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公开(公告)号：US20230166000A1
公开(公告)日：2023-06-01
申请号：US17782439
申请日：2020-12-04
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor： Minguha Dai , Jie J. Liu , Joseph C. Spagnola , Stephen A. O. Olson , Ta-Hua Yu , Junkang J. Liu , Lei Zhang
CPC classification number: A61L15/44 , A61L15/28 , A61L2300/104 , A61L2300/406
Abstract: An article. The article includes a substrate, wherein the substrate having two opposing major surfaces; and particles coated with a metal oxide on the substrate: particles coated with a metal on the substrate; wherein the coated particles are randomly distributed on or in the substrate; and wherein at least some of coated particles are discrete particles.
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公开(公告)号：US10450332B2
公开(公告)日：2019-10-22
申请号：US16114401
申请日：2018-08-28
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor： Thomas P. Klun , Mark A. Roehrig , Joseph C. Spagnola , Alan K. Nachtigal , Charles J. Hoy , Richard J. Pokorny , William J. Hunt , Jason T. Petrin , Paul B. Armstrong , Suresh S. Iyer
IPC: C07F7/00 , C07F7/18 , C08K5/3435 , C09D7/62 , C08F222/22 , C09C3/12 , C08K3/36 , C08K9/06
Abstract: Compounds having hindered amine and oxyalkyl amine light stabilizers can mitigate the adverse effects of actinic radiation, such as visible and ultraviolet light, in particular on substrates such as glass or ceramic substrates. Polymers derived from such compounds. Nanoparticles, substrates, such as glass or ceramic substrates, or both nanoparticles and substrates, having such compounds affixed thereto. Articles containing at least one of such polymers, nanoparticles, substrates, or compounds.
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公开(公告)号：US10011735B2
公开(公告)日：2018-07-03
申请号：US14419324
申请日：2013-03-01
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor： Thomas P. Klun , Alan K. Nachtigal , Joseph C. Spagnola , Mark A. Roehrig , Jennifer K. Schnobrich , Guy D. Joly , Christopher S. Lyons
IPC: H01L51/00 , C09D143/04 , C07F7/18 , H01L51/52 , H01L51/44 , H01L51/10 , B05D3/06 , B32B27/30 , C08J7/04 , C09D133/14 , B05D1/00 , B05D3/10 , C08K3/34 , C09D135/02 , C23C14/08 , C23C14/34 , C23C16/40 , C23C16/44 , C08F130/08 , C09J133/14
CPC classification number: C09D143/04 , B05D1/60 , B05D3/067 , B05D3/068 , B05D3/101 , B32B27/308 , B32B2250/04 , B32B2307/7242 , B32B2307/7244 , C07F7/1804 , C08F130/08 , C08J7/045 , C08J2333/12 , C08K3/34 , C09D133/14 , C09D135/02 , C09J133/14 , C23C14/08 , C23C14/34 , C23C16/40 , C23C16/44 , H01L51/004 , H01L51/107 , H01L51/448 , H01L51/5253 , Y10T428/1064 , Y10T428/31507 , Y10T428/31551 , Y10T428/31609 , Y10T428/31663
Abstract: Diurethane (meth)acrylate-silane precursor compounds prepared by reacting a primary or secondary aminosilane with a cyclic carbonate to yield a hydroxylalkylene-carbamoylalkylene-alkoxysilanes (referred to as a “hydroxylcarbamoylsilane”), which is reacted with a (meth)acrylated material having isocyanate functionality, either neat or in solvent, and optionally with a catalyst, such as a tin compound. Also described are articles including a substrate, a base (co)polymer layer on a major surface of the substrate, an oxide layer on the base (co)polymer layer; and a protective (co)polymer layer on the oxide layer, the protective (co)polymer layer including the reaction product of at least one diurethane (meth)acrylate-silane precursor compound. The substrate may be a (co)polymer film or an electronic device such as an organic light emitting device, electrophoretic light emitting device, liquid crystal display, thin film transistor, or combination thereof. Methods of making the diurethane (meth)acrylate-silane and their use in composite films and electronic devices are described.
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公开(公告)号：US09790396B2
公开(公告)日：2017-10-17
申请号：US14416303
申请日：2013-03-01
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor： Thomas P. Klun , Alan K. Nachtigal , Joseph C. Spagnola , Mark A. Roehrig , Jennifer K. Schnobrich , Guy D. Joly , Christopher S. Lyons
IPC: C09D143/04 , C07F7/18 , H01L51/00 , H01L51/52 , H01L51/44 , H01L51/10 , B05D3/06 , B32B27/30 , C08J7/04 , C09D133/14 , B05D1/00 , B05D3/10 , C08K3/34 , C09D135/02 , C23C14/08 , C23C14/34 , C23C16/40 , C23C16/44 , C08F130/08 , C09J133/14
CPC classification number: C09D143/04 , B05D1/60 , B05D3/067 , B05D3/068 , B05D3/101 , B32B27/308 , B32B2250/04 , B32B2307/7242 , B32B2307/7244 , C07F7/1804 , C08F130/08 , C08J7/045 , C08J2333/12 , C08K3/34 , C09D133/14 , C09D135/02 , C09J133/14 , C23C14/08 , C23C14/34 , C23C16/40 , C23C16/44 , H01L51/004 , H01L51/107 , H01L51/448 , H01L51/5253 , Y10T428/1064 , Y10T428/31507 , Y10T428/31551 , Y10T428/31609 , Y10T428/31663
Abstract: Urethane (multi)-(meth)acrylate (multi)-silane compositions, and articles including a (co)polymer reaction product of at least one urethane (multi)-(meth)acrylate (multi)-silane precursor compound. The disclosure also articles including a substrate, a base (co)polymer layer on a major surface of the substrate, an oxide layer on the base (co)polymer layer; and a protective (co)polymer layer on the oxide layer, the protective (co)polymer layer including the reaction product of at least one urethane (multi) (meth)acrylate (multi)-silane precursor compound. The substrate may be a (co)polymeric film or an electronic device such as an organic light emitting device, electrophoretic light emitting device, liquid crystal display, thin film transistor, or combination thereof. Methods of making urethane (multi)-(meth)acrylate (multi)-silane precursor compounds and their use in composite multilayer barrier films are also described. Methods of using such barrier films in articles selected from a solid state lighting device, a display device, and combinations thereof, are also described.
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公开(公告)号：US20170283444A1
公开(公告)日：2017-10-05
申请号：US15528615
申请日：2015-12-14
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor： Thomas P. Klun , Mark A. Roehrig , Joseph C. Spagnola , Alan K. Nachtigal , Charles J. Hoy , Richard J. Pokorny , William J. Hunt , Jason T. Petrin , Paul B. Armstrong , Suresh S. Iyer
IPC: C07F7/18 , C09C3/12 , C09D7/12 , C08F222/22
CPC classification number: C07F7/1804 , C08F222/22 , C08K3/36 , C08K5/3435 , C08K9/06 , C09C3/12 , C09D7/62
Abstract: Compounds having hindered amine and oxyalkyl amine light stabilizers can mitigate the adverse effects of actinic radiation, such as visible and ultraviolet light, in particular on substrates such as glass or ceramic substrates. Polymers derived from such compounds. Nanoparticles, substrates, such as glass or ceramic substrates, or both nanoparticles and substrates, having such compounds affixed thereto. Articles containing at least one of such polymers, nanoparticles, substrates, or compounds.
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Patent Agency Ranking
公开(公告)号：US10947618B2
公开(公告)日：2021-03-16
申请号：US16266254
申请日：2019-02-04
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor： Joseph C. Spagnola , Mark A. Roehrig , Thomas P. Klun , Alan K. Nachtigal , Christopher S. Lyons , Guy D. Joly
IPC: C23C14/22 , C08J7/04 , C23C14/02 , C23C14/08 , C23C14/12 , C23C14/34 , C23C14/58 , C23C28/00 , C23C14/14 , C08J7/048 , H01J1/70
Abstract: A barrier film including a substrate; a base polymer layer adjacent to the substrate; an oxide layer adjacent to the base polymer layer; a adhesion-modifying layer adjacent to the oxide layer; and a top coat polymer layer adjacent to the adhesion-modifying layer. An optional inorganic layer can be applied over the top coat polymer layer. The inclusion of a adhesion-modifying layer provides for enhanced resistance to moisture and improved peel strength adhesion of the top coat polymer layer to the underlying barrier stack layers.
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公开(公告)号：US10774236B2
公开(公告)日：2020-09-15
申请号：US15955151
申请日：2018-04-17
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor： Thomas P. Klun , Alan K. Nachtigal , Joseph C. Spagnola , Mark A. Roehrig , Jennifer K. Schnobrich , Guy D. Joly , Christopher S. Lyons
IPC: C09D143/04 , H01L51/00 , H01L51/52 , H01L51/44 , H01L51/10 , B05D3/06 , B32B27/30 , C07F7/18 , C09J133/14 , C08J7/04 , C09D133/14 , B05D1/00 , B05D3/10 , C08K3/34 , C09D135/02 , C23C14/08 , C23C14/34 , C23C16/40 , C23C16/44 , C08F130/08
Abstract: Urea (multi)-(meth)acrylate (multi)-silane precursor compounds, synthesized by reaction of (meth)acrylated materials having isocyanate functionality with aminosilane compounds, either neat or in a solvent, and optionally with a catalyst, such as a tin compound, to accelerate the reaction. Also described are articles including a substrate, a base (co)polymer layer on a major surface of the substrate, an oxide layer on the base (co)polymer layer; and a protective (co)polymer layer on the oxide layer, the protective (co)polymer layer including the reaction product of at least one urea (multi)-(meth)acrylate (multi)-silane precursor compound synthesized by reaction of (meth)acrylated materials having isocyanate functionality with aminosilane compounds. The substrate may be a (co)polymer film or an electronic device such as an organic light emitting device, electrophoretic light emitting device, liquid crystal display, thin film transistor, or combination thereof. Methods of making the urea (multi)-(meth)acrylate (multi)-silanes and their use in composite films and electronic devices are described.
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公开(公告)号：US10533111B2
公开(公告)日：2020-01-14
申请号：US15871593
申请日：2018-01-15
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor： Thomas P. Klun , Alan K. Nachtigal , Joseph C. Spagnola , Mark A. Roehrig , Jennifer K. Schnobrich , Guy D. Joly , Christopher S. Lyons
IPC: C09D143/04 , H01L51/00 , H01L51/52 , H01L51/44 , H01L51/10 , B05D3/06 , B32B27/30 , C07F7/18 , C08J7/04 , C09J133/14 , C09D133/14 , B05D1/00 , B05D3/10 , C08K3/34 , C09D135/02 , C23C14/08 , C23C14/34 , C23C16/40 , C23C16/44 , C08F130/08
Abstract: Compositions of matter described as urea (multi)-urethane (meth)acrylate-silanes having the general formula RA—NH—C(O)—N(R4)—R11—[O—C(O)NH—RS]n, or RS—NH—C(O)—N(R4)—R11—[O—C(O)NH—RA]n. Also described are articles including a substrate, a base (co)polymer layer on a major surface of the substrate, an oxide layer on the base (co)polymer layer; and a protective (co)polymer layer on the oxide layer, the protective (co)polymer layer including the reaction product of at least one urea (multi)-urethane (meth)acrylate-silane precursor compound. The substrate may be a (co)polymer film or an electronic device such as an organic light emitting device, electrophoretic light emitting device, liquid crystal display, thin film transistor, or combination thereof. Methods of making such urea (multi)-urethane (meth)acrylate-silane precursor compounds, and their use in composite films and electronic devices are also described. Methods of using multilayer composite films as barrier films in articles selected from solid state lighting devices, display devices, and photovoltaic devices are also described.
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公开(公告)号：US20180362553A1
公开(公告)日：2018-12-20
申请号：US16114401
申请日：2018-08-28
Applicant: 3M Innovative Properties Company
Inventor： Thomas P. Klun , Mark A. Roehrig , Joseph C. Spagnola , Alan K. Nachtigal , Charles J. Hoy , Richard J. Pokorny , William J. Hunt , Jason T. Petrin , Paul B. Armstrong , Suresh S. Iyer
IPC: C07F7/18
CPC classification number: C07F7/1804 , C08F222/22 , C08K3/36 , C08K5/3435 , C08K9/06 , C09C3/12 , C09D7/62
Abstract: Compounds having hindered amine and oxyalkyl amine light stabilizers can mitigate the adverse effects of actinic radiation, such as visible and ultraviolet light, in particular on substrates such as glass or ceramic substrates. Polymers derived from such compounds. Nanoparticles, substrates, such as glass or ceramic substrates, or both nanoparticles and substrates, having such compounds affixed thereto. Articles containing at least one of such polymers, nanoparticles, substrates, or compounds.
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公开(公告)号：US20180138433A1
公开(公告)日：2018-05-17
申请号：US15871560
申请日：2018-01-15
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor： Thomas P. Klun , Suresh Iyer , Alan K. Nachtigal , Joseph C. Spagnola , Mark A. Roehrig
IPC: H01L51/44 , B32B27/08 , B32B27/30 , B32B27/36 , C23C16/44 , C08J7/04 , H01L31/0203 , H01L33/56 , H01L51/52
Abstract: A barrier film including a substrate, a base (co)polymer layer applied on a major surface of the substrate, an oxide layer applied on the base (co)polymer layer, and a protective (co)polymer layer applied on the oxide layer. The protective (co)polymer layer is formed as the reaction product of a first (meth)acryloyl compound and a (meth)acryl-silane compound derived from a Michael reaction between a second (meth)acryloyl compound and an aminosilane. The first and second (meth)acryloyl compounds may be the same. In some embodiments, a multiplicity of alternating layers of the oxide layer and the protective (co)polymer layer may be used. An oxide layer can be applied over the top protective (co)polymer layer. The barrier films provide, in some embodiments, enhanced resistance to moisture and improved peel strength adhesion of the protective (co)polymer layer(s) to the underlying layers. A process of making, and methods of using the barrier film are also described.
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