3.
    发明专利
    未知

    公开(公告)号:DE1154086B

    公开(公告)日:1963-09-12

    申请号:DEB0064725

    申请日:1961-11-10

    Applicant: BASF AG

    Abstract: Glycidamide is prepared by reacting acrylonitrile with hydrogen peroxide at a pH of 7 to 7.5 and treating the reaction mixture with an oxide of a metal of Group IVA, VB, VIB, or VIIB of the Mendel eef Periodic system of elements. Specified metal oxides are tin oxides, lead oxides, vanadium pentoxide, chromium trioxide, tungsten trioxide, manganese oxides. The reaction may be carried out in a saturated alcohol having one to four carbon atoms. The pH may be maintained by adding alkali metal hydroxides, carbonates, and sodium bicarbonate.ALSO:A violet dye of formula is obtained by reacting glycidamide with aniline and coupling the reaction product obtained with diazotized 2,4-dinitroaniline. The dye may be used for dyeing synthetic polyamide fibres.

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