1.
    发明专利
    未知

    公开(公告)号:DE1196179B

    公开(公告)日:1965-07-08

    申请号:DEB0067291

    申请日:1962-05-18

    Applicant: BASF AG

    Abstract: Adiponitrile is produced by entraining solid free-flowing adipic acid in a current of ammonia and introducing the mixture, at a temperature of below 50 DEG C., into a fluidized bed of a dehydration catalyst at 250-550 DEG C., the bed being fluidized by ammonia, and the total molar ratio of ammonia to adipic acid being at least 2: 1. Variations of the procedure are described. Suitable catalysts are silica gel, boron phosphate and catalysts containing phosphoric acid, and which may be activated by small amounts of alkali metal oxides.

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