公开(公告)号：KR100992696B1

公开(公告)日：2010-11-05

申请号：KR1020080069786

申请日：2008-07-18

Applicant: 현대자동차주식회사 ,  기아자동차주식회사

Inventor： 이상남

IPC: G01N23/00 ,  G01N1/28 ,  G01N23/05 ,  G01N1/32

Abstract: 본 발명은 보론 합금강에 함유된 보론(B) 원소의 분포도 분석 방법에 관한 것으로서, 시편의 채취 및 마운팅, 검사면 가공 후 시편 검사면에 필름형 검출기를 부착하는 과정을 거치고, 상기 필름형 검출기에 중성자를 조사한 뒤 시편으로부터 분리된 필름형 검출기에 대해 부식, 세척 및 건조, 그리고 광학 현미경으로 관찰하는 과정으로 진행되는 보론 원소의 분포도 분석 방법에 관한 것이다. 본 발명에서는 상기와 같이 표준화된 최적 분석 방법을 제공하게 됨으로써, 시험자의 경험, 숙련도 차이에 따른 방법의 상이성을 배제하여 분석 오차를 최소화할 수 있고, 시험의 신뢰성을 향상시킬 수 있다.
보론, 분포도, 중성자 조사, 필름형 검출기, 광학 현미경

公开(公告)号：KR1020090022957A

公开(公告)日：2009-03-04

申请号：KR1020070088681

申请日：2007-08-31

Applicant: 현대자동차주식회사

Inventor： 장종석 ,  이상남

IPC: G01N1/28 ,  G01N23/223

Abstract: An X-ray fluorescence analysis manufacturing method compress to the press a pulverized work-piece and mold it as disc type after pulverizing the work-piece refrigerated with liquid nitrogen. An X-ray fluorescence analysis manufacturing method comprises a step for collecting a work-piece from a plastic part to be analyzed; a step for pulverizing the refrigerated work-piece after putting the collected work-piece into the liquid nitrogen; a step for molding the pulverized work-piece as the disc type by heating and it pressurizing with the disc forming equipment; and a step for keeping the work-piece of the compacted disc type in desiccators which are blocked with outside.

Abstract translation: 在将用液氮冷却的工件粉碎后，X射线荧光分析制造方法压缩粉碎的工件并将其成型为圆盘型。 X射线荧光分析制造方法包括从要分析的塑料部件收集工件的步骤; 在将收集的工件放入液氮中之后粉碎冷冻工件的步骤; 通过加热将粉碎的工件成型为圆盘型并用盘形成设备加压的步骤; 以及将压实盘型的工件保持在被外部阻挡的干燥器中的步骤。

公开(公告)号：KR1020020094663A

公开(公告)日：2002-12-18

申请号：KR1020010033015

申请日：2001-06-12

Applicant: 현대자동차주식회사

Inventor： 이상남

IPC: G01M7/08

Abstract: PURPOSE: A fall impact test apparatus is provided to achieve improved reliability for entire car in a low temperature region by evaluating impact levels under the low temperature condition, while improving reliability of the test. CONSTITUTION: A fall impact test apparatus(1) comprises an impact unit(10) for providing a preset fall impact load to a test product; a fixing unit(20) including a jig for mounting and fixing the test product, and an impact bar(22) for transmitting impact load of the impact unit to the test product; and a low temperature forming/maintain unit(30) including a low temperature chamber(42) for forming/maintaining a low temperature condition around the test product. The impact unit includes a hoist(110) arranged in the upper portion of the apparatus, which lifts or drops a drop weight(120); the drop weight connected to the hoist through a clamping member(118) including a wire(116), and arranged to be slidable in a vertical direction at a guide post(132); a hammer(122) arranged at the outer bottom of the drop weight, which applies impact load to the impact bar; a base(130) supporting the apparatus; the guide post arranged in a vertical direction on the base; and a support pipe arranged upright on the base, which has a top supporting the guide post.

Abstract translation: 目的：提供一种秋季冲击试验装置，通过评估低温条件下的冲击水平，同时提高试验的可靠性，从而提高低温区域整车的可靠性。 构成：跌倒冲击试验装置（1）包括用于向试验产品提供预设的跌落冲击载荷的冲击装置（10） 包括用于安装和固定测试产品的夹具的固定单元（20）和用于将冲击单元的冲击载荷传递到测试产品的冲击杆（22）; 以及包括用于在所述测试产品周围形成/保持低温条件的低温室（42）的低温成形/维持单元（30）。 冲击单元包括设置在设备的上部的起重机（110），其升降落锤（120）; 通过包括导线（116）的夹紧构件（118）连接到起重机的落锤重量，并且布置成可以在引导柱（132）处沿垂直方向滑动; 设置在所述液滴重物的外部底部的锤子（122），其对冲击杆施加冲击载荷; 支撑所述装置的基座（130） 所述导柱在所述基座上沿垂直方向排列; 以及直立设置在基座上的支撑管，其具有支撑引导柱的顶部。

公开(公告)号：KR1020020047667A

公开(公告)日：2002-06-22

申请号：KR1020000076200

申请日：2000-12-13

Applicant: 현대자동차주식회사

Inventor： 이상남

IPC: C21D9/36

Abstract: PURPOSE: A method for manufacturing a stud bolt for a ball joint is provided which prevents damage through improvement of impact strength and minimizes loss during breakage by quenching and normalizing an SCM435 material so as to solidly manufacture the stud bolt for the ball joint. CONSTITUTION: The method for manufacturing a stud bolt for a ball joint comprises the steps of forming the material into the stud bolt by form rolling or machining an SCM435 material; quenching the formed stud bolt; and stabilizing the structure of the stud bolt by tempering the quenched stud bolt, wherein the quenching means a heat treatment hardening the structure of steel by putting the steel into a quenching agent such as water or oil in the state that steel is heated to a critical temperature or more, thereby rapidly cooling the steel, and the heat treated steel is tempered to secure appropriate toughness since the heat treated steel is very hard, but weak in brittleness and has the unstable structure.

Abstract translation: 目的：提供一种用于制造用于球窝接头的双头螺栓的方法，其通过提高冲击强度来防止损坏，并且通过淬火和标准化SCM435材料来最大限度地减少损坏，以便牢固地制造用于球窝接头的双头螺栓。 构成：用于制造球接头的双头螺栓的方法包括以下步骤：通过轧制或加工SCM435材料将材料形成到双头螺栓中; 淬火形成的双头螺栓; 并且通过对淬火的双头螺栓进行回火来稳定双头螺栓的结构，其中淬火是指通过在钢被加热至关键的状态下将钢放入诸如水或油的淬火剂中而使钢的结构硬化的热处理 温度以上，由此对钢进行快速冷却，由于热处理钢非常硬，脆性弱，结构不稳定，因此对热处理钢进行回火以确保适当的韧性。

公开(公告)号：KR101394680B1

公开(公告)日：2014-05-14

申请号：KR1020120069455

申请日：2012-06-27

Applicant: 현대자동차주식회사

Inventor： 이상남

IPC: G01N1/28 ,  B01J19/12 ,  B01J23/10

Abstract: 본 발명은 엔진 촉매에 사용되는 희토류원소의 함량 분석을 위한 시료 전처리 방법에 관한 것으로, 더욱 상세하게는 유도결합 플라즈마 분광분석기를 이용한 함량 분석시 촉매 내 희토류원소 특히, 프라세오디뮴(Pr)의 정밀한 함량 분석을 위한 시료의 전처리 방법에 관한 것이다.
이에 본 발명은, 촉매 내 함유된 희토류 원소의 함량 분석을 위한 시료 전처리 방법으로서, 촉매 시료를 건조시키는 단계; 상기 건조시킨 시료를 3등분하여 절단하는 단계; 상기 3등분으로 절단한 시료를 조분쇄하는 단계; 상기 조분쇄한 시료를 미분쇄하는 단계; 상기 미분쇄한 시료를 정밀 계량하여서 일정량으로 분취하는 단계; 상기 분취한 각 시료를 혼합산에 투입한 뒤 마이크로웨이브를 조사하여 용해시키는 단계;를 포함하는 것을 특징으로 하는 촉매의 희토류원소 함량 분석을 위한 시료 전처리 방법을 제공한다.

公开(公告)号：KR1020140024182A

公开(公告)日：2014-02-28

申请号：KR1020120090850

申请日：2012-08-20

Applicant: 현대자동차주식회사

Inventor： 이상남

IPC: G01N1/06 ,  G01N23/223 ,  G01N33/38

Abstract: The present invention is to provide a sample preprocessing and analyzing method for analyzing the compound content of a glass material for a vehicle. The present invention can increase the reliability of analysis results by optimally standardizing a sample preprocessing method of a glass material required to analyze a compound using a spectrum analyzer to reduce the errors, can optimize a method for manufacturing a sample by examining the method depending on conditions using fusion-glass bead equipment, and can solve a problem on the analysis errors by optimizing the acceleration voltage of a spectrometric procedure, the selection of detectors, and the time of analysis. To achieve the purpose, the sample preprocessing and analyzing method for analyzing the compound content of a glass material for a vehicle according to the present invention comprises: a step of manufacturing the sample using the fusion-glass bead equipment; a step of cutting the surface of the manufactured sample using a grinding machine; a step of processing the surface of the cut sample using a polishing machine; and a step of quantitatively analyzing the compound of the surface-processed sample using an X-ray fluorescence spectrometer. The present invention can increase the reliability of the analysis results because the method is optimally standardized by using equipment optimized for each step and optimizing the acceleration voltage of an X-ray pipe of the spectrum analyzer, the applied detectors, and the area and time of analysis. [Reference numerals] (AA) Safety glass for a vehicle; (BB) Inside mirror/ Outside mirror/ Sun visor mirror; (CC) Glass fiber (Muffler, battery cover, and EGR cover); (DD) Camera lens; (EE) Lamp bulb

Abstract translation: 本发明提供一种用于分析车辆用玻璃材料的化合物含量的样品预处理分析方法。 本发明可以通过最佳地标准化使用频谱分析仪分析化合物所需的玻璃材料的样品预处理方法以减少误差来提高分析结果的可靠性，可以通过根据条件检查方法来优化制造样品的方法 使用熔融玻璃珠设备，通过优化光谱测定程序的加速电压，检测器的选择和分析时间，可以解决分析误差的问题。 为了达到上述目的，本发明的车辆用玻璃材料的化合物含量分析用样品预处理分析方法包括：使用熔融玻璃珠设备制造样品的步骤; 使用研磨机切割制造的样品的表面的步骤; 使用抛光机处理切割样品的表面的步骤; 以及使用X射线荧光光谱仪定量分析表面处理样品的化合物的步骤。 本发明可以提高分析结果的可靠性，因为该方法通过使用针对每个步骤优化的设备进行最佳标准化，并优化频谱分析仪的X射线管的加速电压，所应用的检测器，以及应用的检测器的面积和时间 分析。 （附图标记）（AA）车辆用安全玻璃; （BB）内镜/外镜/遮阳镜; （CC）玻璃纤维（消声器，电池盖和EGR盖）; （DD）相机镜头; （EE）灯泡

公开(公告)号：KR1020080111720A

公开(公告)日：2008-12-24

申请号：KR1020070060026

申请日：2007-06-19

Applicant: 현대자동차주식회사

Inventor： 이상남

IPC: G01N33/44 ,  G01N35/00 ,  G01N33/00 ,  G01N37/00

Abstract: A pre-treating process for analyzing infinitesimal heavy metals included in a plastic composition is provided to analyze the content of heavy metals easily about the vehicle plastic-related parts and to contribute to the improvement of productivity and vehicle quality. A pre-treating process for analyzing infinitesimal heavy metals included in a plastic composition comprises a step for adding a sulfuric acid (H2SO4) to a plastic composition analyte sample and heating it at 150 ~ 200 ‹C to carbonize; a step for adding a nitric acid (HNO3) and heating it at 250 ~ 300 ‹C; and a step for evaporating and drying the sample at 250 ~ 330 ‹C.

Abstract translation: 提供了用于分析包含在塑料组合物中的无限小重金属的预处理方法，用于容易地分析与汽车塑料相关部件的重金属含量，并有助于提高生产率和车辆质量。 用于分析包含在塑料组合物中的无限小重金属的预处理方法包括将硫酸（H 2 SO 4）加入到塑料组合物分析物样品中并在150〜200℃下加热以进行碳化的步骤; 加入硝酸（HNO 3）并在250〜300℃加热的步骤; 以及在250〜330℃下蒸发和干燥样品的步骤。

公开(公告)号：KR100783943B1

公开(公告)日：2007-12-10

申请号：KR1020060062821

申请日：2006-07-05

Applicant: 현대자동차주식회사

Inventor： 이상남

IPC: G01N33/20 ,  G01N33/00

Abstract: A pre-treating method for analyzing a trace amount of heavy metals in a sealing agent of vehicle is provided to analyze a trace amount of Pb contained in a brake lining accurately by decomposing the sealing agent except the Pb. A pre-treating method for analyzing a trace amount of heavy metals in a sealing agent of vehicle comprises the steps of: (a) after putting a sample and nitric acid in a container, gradually heating it at a temperature of 160-170 deg.C to decompose organic materials; (b) after putting nitric acid and perchloric acid in the container, gradually heating it at a temperature of 160-170 deg.C to decompose organic materials; (c) diluting the solution obtained from the step(b) with distilled water; (d) after putting 25% of ammonium citrate dibasic in the solution, adjusting the pH using ammonia water to be 6.5-6.7; (e) after moving the solution to a separating funnel and putting ammonium sulfate and DDTC(5% sodium diethyldithiocarbamate solution) therein with mixing, adding MIBK(methylisobutylketone) thereto and leaving it for a certain period of time to separate the solution into two layers; (f) throwing an aqueous solution layer from the layers and moving an MIBK layer to a container; (g) after gradually heating the solution to evaporate and dry, adding nitric acid thereto to decompose the MIBK; and (h) after cooling down the solution obtained from the step(g) for a certain period of time and moving the solution to a container having a certain volume, diluting the solution with distilled water and analyzing the quantified sample using an ICP analyzing equipment.

Abstract translation: 提供了一种用于分析车辆密封剂中微量重金属的预处理方法，通过分解除Pb以外的密封剂，精确地分析制动衬片中含有的痕量铅。 用于分析车辆密封剂中微量重金属的预处理方法包括以下步骤：（a）将样品和硝酸放入容器中后，在160-170℃的温度下逐渐加热。 C分解有机材料; （b）将硝酸和高氯酸放入容器中后，在160-170℃的温度下逐渐加热，分解有机物; （c）用蒸馏水稀释步骤（b）获得的溶液; （d）在溶液中加入25％柠檬酸二氢铵后，用氨水调节pH为6.5-6.7; （e）将溶液移至分液漏斗中并混合后加入硫酸铵和DDTC（5％二乙基二硫代氨基甲酸钠溶液），加入MIBK（甲基异丁基酮）并保留一定时间后将溶液分离成两层 ; （f）从层中投掷水溶液层并将MIBK层移至容器; （g）在逐渐加热溶液蒸发干燥后，加入硝酸分解MIBK; 和（h）在将步骤（g）获得的溶液冷却一定时间后，将溶液移至具有一定体积的容器中，用蒸馏水稀释该溶液，并使用ICP分析设备分析定量样品 。

公开(公告)号：KR1020060135132A

公开(公告)日：2006-12-29

申请号：KR1020050054815

申请日：2005-06-24

Applicant: 현대자동차주식회사

Inventor： 이상남

IPC: G21F7/00 ,  G21F1/00

CPC classification number: G21F7/02 ,  G21F1/085 ,  G21F5/10 ,  G21F7/065

Abstract: A radiation shielding apparatus of a CT(Computed Tomography) apparatus is provided to enable a testing person to perform CT test safely by shielding the leakage of radioactive rays. A shielding case(100) has a sealed inner space to accommodate a CT(Computed Tomography) apparatus and shields outer leakage of radioactive rays emitted from the CT apparatus. The shield case has a structure with all walls including a lead plate. In the shielding case, an air ventilation part(120) ventilates heat generated in the CT apparatus to the outside together with inner air. An entrance part introduces a power supply line and a cooling water supply line. The shield case also has a door system.

Abstract translation: 提供CT（计算机断层摄影）装置的放射线屏蔽装置，以使得测试人员能够通过屏蔽放射线的泄漏来安全地执行CT测试。 屏蔽壳（100）具有密封的内部空间以容纳CT（计算机断层扫描）装置，并屏蔽从CT装置发射的放射线的外部泄漏。 屏蔽壳具有包括铅板的所有壁的结构。 在屏蔽壳体中，空气通风部件（120）与内部空气一起将CT装置中产生的热量与外部通风。 入口部分介绍电源线和冷却水供应线。 屏蔽盒还具有门系统。

公开(公告)号：KR100590964B1

公开(公告)日：2006-06-19

申请号：KR1020040032741

申请日：2004-05-10

Applicant: 현대자동차주식회사

Inventor： 이상남

IPC: G01N1/28

Abstract: 본 발명은 철강에 포함된 중금속의 극미량 분석을 위한 전처리 방법에 관한 것으로서, 더욱 상세하게는 극미량의 카드뮴, 납 등의 중금속 분석을 위한 전처리 공정에 있어서 주파수가 2400 ∼ 2600 MHz인 마이크로파를 이용해서 철강 시료를 세밀하게 분해하는 단계와 술폰산기를 교환기로 갖는 강산성 양이온 교환수지를 사용하여 분해된 철강 시료에서 철 매트릭스를 선택적으로 분리하는 단계를 포함하여 이루어짐으로써 ppb(part per billion) 수준까지 중금속 분석이 가능하도록 개선된 철강에 포함된 중금속의 극미량 분석을 위한 전처리 방법에 관한 것이다.
중금속, 강산성 양이온교환 수지, 극미량 분석