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    Continuous production of ethylene homopolymers
    2.
    发明授权
    Continuous production of ethylene homopolymers 失效
    连续生产乙烯均聚物

    公开(公告)号：US3917577A

    公开(公告)日：1975-11-04

    申请号：US17532471

    申请日：1971-08-26

    Applicant: BASF AG

    Inventor： TRIESCHMANN HANS-GEORG ,  PFANNMUELLER HELMUT ,  URBAN FRIEDRICH ,  BUECHNER OSKAR ,  STEIGERWALD KLAUS ,  BALL WOLFGANG

    IPC: C08F110/02 ,  C08F4/34 ,  C08F10/02

    CPC classification number: C08F110/02 ,  C08F2/34 ,  C08F2/38

    Abstract: A process for the continuous production of ethylene homopolymers by polymerization of ethylene by means of a polymerization initiator and a polymerization regulator at elevated temperature and superatmospheric pressure in a tubular reactor having two or three successive reaction zones, a mixture of ethylene, the polymerization initiator and the polymerization regulator being introduced continuously at the beginning of each reaction zone. It is characteristic of the process according to the invention that special conditions as regards temperature, pressure, polymerization initiator and polymerization regulator are maintained in the individual reaction zones.

    Abstract translation: 在具有两个或三个连续反应区域的管式反应器中，通过聚合引发剂和聚合调节剂在升高的温度和超大气压下聚合乙烯来连续生产乙烯均聚物的方法，乙烯，聚合引发剂和 聚合调节剂在每个反应区的开始处连续引入。 根据本发明的方法的特征在于，在各个反应区域中保持关于温度，压力，聚合引发剂和聚合调节剂的特殊条件。

    PREPARATION OF HOMOPOLYMERS OF ETHENE AND COPOLYMERS OF ETHENE WITH HIGHER (ALPHA)-MONOOLEFINS USING A ZIEGLER CATALYST SYSTEM
    7.
    发明专利
    PREPARATION OF HOMOPOLYMERS OF ETHENE AND COPOLYMERS OF ETHENE WITH HIGHER (ALPHA)-MONOOLEFINS USING A ZIEGLER CATALYST SYSTEM 未知

    公开(公告)号：CA1251895A

    公开(公告)日：1989-03-28

    申请号：CA479993

    申请日：1985-04-24

    Applicant: BASF AG

    Inventor： BACHL ROBERT ,  WARZELHAN VOLKER ,  SCHWEIER GUENTHER ,  GROPPER HANS ,  BALL WOLFGANG

    IPC: C08F4/00 ,  C08F4/60 ,  C08F4/64 ,  C08F4/642 ,  C08F4/658 ,  C08F4/68 ,  C08F10/00 ,  C08F10/02

    Abstract: Homopolymers and copolymers of ethene are prepared using a Ziegler catalyst system comprising (1) a transition metal catalyst component, (2) an organoaluminum catalyst component and (3) an organohalogen catalyst component, by a method in which the transition metal catalyst component (1) employed is a solid-phase product (VI) obtained by (1.1) first combining (1.1.1) an inorganic oxidic substance ((I), as the carrier, with (1.1.2) a solution (II) consisting of (IIa) a certain oxahydrocarbon and (IIb) a mixture of (IIb1) a vanadium trichloride/alcohol complex, (IIb2) a titanium trihalide or titanium trihalide/alcohol complex and, if required, (IIb3) a zirconium tetrahalide to form a suspension (III), evaporating down this suspension to form a solid-phase intermediate (IV), and (1.2) then (1.2.1) combining the solid-phase intermediate (IV) obtained from (1.1) with (1.2.2) a solution of an organoaluminum compound (V) to form a suspension, the resulting suspended solid-phase product (VI) being the transition metal catalyst component (1).

    PREPARATION OF HOMOPOLYMERS AND COPOLYMERS OF .alpha.- MONOOLEFINS USING A ZIEGLER CATALYST SYSTEM
    8.
    发明专利
    PREPARATION OF HOMOPOLYMERS AND COPOLYMERS OF .alpha.- MONOOLEFINS USING A ZIEGLER CATALYST SYSTEM 未知

    公开(公告)号：CA1244197A

    公开(公告)日：1988-11-01

    申请号：CA473588

    申请日：1985-02-05

    Applicant: BASF AG

    Inventor： WARZELHAN VOLKER ,  BACHL ROBERT ,  BALL WOLFGANG ,  FUNK GUIDO ,  LAUN MARTIN

    IPC: C08F4/00 ,  C08F4/14 ,  C08F4/16 ,  C08F4/20 ,  C08F4/60 ,  C08F4/622 ,  C08F4/64 ,  C08F4/658 ,  C08F4/68 ,  C08F10/00

    Abstract: .alpha.-Monoolefins are polymerized using a Ziegler cataLyst system comprising (1) a transition metal catalyst component and (2) an organoaluminum catalyst component, in which (1) is a solid-phase product (VI) obtained by (1.1) first combining (1.1.1) an inorganic oxidic substance (I), as the carrier, with (1.1.2) a solution (II) consisting of (IIa) an organic solvent and (IIb) a transition metal composition to form a suspension (III), evaporating down this suspension to form a solid-phase intermediate (IV), and (1.2) then (1.2.1) combining the solid-phase intermediate (IV), obtained from (1.1), with (1.2.2) a solution of an organoaluminum compound (V) to form a suspension, the resulting suspended solid-phase product (VI) being the transition metal catalyst component (1). The characteristic feature is that (1) is a solidphase product (VI) obtained using a solution (II) consisting of (IIa) a certain oxahydrocarbon and (IIb) a mixture of (IIb1) a vanadium trichloride/alcohol complex, (IIb2) a titanium trihalide and (IIb3) a zirconium tetrahalide.

    Process for the preparation of a catalyst component containing transition metals for Ziegler catalyst systems
    9.
    发明专利
    Process for the preparation of a catalyst component containing transition metals for Ziegler catalyst systems 未知

    公开(公告)号：DE3332956A1

    公开(公告)日：1985-03-28

    申请号：DE3332956

    申请日：1983-09-13

    Applicant: BASF AG

    Inventor： WARZELHAN VOLKER DR ,  BALL WOLFGANG

    IPC: C08F4/12 ,  C08F4/16 ,  C08F4/20 ,  C08F10/00 ,  C08F4/52 ,  C08F10/14

    Abstract: The invention relates to a process for the preparation of a catalyst component (1) containing transition metals for Ziegler catalyst systems, in which (1.1) first (1.1.1) a finely divided, porous, inorganic oxidic material (I) as support material and (1.1.2) a solution (II) as obtained when (IIa) an alcohol and (IIb) a transition-metal composition are combined, are brought into contact with one another, forming a suspension (III), the latter is evaporated to dryness, forming a solid-phase intermediate (IV), and (1.2) then (1.2.1) the solid-phase intermediate (IV) obtained from step (1.1) and (1.2.2) an organoaluminium compound (V) dissolved in an organic solvent are brought into contact with one another, forming a suspension, the solid-phase product (VI) formed as suspended material being the transition-metal catalyst component (1), characterised in that the transition-metal composition (IIb) employed in step (1.1) is composed in a certain manner of (IIb1) a vanadium trihalide and (IIb2) a zirconium tetrahalide.

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