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    FACILITY AND METHOD FOR THE PRODUCTION OF ANHYDROUS FORMIC ACID
    1.
    发明申请
    FACILITY AND METHOD FOR THE PRODUCTION OF ANHYDROUS FORMIC ACID 审中-公开
    SYSTEM AND METHOD FOR WATER FREE FORMIC生产

    公开(公告)号：WO0155077A3

    公开(公告)日：2002-02-07

    申请号：PCT/EP0100748

    申请日：2001-01-24

    Applicant: BASF AG ,  AUER HEINZ ,  BESSLING BERND ,  HAMMER HANS ,  HASSE HANS ,  SAUER FRIEDRICH ,  VICARI MAXIMILIAN ,  WAGNER GERHARD ,  ADRIAN TILL

    Inventor： AUER HEINZ ,  BESSLING BERND ,  HAMMER HANS ,  HASSE HANS ,  SAUER FRIEDRICH ,  VICARI MAXIMILIAN ,  WAGNER GERHARD ,  ADRIAN TILL

    IPC: C07C51/09 ,  C07C51/44 ,  C07C51/48 ,  C22C14/00 ,  C22C38/00 ,  C22C38/42 ,  C22C38/44 ,  C07C53/02 ,  C22C19/05

    CPC classification number: C22C38/44 ,  C07C51/09 ,  C07C51/44 ,  C07C51/48 ,  C22C14/00 ,  C22C38/001 ,  C22C38/42 ,  C07C53/02

    Abstract: The invention concerns a device and a method for obtaining anhydrous or substantially anhydrous formic acid. Said device is partly or totally made of a zirconium-free material. A liquid of general formula (I) is used as extracting agent, wherein radicals R and R represent alkyl, cycloalkyl, aryl or aralkyl groups or R and R form together with the N atom a heterocyclic five or six-membered ring and in which only one of the radicals is an aryl group and in which R stands for hydrogen or a C1-C4-alkyl group. The device comprises the following equipment: (i) a synthesis reactor (6); (ii) a hydrolysis reactor (1); (iii) a first distillation device (2); (iv) a second distillation device (4); (v) an extraction device (3) and (vi) a third distillation device (5). The material has been selected from the group consisting of the following classes of materials: titanium-palladium alloys, nickel-based materials containing chrome, molybdenum, and/or wolfram and high-alloy, austenitic special chrome-nickel steels containing molybdenum.

    Abstract translation: 本发明涉及一种装置和用于获得无水或基本上无水的甲酸的方法。 该装置部分地或完全地由zirkoniumarmen材料构成。 作为提取手段是通式（I）的液体被使用，其中基团R <1>和R <2>表示或烷基，环烷基，芳基或芳烷基的基团R <1>和R <2>连同 的N原子形成杂环5或6元环，且其中仅一个基团是芳基和<3>，其中R是氢或C1-C4烷基。 该装置包括下列装置（I）的合成反应器（6），（II）的水解反应器（1），（iii）第一蒸馏装置（2），（iv）第二蒸馏装置（4），（v）的提取装置 （3）和（vi）第三蒸馏装置（5）。 所述材料是选自以下组的材料类钛 - 钯合金，铬，钼和/或含钨的镍基材料和含钼高合金化的奥氏体铬 - 镍特种钢。

    3.
    发明专利
    未知

    公开(公告)号：NO20023515L

    公开(公告)日：2002-08-26

    申请号：NO20023515

    申请日：2002-07-23

    Applicant: BASF AG

    Inventor： AUER HEINZ ,  BESSLING BERND ,  HAMMER HANS ,  HASSE HANS ,  SAUER FRIEDRICH ,  VICARI MAXIMILIAN ,  WAGNER GERHARD ,  ADRIAN TILL

    IPC: C07C51/09 ,  C07C51/44 ,  C07C51/48 ,  C22C14/00 ,  C22C38/00 ,  C22C38/42 ,  C22C38/44 ,  C07C

    Abstract: The invention relates to an apparatus and a process for the preparation of anhydrous or substantially anhydrous formic acid. This apparatus is constructed partly or entirely of substantially zirconium-free materials. The extractant employed is a liquid of the general formula I where the radicals R 1 and R 2 are alkyl, cycloalkyl, aryl or aralkyl groups, or R 1 and R 2 jointly, together with the N atom, form a heterocyclic 5- or 6-membered ring, and only one of the radicals is an aryl group, and where R 3 is hydrogen or a C 1 -C 4 -alkyl group. The apparatus has a synthesis reactor ( 6 ), a hydrolysis reactor ( 1 ), three distillation devices ( 2,4,5 ) and an extraction device ( 3 ).

    5.
    发明专利
    未知

    公开(公告)号：NO20023515D0

    公开(公告)日：2002-07-23

    申请号：NO20023515

    申请日：2002-07-23

    Applicant: BASF AG

    Inventor： AUER HEINZ ,  BESSLING BERND ,  HAMMER HANS ,  HASSE HANS ,  SAUER FRIEDRICH ,  VICARI MAXIMILIAN ,  WAGNER GERHARD ,  ADRIAN TILL

    IPC: C07C51/09 ,  C07C51/44 ,  C07C51/48 ,  C22C14/00 ,  C22C38/00 ,  C22C38/42 ,  C22C38/44 ,  C07C

    Abstract: The invention relates to an apparatus and a process for the preparation of anhydrous or substantially anhydrous formic acid. This apparatus is constructed partly or entirely of substantially zirconium-free materials. The extractant employed is a liquid of the general formula I where the radicals R 1 and R 2 are alkyl, cycloalkyl, aryl or aralkyl groups, or R 1 and R 2 jointly, together with the N atom, form a heterocyclic 5- or 6-membered ring, and only one of the radicals is an aryl group, and where R 3 is hydrogen or a C 1 -C 4 -alkyl group. The apparatus has a synthesis reactor ( 6 ), a hydrolysis reactor ( 1 ), three distillation devices ( 2,4,5 ) and an extraction device ( 3 ).

    6.
    发明专利
    未知

    公开(公告)号：DE10002795A1

    公开(公告)日：2001-08-02

    申请号：DE10002795

    申请日：2000-01-24

    Applicant: BASF AG

    Inventor： AUER HEINZ ,  BESLING BERND ,  HAMMER HANS ,  HASSE HANS ,  SAUER FRIEDRICH ,  VICARI MAXIMILIAN ,  WAGNER GERHARD ,  TILL ADRIAN

    IPC: C07C51/09 ,  C07C51/44 ,  C07C51/48 ,  C22C14/00 ,  C22C38/00 ,  C22C38/42 ,  C22C38/44 ,  C07C53/02 ,  C07C233/01 ,  B01J19/02

    Abstract: The invention concerns a device and a method for obtaining anhydrous or substantially anhydrous formic acid. Said device is partly or totally made of a zirconium-free material. A liquid material of general formula (I) is used as extracting agent, wherein radicals R and R represent alkyl, cycloalkyl, aryl or aralkyl groups or R and R together form with the N atom a heterocyclic five or six-membered ring and in which only one of the radicals is an aryl group and in which R stands for hydrogen or a C1-C4-alkyl group. The device comprises the following: (i) a synthesis reactor (6); (ii) a hydrolysis reactor (1); (iii) a first distillation device (2); (iv) a second distillation device (4); (v) an extraction device (3) and (vi) a third distillation device (5).

    Improvements in the production of manganese pentacarbonyl hydride
    7.
    发明专利
    Improvements in the production of manganese pentacarbonyl hydride 未知

    公开(公告)号：GB883280A

    公开(公告)日：1961-11-29

    申请号：GB780459

    申请日：1959-03-06

    Applicant: BASF AG

    Inventor： HIEBER WALTER ,  WAGNER GERHARD

    IPC: C01G45/04

    Abstract: Manganese pentacarbonyl hydride is prepared by dissolving manganese pentacarbonyl in an inert polar organic liquid, adding a free-H ion containing medium and treating the resulting solution with a reducing agent. In a modification the manganese pentacarbonyl may be dissolved in the inert polar organic liquid to which the free-H ion-containing medium has already been added. Reference is made to the use, as inert polar organic liquids, of alcohols, e.g. methyl-, ethyl- or propyl-alcohol or ethers, e.g. diethyl-, or dibutyl-ether, tetrahydrofuran, glycol ethers, dimethyl formamide or dioxane. The free-H ion containing medium may be aqueous solutions of acids, e.g. sulphuric or hydrochloric acids, or organic acids such as formic or acetic, acid salts, e.g. sodium hydrogen sulphate or sodium dihydrogen phosphate or salts which react with water to form acids, for example aluminium trichloride. The reducing agent may be any compound having a reducing action in acid solution, the use of metals, e.g. magnesium and aluminium, metal alloys and amalgams, the compound NaHSO2-CH2O, dithionite and formamidine sulphinic acid being specifically referred to. The reaction may be carried out at normal or elevated temperatures preferably between 5 DEG C. and 100 DEG C. and at normal or increased pressure. Specification 855,065 is referred to.

    9.
    发明专利
    未知

    公开(公告)号：NO327850B1

    公开(公告)日：2009-10-05

    申请号：NO20023515

    申请日：2002-07-23

    Applicant: BASF AG

    Inventor： AUER HEINZ ,  HAMMER HANS ,  BESSLING BERND ,  HASSE HANS ,  SAUER FRIEDRICH ,  WAGNER GERHARD ,  ADRIAN TILL ,  VICARI MAXIMILIAN

    IPC: C07C51/09 ,  C07C51/44 ,  C07C51/48 ,  C22C14/00 ,  C22C38/00 ,  C22C38/42 ,  C22C38/44

    Abstract: The invention relates to an apparatus and a process for the preparation of anhydrous or substantially anhydrous formic acid. This apparatus is constructed partly or entirely of substantially zirconium-free materials. The extractant employed is a liquid of the general formula I where the radicals R 1 and R 2 are alkyl, cycloalkyl, aryl or aralkyl groups, or R 1 and R 2 jointly, together with the N atom, form a heterocyclic 5- or 6-membered ring, and only one of the radicals is an aryl group, and where R 3 is hydrogen or a C 1 -C 4 -alkyl group. The apparatus has a synthesis reactor ( 6 ), a hydrolysis reactor ( 1 ), three distillation devices ( 2,4,5 ) and an extraction device ( 3 ).

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