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公开(公告)号:DE59600972D1
公开(公告)日:1999-01-21
申请号:DE59600972
申请日:1996-03-28
Applicant: BASF AG
Inventor: GOETZ WALTER , HOFMANN JUERGEN , KOPIETZ MICHAEL , HORLE HELMUT
IPC: C08G69/26 , C08G69/04 , C08G69/28 , C08G73/10 , G03F7/004 , G03F7/038 , G11B5/48 , G11B21/00 , H05K1/05
Abstract: A polymer based on a dicarboxylic acid and a diamine is prepared by polycondensation in an extruder, by(a) heating a mixture of a dicarboxylic acid having from 4 to 12 carbon atoms and a diamine having from 4 to 12 carbon atoms, which mixture is solid at room temperature and has a residual moisture content of less than 5% by weight, to a temperature in the range from 150 to 400° C. under autogenous pressure in a contrarotating twin-screw extruder to give a product A,(b) feeding the product A to a corotating twin-screw extruder, with the product A being exposed to a temperature in the range from 150 to 400° C. and residual water present and also water from the polycondensation being removed through the degassing openings, to give a product B, with the proviso that the corotating twin-screw extruder has at least two segments having different pressures.
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公开(公告)号:BR9608052A
公开(公告)日:1999-02-17
申请号:BR9608052
申请日:1996-03-28
Applicant: BASF AG
Inventor: KOPIETZ MICHAEL , GOETZ WALTER , HORLE HELMUT , HOFMANN JUERGEN
IPC: C08G69/26 , C08G69/04 , C08G69/28 , C08G73/10 , G03F7/004 , G03F7/038 , G11B5/48 , G11B21/00 , H05K1/05
Abstract: A polymer based on a dicarboxylic acid and a diamine is prepared by polycondensation in an extruder, by(a) heating a mixture of a dicarboxylic acid having from 4 to 12 carbon atoms and a diamine having from 4 to 12 carbon atoms, which mixture is solid at room temperature and has a residual moisture content of less than 5% by weight, to a temperature in the range from 150 to 400° C. under autogenous pressure in a contrarotating twin-screw extruder to give a product A,(b) feeding the product A to a corotating twin-screw extruder, with the product A being exposed to a temperature in the range from 150 to 400° C. and residual water present and also water from the polycondensation being removed through the degassing openings, to give a product B, with the proviso that the corotating twin-screw extruder has at least two segments having different pressures.
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公开(公告)号:ES2125106T3
公开(公告)日:1999-02-16
申请号:ES96909142
申请日:1996-03-28
Applicant: BASF AG
Inventor: GOTZ WALTER , HOFMANN JURGEN , KOPIETZ MICHAEL , HORLE HELMUT
IPC: C08G69/26 , C08G69/04 , C08G69/28 , C08G73/10 , G03F7/004 , G03F7/038 , G11B5/48 , G11B21/00 , H05K1/05
Abstract: A polymer based on a dicarboxylic acid and a diamine is prepared by polycondensation in an extruder, by(a) heating a mixture of a dicarboxylic acid having from 4 to 12 carbon atoms and a diamine having from 4 to 12 carbon atoms, which mixture is solid at room temperature and has a residual moisture content of less than 5% by weight, to a temperature in the range from 150 to 400° C. under autogenous pressure in a contrarotating twin-screw extruder to give a product A,(b) feeding the product A to a corotating twin-screw extruder, with the product A being exposed to a temperature in the range from 150 to 400° C. and residual water present and also water from the polycondensation being removed through the degassing openings, to give a product B, with the proviso that the corotating twin-screw extruder has at least two segments having different pressures.
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公开(公告)号:AT174361T
公开(公告)日:1998-12-15
申请号:AT96909142
申请日:1996-03-28
Applicant: BASF AG
Inventor: GOETZ WALTER , HOFMANN JUERGEN , KOPIETZ MICHAEL , HORLE HELMUT
IPC: C08G69/26 , C08G69/04 , C08G69/28 , C08G73/10 , G03F7/004 , G03F7/038 , G11B5/48 , G11B21/00 , H05K1/05
Abstract: A polymer based on a dicarboxylic acid and a diamine is prepared by polycondensation in an extruder, by(a) heating a mixture of a dicarboxylic acid having from 4 to 12 carbon atoms and a diamine having from 4 to 12 carbon atoms, which mixture is solid at room temperature and has a residual moisture content of less than 5% by weight, to a temperature in the range from 150 to 400° C. under autogenous pressure in a contrarotating twin-screw extruder to give a product A,(b) feeding the product A to a corotating twin-screw extruder, with the product A being exposed to a temperature in the range from 150 to 400° C. and residual water present and also water from the polycondensation being removed through the degassing openings, to give a product B, with the proviso that the corotating twin-screw extruder has at least two segments having different pressures.
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