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    Production of auramine salts and auramine salt solutions
    2.
    发明授权
    Production of auramine salts and auramine salt solutions 失效
    制备芳香胺盐和芳香胺盐溶液

    公开(公告)号：US3927095A

    公开(公告)日：1975-12-16

    申请号：US37877573

    申请日：1973-07-12

    Applicant: BASF AG

    Inventor： EISERT MANFRED ,  SCHMEIDL KARL

    IPC: C09B11/00 ,  C09B11/02 ,  C09B55/00 ,  C09B67/26 ,  C09B69/06 ,  C07C119/00

    CPC classification number: C09B69/06 ,  C09B11/02

    Abstract: Production of auramine salts and auramine salt solutions from 4,4''-bisdimethylaminodiphenylmethane or 4,4''bisdiethylaminodiphenylmethane in the presence of sulfur and urea by reaction of the components, with or without the addition of an ammonium salt, taking up the auramine base in a solvent which is not miscible with water and extracting the auramine base by reaction with an acid in water, formamide or glycol with the formation of a salt. The auramine salts and auramine salt solutions obtained are outstandingly suitable for the production of dye liquors.

    Abstract translation: 在硫和尿素存在下，由4,4'-双二甲基氨基二苯基甲烷或4,4'-二二乙基氨基二苯基甲烷制备芳香胺盐和芳胺盐溶液，通过组分的反应，加入或不加入铵盐， 在不与水混溶并通过与水中的酸反应，甲酰胺或二醇形成盐的溶剂中萃取出的溶剂。 所得的芳胺盐和芳族胺盐溶液非常适合生产染液。

    POLYHALOCOPPER PHTHALOCYANINE PIGMENTS
    4.
    发明专利
    POLYHALOCOPPER PHTHALOCYANINE PIGMENTS 未知

    公开(公告)号：AU8008587A

    公开(公告)日：1988-04-28

    申请号：AU8008587

    申请日：1987-10-23

    Applicant: BASF AG

    Inventor： KRANZ JOACHIM ,  SCHMEIDL KARL

    IPC: C09B67/20 ,  C09B67/00 ,  C09B67/12 ,  C09C1/00

    Abstract: Polyhalocopper phthalocyanine pigments of high color strength are prepared by recrystallizing the finely divided agglomerated crude pigment in a heterogeneous aqueous organic phase at elevated temperatures by a process in which the aqueous organic phase used is a heterogeneous mixture of an aliphatic ketone having a total of 3 to 9 carbon atoms and water. The process gives the pigments in the form of spherical granules which are dust-free or have a low dust content. The pigments give deep, brilliant colorations of pure hues.

    Purification of organic salts
    6.
    发明专利
    Purification of organic salts 未知

    公开(公告)号：GB945915A

    公开(公告)日：1964-01-08

    申请号：GB76062

    申请日：1962-01-09

    Applicant: BASF AG

    Inventor： SCHMEIDL KARL ,  SCHENK WALTER

    IPC: B01J20/22 ,  C02F1/54 ,  C07C51/41 ,  C07C51/43 ,  C07C51/47 ,  C07D213/78

    Abstract: In a process for the purification of aqueous solutions of carboxylic acid salts, suspended and colloidally dissolved impurities are removed by mixing the solution with a water-soluble polymer of MW. between 100,000 and 10,000.000 and in an amount of 0.3 to 300 grams of polymer per kilogram of impurity. Polymers mentioned are homopolymers of acrylic acid and acrylamide and copolymers of acrylic or methacrylic acid salts, and esters, acrylonitrile, crotonic, maleic or fumaric acid, alkali metal salts of vinyl phosphoric acid, vinyl pyrrolidone, and alkali metal salts of styrene sulphonic acid. Examples describe the treatment of dipotassium terephthalate with an acrylamide-sodium vinyl sulphonate copolymer; a dipotassium salt of trans-cyclohexane dicarboxylic acid with an acrylamide-acrylic acid copolymer; a dipotassium salt of isocinchomeronic acid with a copolymer of methacrylamide and a condensation product of methacrylamide, formaldehyde-diethylamine quaternised with dimethyl sulphate; and a dipotassium salt of naphthalene-2,6-dicarboxylic acid with a copolymer of acrylamide, methyl acrylate acrylic acid, vinyl pyrrolidone, sodium vinyl sulphonate, methacrylamide, and acrylonitrile. The impurities separate and are filtered off.

    Emulsifiable waxes and their production
    9.
    发明专利
    Emulsifiable waxes and their production 未知

    公开(公告)号：GB967820A

    公开(公告)日：1964-08-26

    申请号：GB394763

    申请日：1963-01-31

    Applicant: BASF AG

    Inventor： SCHMEIDL KARL

    IPC: C08F8/04 ,  C08F8/06

    Abstract: A wax emulsifiable in aqueous media and obtainable by the oxidation of thermally cracked polymers of aliphatic alpha-mono-olefines, ethylene, propylene or butylene, has an acid number of 4-80 and a melt viscosity which is lower than that of the unoxidised material. The polymers may have a molecular weight of 1,000-15,000. Prior to oxidation of the polymers, at least part of the double linkages present in the initial material is saturated by hydrogenation until the bromine number is less than 1 and the hydrogenation may be continuous using a fixed bed catalyst e.g. nickel-diatomaceous earth. Specifications 728,551 and 918,295 are referred to.

    Production of emulsifiable waxes
    10.
    发明专利
    Production of emulsifiable waxes 未知

    公开(公告)号：GB959362A

    公开(公告)日：1964-06-03

    申请号：GB4742062

    申请日：1962-12-17

    Applicant: BASF AG

    Inventor： JAHRSTORFER MICHAEL ,  SCHMEIDL KARL ,  STAIGER GERHARD ,  VOGEL LUDWIG

    IPC: C08F8/06 ,  C08F8/50 ,  C09G1/08

    Abstract: Molten polyolefins having a molecular weight of between 1,000 and 50,000 are oxidized with oxygen or oxygen-containing gas under increased pressure and at a temperature between 130 DEG and 250 DEG C. until 0.5 to 25 kg of oxygen has been absorbed for each 100 kg of polyolefin and the oxidation is carried out with intense agitation with an agitator output of from 1 to 15 kilowatts per 100 kg of polyolefin. Polyolefins exemplified are polyethylene, polypropylene, and a copolymer of ethylene and carbon monoxide containing between 1 and 3 carbonyl groups per 50 ethylene groups. The materials may be made by thermally degrading high molecular weight polyolefins. The products are easily emulsifiable waxes.

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