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公开(公告)号：KR1020150110131A
公开(公告)日：2015-10-02
申请号：KR1020140034094
申请日：2014-03-24
Applicant: 한국과학기술원
IPC: B01J23/75 , B01J23/745 , B01J37/04 , B01J37/06
CPC classification number: B01J37/04 , B01J23/745 , B01J23/75 , B01J35/004
Abstract: 본발명은물산화용 Co-Fe 2중층상수산화물광촉매에관한것으로보다상세하게는코발트와철의혼합비율을 2∼4 : 1의비율로구성되는 Co-Fe 2중층상수산화물물산화광촉매를제공한다. 본발명의코발트-철이중층상수산화물촉매가가시광선하에서약 450%의산소를더 발생시킬수 있다. 따라서전이금속을사용한이중층상수산화물의광촉매적효율증가에있어서크게기여할수 있을것으로예상된다.
Abstract translation: 本发明涉及一种用于水氧化的Co-Fe层状双氢氧化物光催化剂，其由钴和铁以2至4：1的混合比组成。根据本发明，Co-Fe层状双氢氧化物催化剂可以产生 在可见光下约450％的氧气。 因此，预期本发明将有助于提高使用过渡金属的层状双氢氧化物光催化剂的效率。
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公开(公告)号：KR100975657B1
公开(公告)日：2010-08-17
申请号：KR1020090062279
申请日：2009-07-08
Applicant: 한국과학기술원
CPC classification number: C01G23/005 , B82Y30/00 , C01P2002/72 , C01P2004/03 , C01P2004/13 , C01P2006/12 , C01P2006/14 , Y02E60/324
Abstract: PURPOSE: A titanate nanostructure and a manufacturing method thereof are provided to control the length and the diameter of the nanostructure by controlling an alkaline solution. CONSTITUTION: A titanate nanostructure is marked with AaBbTixOy. A and B are alkali metals, and a, b, x, and y are fixed numbers. A manufacturing method of the titanate nanostructure comprises the following steps: mixing an alkaline solution with titanium dioxide powder to form a titanium dioxide solution; hydrothermally synthesizing the titanium dioxide solution for 120~180 deg C, to obtain the titanate nanostructure.
Abstract translation: 目的：提供钛酸钠纳米结构及其制造方法，以通过控制碱溶液来控制纳米结构的长度和直径。 构成：钛酸盐纳米结构用AaBbTixOy标记。 A和B是碱金属，a，b，x和y是固定数。 钛酸钠纳米结构的制造方法包括以下步骤：将碱性溶液与二氧化钛粉末混合以形成二氧化钛溶液; 水热合成二氧化钛溶液120〜180℃，得到钛酸盐纳米结构。
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公开(公告)号：KR101437557B1
公开(公告)日：2014-09-15
申请号：KR1020120078747
申请日：2012-07-19
Applicant: 한국과학기술원
IPC: B01J37/02 , C01G23/047 , B82B1/00 , B82B3/00
CPC classification number: H01L21/0228 , H01L29/0603 , H01L51/0045 , Y10S977/811 , Y10S977/823 , Y10S977/90
Abstract: 본 발명은 흑연 구조의 탄소막을 반도체 광촉매 표면에 균일하게 코팅한 물질 및 이의 제조방법에 관한 것이다. 본 발명은 글루코스를 수열합성법과 열분해법(pyrolysis) 방법을 이용하여 반도체 표면에 두께 1 나노미터 이하의 흑연구조의 탄소막을 균일하게 형성시키면서, 탄소막의 지지체가 되는 반도체 광촉매 본연의 구조와 결정성을 그대로 유지하는 것을 특징으로 한다. 본 발명에 의해 개발된 탄소막-반도체 복합체 광촉매의 경우 반도체 광촉매에 발생되는 광전자들을 외부 계의 양성자에게 잘 전달할 수 있게 되므로 전자 정공 재결합을 효과적으로 억제할 수 있으며, 물을 분해하여 수소를 발생시키는 광촉매로서 매우 높을 활성을 가지고 있다.
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公开(公告)号：KR101579092B1
公开(公告)日：2015-12-21
申请号：KR1020140034094
申请日：2014-03-24
Applicant: 한국과학기술원
IPC: B01J23/75 , B01J23/745 , B01J37/04 , B01J37/06
Abstract: 본발명은물산화용 Co-Fe 2중층상수산화물광촉매에관한것으로보다상세하게는코발트와철의혼합비율을 2∼4 : 1의비율로구성되는 Co-Fe 2중층상수산화물물산화광촉매를제공한다. 본발명의코발트-철이중층상수산화물촉매가가시광선하에서약 450%의산소를더 발생시킬수 있다. 따라서전이금속을사용한이중층상수산화물의광촉매적효율증가에있어서크게기여할수 있을것으로예상된다.
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Patent Agency Ranking
公开(公告)号：KR1020140012299A
公开(公告)日：2014-02-03
申请号：KR1020120078747
申请日：2012-07-19
Applicant: 한국과학기술원
IPC: B01J37/02 , C01G23/047 , B82B1/00 , B82B3/00
CPC classification number: H01L21/0228 , H01L29/0603 , H01L51/0045 , Y10S977/811 , Y10S977/823 , Y10S977/90
Abstract: The present invention relates to a semiconductor photocatalyst coated uniformly with a graphitic carbon film on the surface thereof and a fabricating method thereof. The present invention forms a graphitic carbon film having a thickness of 1 nm or less uniformly on the surface of a semiconductor by performing hydrothermal synthesis and pyrolysis on glucose, so as to keep the original structure and crystallinity of the semiconductor photocatalyst which is a support for the carbon film. The carbon film-semiconductor composite photocatalyst fabricated according to the present invention inhibits electron-hole recombination effectively because photoelectrons generated from the semiconductor photocatalyst are transmitted well to protons in an external system; and has high activity as a photocatalyst for generating hydrogen by electrolyzing water.
Abstract translation: 本发明涉及在其表面上均匀地涂覆有石墨碳膜的半导体光催化剂及其制造方法。 本发明通过对葡萄糖进行水热合成和热解而在半导体的表面上均匀地形成厚度为1nm以下的石墨碳膜，以保持作为载体的半导体光催化剂的原始结构和结晶度 碳膜。 根据本发明制造的碳膜 - 半导体复合光催化剂有效地抑制电子 - 空穴复合，因为由半导体光催化剂产生的光电子能良好地传递到外部系统中的质子; 作为用于通过电解水生成氢的光催化剂具有高活性。
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公开(公告)号：KR100995090B1
公开(公告)日：2010-11-18
申请号：KR1020090122650
申请日：2009-12-10
Applicant: 한국과학기술원
CPC classification number: C08F238/00
Abstract: PURPOSE: A synthesis method of a micro-porous triple bond based polymer network is provided to simplify the synthesis method, and to mass produce the polymer network while forming a triple bond at the same time. CONSTITUTION: A synthesis method of a micro-porous triple bond based polymer network(TPN-1) comprises the following steps: inserting tetrakis(4-iodophenyl) methane, CuI, and dichlorobis(triphenylphosphine)peledium(II) to a circular flask, adding piperidine as a solvent before bubbling acetylene gas, and stirring for 12 hours in 60 deg C to initiate the coupling reaction; stirring the outcome for 12 hours without bubbling the acetylene gas, heat-processing before cooling at room temperature, filtering, and washing the outcome with dichloromethane, water, and acetone; and drying the washed product for 23~25 hours, and heat processing for 170~190 minutes in 140~160 deg C.
Abstract translation: 目的：提供一种微孔三键聚合物网络的合成方法，以简化合成方法，同时大量生产聚合物网络同时形成三键。 构造：微孔三键基聚合物网络（TPN-1）的合成方法包括以下步骤：将四（4-碘苯基）甲烷，CuI和二氯双（三苯基膦）pel（II）插入圆形烧瓶中， 在乙炔气体鼓泡前加入哌啶作为溶剂，并在60℃下搅拌12小时以引发偶联反应; 将结果搅拌12小时而不鼓泡乙炔气体，在室温冷却下进行加热处理，过滤并用二氯甲烷，水和丙酮洗涤; 并将洗涤后的产品干燥23〜25小时，在140〜160℃热处理170〜190分钟。
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公开(公告)号：KR101260741B1
公开(公告)日：2013-05-06
申请号：KR1020110036863
申请日：2011-04-20
Applicant: 한국과학기술원
IPC: B01J23/755 , B01J23/72 , B01J37/03 , B01J35/02
Abstract: 본발명은가시광선영역하에서물을산화하는티타늄이삽입된레이어드더블하이드록사이드광촉매의제조방법에관한것으로보다상세하게는금속전구체, 티타늄금속전구체를우레아(urea) 수용액에첨가하고용해시켜용액을얻는단계; 상기의용액을반응시키는단계; 및상기의반응후 냉각시킨다음원심분리기로반응물을분리한후 세척한다음건조시키는단계를포함하는가시광선영역하에서물을산화하는티타늄이삽입된레이어드더블하이드록사이드광촉매의제조방법에관한것이다.
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公开(公告)号：KR1020120119102A
公开(公告)日：2012-10-30
申请号：KR1020110036863
申请日：2011-04-20
Applicant: 한국과학기술원
IPC: B01J23/755 , B01J23/72 , B01J37/03 , B01J35/02
CPC classification number: B01J37/00 , B01J23/70 , B01J35/004
Abstract: PURPOSE: A manufacturing method of titanium embedded layered double hydroxide photo-catalysts is provided to simplify manufacturing processes using nickel or copper, and titanium as metals. CONSTITUTION: A manufacturing method of titanium embedded layered double hydroxide photo-catalysts for oxidizing water under a visible ray region includes the following: a metal precursor and a titanium metal precursor are added into an urea aqueous solution to be dissolved, and a solution is obtained; the solution is reacted to obtain a resultant product; the resultant product is centrifuged by a centrifuge, and a washing process and a drying process are further implemented.
Abstract translation: 目的：提供钛嵌层式双氢氧化物光催化剂的制造方法，以简化使用镍或铜和钛作为金属的制造工艺。 构成：用于在可见光区域氧化水的钛嵌入层状双氢氧化物光催化剂的制造方法包括：将金属前体和钛金属前体加入待溶解的尿素水溶液中，得到溶液 ; 使溶液反应得到所得产物; 将所得产物通过离心机离心，进一步实施洗涤过程和干燥过程。
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公开(公告)号：KR100947832B1
公开(公告)日：2010-03-18
申请号：KR1020090050087
申请日：2009-06-05
Applicant: 한국과학기술원
CPC classification number: C01B21/0605 , C01P2002/72 , C01P2002/85 , C01P2004/03 , C01P2004/04 , C01P2006/42 , B82B3/0009 , B82Y25/00
Abstract: PURPOSE: A method for manufacturing a hybrid of magnetite nanoparticles and carbonnitride nanotube is provided to obtain the hybrid which is uniformly doped on the surface of the carbonnitride nanotube while maintaining superparamagnetism of the magnetite nanoparticles. CONSTITUTION: A method for manufacturing a hybrid of magnetite nanoparticles and carbonnitride nanotube comprises the following steps: manufacturing the carbonnitride nanotube through a plasma chemical vapor deposition process; obtaining the mixture by adding steel acetylacetonate to the mixture after dissolving the carbonnitride nanotube in triethyleneglycol; and manufacturing the hybrid of the magnetite nanoparticle and the carbonnitride nanotube in which the magnetite nanoparticle is doped by cooling the mixture.
Abstract translation: 目的：提供一种用于制造磁铁矿纳米颗粒和碳氮化物纳米管的混合物的方法，以获得均匀掺杂在碳氮纳米管表面上的混合物，同时保持磁铁矿纳米颗粒的超顺磁性。 构成：制造磁铁矿纳米颗粒和碳纳米管纳米颗粒的混合物的方法包括以下步骤：通过等离子体化学气相沉积工艺制造氮化碳纳米管; 在将碳氮化钠纳米管溶解在三乙二醇中后，通过向混合物中加入乙酰丙酮酸锌获得混合物; 并通过冷却混合物来制造掺杂有磁铁矿纳米颗粒的磁铁矿纳米颗粒和碳氮化物纳米管的杂化物。
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