反应器中，从而在碳颗粒的表面上形成簇状的纳米尺寸涂层。 此外，制备方法包括在通过等离子体激活硅前体之后通过等离子体喷涂法喷射活化的硅前体。 硅前驱体是选自SiH 4，SiH 2 Cl 2，SiH 3 Cl，SiCl 4，Si 2 Cl 6和Si（OC 2 H 5）4中的一种或多种的混合物。