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公开(公告)号：DE50006844D1
公开(公告)日：2004-07-22
申请号：DE50006844
申请日：2000-10-27
Applicant: BASF AG
Inventor： RATH PETER , HAHN DIETER , SANDROCK GERHARD , VAN DEYCK FRANS , VANDER STRAETEN BART , DE VREE EDDY
Abstract: Polyisobutene is prepared by cationic polymerization of isobutene and/or isobutene-containing hydrocarbons in the liquid phase in the presence of a complex of BF3 and at least one cocatalyst which is preferably chosen from oxygen-containing compounds, the BF3/cocatalyst complex being produced in situ by adding BF3 and cocatalyst to a reaction stream, wherein BF3 and oxygen-containing cocatalyst are added to the reaction stream via a common binary nozzle comprising an outlet for BF3 and an outlet for the oxygen-containing cocatalyst. The invention also describes a binary nozzle having a centrally arranged outlet for the catalyst.
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公开(公告)号：AU7923300A
公开(公告)日：2001-05-08
申请号：AU7923300
申请日：2000-10-27
Applicant: BASF AG
Inventor： RATH HANS PETER , HAHN DIETER , SANDROCK GERHARD , DEYCK FRANS VAN , STRAETEN BART VANDER , VREE EDDY DE
Abstract: Polyisobutene is prepared by cationic polymerization of isobutene and/or isobutene-containing hydrocarbons in the liquid phase in the presence of a complex of BF3 and at least one cocatalyst which is preferably chosen from oxygen-containing compounds, the BF3/cocatalyst complex being produced in situ by adding BF3 and cocatalyst to a reaction stream, wherein BF3 and oxygen-containing cocatalyst are added to the reaction stream via a common binary nozzle comprising an outlet for BF3 and an outlet for the oxygen-containing cocatalyst. The invention also describes a binary nozzle having a centrally arranged outlet for the catalyst.
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公开(公告)号：MY128424A
公开(公告)日：2007-01-31
申请号：MYPI20004963
申请日：2000-10-20
Applicant: BASF AG
Inventor： RATH HANS PETER DR , HAHN DIETER , SANDROCK GERHARD DR , DEYCK FRANS VAN , STRAETEN BART VANDER , VREE EDDY DE
Abstract: POLYISOBUTENE ARE PREPARED BY THE CONTINUOUS PREPARATION PROCESS, BY POLYMERIZING ISOBUTENE IN THE PRESENCE OF A CATALYST COMPRISING BORON TRIFLUORIDE AND AT LEAST ONE CATALYST IN AN INERT ORGANIC SOLVENT, A)A PART OF THE REACTION MIXTURE OBTAINED THEREBY BEING DISCHARGED CONTONUOUSLY FROM THE POLYMERIZATION REACTOR, B)THE CATALYST BEING SEPARATED FROM THE DISCHARGE AND/OR BEING DEACTIVATED IN THE DISCHARGE, AND C)THE SOLVENT AND ANY UNCOVERTED ISOBUTENE BEING SEPARATED FROM THE DISCHARGE AND RECYCLED TO THE POLYMERIZATION REACTOR, WHEREIN THE RECYCLED SOLVENT AND, IF PRESENT, THE ISOBUTENE ARE SUBJECTED TO A WASH WITH WATER BEFORE RECYCLING TO THE POLYMERIZATION REACTOR AND ARE THEN DRIED.
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公开(公告)号：MY126058A
公开(公告)日：2006-09-29
申请号：MYPI20004962
申请日：2000-10-20
Applicant: BASF AG
Inventor： RATH HANS PETER DR , HAHN DIETER , SANDROCK GERHARD DR , DEYCK FRANS VAN , STRAETEN BART VANDER , VREE EDDY DE
Abstract: POLYISOBUTENE IS PREPARED BY CATIONIC POLYMERIZATION OF ISOBUTENE AND/OR ISOBUTENE-CONTAINING HYDROCARBONS IN THE LIQUID PHASE IN THE PRESENCE OF A COMPLEX OF BF3 AND AT LEAST ONE COCATALYST WHICH IS PREFERABLY CHOSEN FROM OXYGEN-CONTAINING COMPOUNDS, THE BF3/COCATALYST COMPLEX BEING PRODUCED IN SITU BY ADDING BF3 AND COCATALYST TO A REACTION STREAM, WHEREIN BF3 AND OXYGEN-CONTAINING COCATALYST ARE ADDED TO THE REACTION STREAM VIA A COMMON BINARY NOZZLE COMPRISING AN OUTLET FOR BF3 AND AN OUTLET FOR THE OXYGEN-CONTAINING COCATALYST. THE INVENTION ALSO DESCRIBES A BINARY NOZZLE HAVING A CENTRALLY ARRANGED OUTLET FOR THE CATALYST.
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公开(公告)号：AT269365T
公开(公告)日：2004-07-15
申请号：AT00969556
申请日：2000-10-27
Applicant: BASF AG
Inventor： RATH HANS PETER , HAHN DIETER , SANDROCK GERHARD , VAN DEYCK FRANS , VANDER STRAETEN BART , DE VREE EDDY
Abstract: Polyisobutene is prepared by cationic polymerization of isobutene and/or isobutene-containing hydrocarbons in the liquid phase in the presence of a complex of BF3 and at least one cocatalyst which is preferably chosen from oxygen-containing compounds, the BF3/cocatalyst complex being produced in situ by adding BF3 and cocatalyst to a reaction stream, wherein BF3 and oxygen-containing cocatalyst are added to the reaction stream via a common binary nozzle comprising an outlet for BF3 and an outlet for the oxygen-containing cocatalyst. The invention also describes a binary nozzle having a centrally arranged outlet for the catalyst.
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Patent Agency Ranking
公开(公告)号：AT267220T
公开(公告)日：2004-06-15
申请号：AT00975937
申请日：2000-10-27
Applicant: BASF AG
Inventor： RATH HANS PETER , HAHN DIETER , SANDROCK GERHARD , VAN DEYCK FRANS , VANDER STRAETEN BART , DE VREE EDDY
Abstract: Polyisobutenes are prepared by the continuous preparation process, by polymerizing isobutene in the presence of a catalyst comprising boron trifluoride and at least one cocatalyst in an inert organic solvent,a) a part of the reaction mixture obtained thereby being discharged continuously from the polymerization reactor,b) the catalyst being separated from the discharge and/or being deactivated in the discharge, andc) the solvent and any unconverted isobutene being separated from the discharge and recycled to the polymerization reactor,wherein the recycled solvent and, if present, the isobutene are subjected to a wash with water before recycling to the polymerization reactor and are then dried.
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公开(公告)号：AU1388601A
公开(公告)日：2001-05-08
申请号：AU1388601
申请日：2000-10-27
Applicant: BASF AG
Inventor： RATH HANS PETER , HAHN DIETER , SANDROCK GERHARD , DEYCK FRANS VAN , STRAETEN BART VANDER , VREE EDDY DE
Abstract: Polyisobutenes are prepared by the continuous preparation process, by polymerizing isobutene in the presence of a catalyst comprising boron trifluoride and at least one cocatalyst in an inert organic solvent,a) a part of the reaction mixture obtained thereby being discharged continuously from the polymerization reactor,b) the catalyst being separated from the discharge and/or being deactivated in the discharge, andc) the solvent and any unconverted isobutene being separated from the discharge and recycled to the polymerization reactor,wherein the recycled solvent and, if present, the isobutene are subjected to a wash with water before recycling to the polymerization reactor and are then dried.
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公开(公告)号：CA2389249A1
公开(公告)日：2001-05-03
申请号：CA2389249
申请日：2000-10-27
Applicant: BASF AG
Inventor： VANDER STRAETEN BART , DE VREE EDDY , SANDROCK GERHARD , VAN DEYCK FRANS , HAHN DIETER , RATH HANS PETER
Abstract: The invention relates to a continuous method for producing polyisobutene by polymerization of isobutene in the presence of a catalyst from boron trifluoride and at least one cocatalyst in an inert organic solvent. The inventive method comprises the steps of a) discharging, in a continuous manner, a part of the reaction mixture obtained by the polymerization from t he polymerization reactor, b) removing the catalyst from the discharged materia l and/or deactivating it during the discharge, c) removing the solvent and non - reacted isobutene from the discharged material and returning it to the polymerization reactor. The inventive method is further characterized in tha t the returned solvent and optionally the isobutene are first washed with wate r and dried before they are returned to the polymerization reactor.
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公开(公告)号：DE50006524D1
公开(公告)日：2004-06-24
申请号：DE50006524
申请日：2000-10-27
Applicant: BASF AG
Inventor： RATH PETER , HAHN DIETER , SANDROCK GERHARD , VAN DEYCK FRANS , VANDER STRAETEN BART , DE VREE EDDY
Abstract: Polyisobutenes are prepared by the continuous preparation process, by polymerizing isobutene in the presence of a catalyst comprising boron trifluoride and at least one cocatalyst in an inert organic solvent,a) a part of the reaction mixture obtained thereby being discharged continuously from the polymerization reactor,b) the catalyst being separated from the discharge and/or being deactivated in the discharge, andc) the solvent and any unconverted isobutene being separated from the discharge and recycled to the polymerization reactor,wherein the recycled solvent and, if present, the isobutene are subjected to a wash with water before recycling to the polymerization reactor and are then dried.
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公开(公告)号：DE19952030A1
公开(公告)日：2001-05-03
申请号：DE19952030
申请日：1999-10-28
Applicant: BASF AG
Inventor： RATH HANS PETER , HAHN DIETER , SANDROCK GERHARD , DEYCK FRANS VAN , VANDER STRAETEN BART , VREE EDDY DE
Abstract: The invention relates to a method for the continuous production of polyisobutenes by cationic polymerization of isobutenes and/or isobutene-containing hydrocarbons in the liquid phase in the presence of a complex of BF3 and at least one cocatalyst preferably selected from oxygen-containing compounds, whereby the BF3/cocatalyst complex is generated in situ in reaction stream by addition of BF3 and a cocatalyst. The invention is characterized in that BF3 and said oxygen-containing cocatalyst are added to the reaction stream via a common two-material nozzle with an outlet for BF3 and an outlet for said oxygen-containing cocatalyst. The invention also relates to a two-material nozzle with a centrally located outlet for the catalyst.
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