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    METHOD FOR SEPARATING TRIETHANOLAMIN FROM A MIXTURE OBTAINABLE BY AMMONIA AND ETHYLENE OXIDE REACTION
    2.
    发明申请
    METHOD FOR SEPARATING TRIETHANOLAMIN FROM A MIXTURE OBTAINABLE BY AMMONIA AND ETHYLENE OXIDE REACTION 审中-公开
    方法用于分离三乙醇胺从THROUGH氨氧化乙烯燃混合物的实现

    公开(公告)号：WO2005035481A3

    公开(公告)日：2005-06-02

    申请号：PCT/EP2004011022

    申请日：2004-10-02

    Applicant: BASF AG ,  REIF WOLFGANG ,  HAMMER HANS ,  RUIDER GUENTHER ,  MEIER ANTON ,  BUSKENS PHILIPP ,  FRAUENKRON MATTHIAS

    Inventor： REIF WOLFGANG ,  HAMMER HANS ,  RUIDER GUENTHER ,  MEIER ANTON ,  BUSKENS PHILIPP ,  FRAUENKRON MATTHIAS

    IPC: C07C213/10 ,  C07C215/12

    CPC classification number: C07C213/10 ,  C07C215/12

    Abstract: The invention relates to a method for distillative separation of triethanolamin from a substance mixture consisting of mono- di-, and triethanolamin, ethanolamin-ether and water obtainable by an ammonia and ethylene oxide reaction in a liquid phase at a high pressure and temperature consisting in distilling the substance mixture in two stages. In the first stage, a low-boiling fraction and a high-boiling fraction are withdrawn and discharged, and in the second stage, a medium-boiling fractions is distilled at a triethanolamin content >99.4 % by weight and a diethanolamin content

    Abstract translation: 一种用于三乙醇胺的从图像在压力下，并在一，二和三乙醇胺的升高的温度下混合，以及乙醇胺醚和水，通过氨与环氧乙烷在液相中反应而获得的连续蒸馏分离工艺，其中在两个阶段中蒸馏该混合物 是。 在第一阶段中的低沸点馏分和高沸点馏分被取出和排出并在第二阶段中，中间沸点馏分蒸馏具有<0.2重量％的> 99.4重量％三乙醇胺的含量和二乙醇胺。 该混合物的蒸馏在第一列中优选进行和相互连接该第二塔或间壁塔。

    FACILITY AND METHOD FOR THE PRODUCTION OF ANHYDROUS FORMIC ACID
    3.
    发明申请
    FACILITY AND METHOD FOR THE PRODUCTION OF ANHYDROUS FORMIC ACID 审中-公开
    SYSTEM AND METHOD FOR WATER FREE FORMIC生产

    公开(公告)号：WO0155077A3

    公开(公告)日：2002-02-07

    申请号：PCT/EP0100748

    申请日：2001-01-24

    Applicant: BASF AG ,  AUER HEINZ ,  BESSLING BERND ,  HAMMER HANS ,  HASSE HANS ,  SAUER FRIEDRICH ,  VICARI MAXIMILIAN ,  WAGNER GERHARD ,  ADRIAN TILL

    Inventor： AUER HEINZ ,  BESSLING BERND ,  HAMMER HANS ,  HASSE HANS ,  SAUER FRIEDRICH ,  VICARI MAXIMILIAN ,  WAGNER GERHARD ,  ADRIAN TILL

    IPC: C07C51/09 ,  C07C51/44 ,  C07C51/48 ,  C22C14/00 ,  C22C38/00 ,  C22C38/42 ,  C22C38/44 ,  C07C53/02 ,  C22C19/05

    CPC classification number: C22C38/44 ,  C07C51/09 ,  C07C51/44 ,  C07C51/48 ,  C22C14/00 ,  C22C38/001 ,  C22C38/42 ,  C07C53/02

    Abstract: The invention concerns a device and a method for obtaining anhydrous or substantially anhydrous formic acid. Said device is partly or totally made of a zirconium-free material. A liquid of general formula (I) is used as extracting agent, wherein radicals R and R represent alkyl, cycloalkyl, aryl or aralkyl groups or R and R form together with the N atom a heterocyclic five or six-membered ring and in which only one of the radicals is an aryl group and in which R stands for hydrogen or a C1-C4-alkyl group. The device comprises the following equipment: (i) a synthesis reactor (6); (ii) a hydrolysis reactor (1); (iii) a first distillation device (2); (iv) a second distillation device (4); (v) an extraction device (3) and (vi) a third distillation device (5). The material has been selected from the group consisting of the following classes of materials: titanium-palladium alloys, nickel-based materials containing chrome, molybdenum, and/or wolfram and high-alloy, austenitic special chrome-nickel steels containing molybdenum.

    Abstract translation: 本发明涉及一种装置和用于获得无水或基本上无水的甲酸的方法。 该装置部分地或完全地由zirkoniumarmen材料构成。 作为提取手段是通式（I）的液体被使用，其中基团R <1>和R <2>表示或烷基，环烷基，芳基或芳烷基的基团R <1>和R <2>连同 的N原子形成杂环5或6元环，且其中仅一个基团是芳基和<3>，其中R是氢或C1-C4烷基。 该装置包括下列装置（I）的合成反应器（6），（II）的水解反应器（1），（iii）第一蒸馏装置（2），（iv）第二蒸馏装置（4），（v）的提取装置 （3）和（vi）第三蒸馏装置（5）。 所述材料是选自以下组的材料类钛 - 钯合金，铬，钼和/或含钨的镍基材料和含钼高合金化的奥氏体铬 - 镍特种钢。

    METHOD FOR THE CONTINUOUS PRODUCTION OF METHYL FORMIATE
    4.
    发明申请
    METHOD FOR THE CONTINUOUS PRODUCTION OF METHYL FORMIATE 审中-公开
    METHOD FOR甲基的连续制备

    公开(公告)号：WO0107392A9

    公开(公告)日：2003-04-03

    申请号：PCT/EP0007199

    申请日：2000-07-26

    Applicant: BASF AG ,  AUER HEINZ ,  DAHLHAUS JUERGEN ,  FISCHER KARL ,  HAMMER HANS ,  KELLENBENZ JOCHEN ,  SCHULZ MICHAEL ,  THIEL JOACHIM ,  VICARI MAXIMILIAN

    Inventor： AUER HEINZ ,  DAHLHAUS JUERGEN ,  FISCHER KARL ,  HAMMER HANS ,  KELLENBENZ JOCHEN ,  SCHULZ MICHAEL ,  THIEL JOACHIM ,  VICARI MAXIMILIAN

    IPC: B01D3/00 ,  B01J3/00 ,  B01J3/02 ,  B01J19/00 ,  C07B61/00 ,  C07C29/80 ,  C07C31/04 ,  C07C67/36 ,  C07C69/06

    CPC classification number: C07C67/36 ,  C07C69/06

    Abstract: The invention relates to a method of producing methyl formiate by reacting excess methanol with carbon monoxide under increased pressure and increased temperature in the presence of an alkalimethylate or alkaline earth methylate as the catalyst in a pressure-proof reactor. The inventive method uses at least two reactor elements, preferably countercurrent reactors, at a temperature of approximately 100 DEG C and a pressure of approximately 100 bar in combination with a solid-matter free desalination of the reactor product. The inventive method provides a means for producing methyl formiate of any quality desired and with an excellent production capacity in a very economical and complication-free manner. The invention further relates to a method of solid-matter free desalination and to devices for carrying out the inventive method.

    Abstract translation: 公开了一种用于由过量的甲醇与下在碱金属或碱土金属甲醇盐如在耐压反应器催化剂的存在超大气压力和升高的温度下一氧化碳反应，制备甲酸甲酯的方法，其中操作通过使用至少两个，优选在逆流反应器元件 温度至100℃，并在组合100巴的以任何所需质量非常经济的，无故障的主要生产甲酸甲酯和具有很好的生产能力成为可能的反应器的无固体的脱盐的压力。 此外，描述了用于执行该方法的无固体的脱盐和装置的过程。

    7.
    发明专利
    未知

    公开(公告)号：DE50014201D1

    公开(公告)日：2007-05-10

    申请号：DE50014201

    申请日：2000-07-26

    Applicant: BASF AG

    Inventor： AUER HEINZ ,  DAHLHAUS JUERGEN ,  FISCHER KARL ,  HAMMER HANS ,  KELLENBENZ JOCHEN ,  SCHULZ MICHAEL ,  THIEL JOACHIM ,  VICARI MAXIMILIAN

    IPC: B01D3/00 ,  C07C67/36 ,  B01J3/00 ,  B01J3/02 ,  B01J19/00 ,  C07B61/00 ,  C07C29/80 ,  C07C31/04 ,  C07C69/06

    Abstract: A description is given of a process for preparing methyl formate by reacting excess methanol with carbon monoxide under superatmospheric pressure and at elevated temperature in the presence of alkali metal methoxide or alkaline earth metal methoxide as catalyst in a pressure-rated reactor, in which the use of at least two reactor elements, preferably operated in countercurrent, at about 100° C. and a pressure of about 100 bar in combination with a solids-free desalting of the reaction product makes possible very economical, largely trouble-free production of methyl formate in any desired quality and with a very good production capacity. Furthermore, the process for solids-free desalting and apparatuses for carrying out this process are described.

    10.
    发明专利
    未知

    公开(公告)号：DE50103216D1

    公开(公告)日：2004-09-16

    申请号：DE50103216

    申请日：2001-01-12

    Applicant: BASF AG

    Inventor： AUER HEINZ ,  BESSLING BERND ,  HAMMER HANS ,  HASSE HANS ,  SAUER FRIEDRICH ,  VICARI MAXIMILIAN ,  ADRIAN TILL

    IPC: C07C51/09 ,  C07C51/44 ,  C07C51/48 ,  C07C53/02

    Abstract: The invention relates to a process for obtaining anhydrous or substantially anhydrous formic acid, in which firstly aqueous formic acid is produced by hydrolysis of methyl formate, with the methanol content in the methyl formate having been reduced in advance. The process according to the invention has the special feature that-before the hydrolysis of the methyl formate-the methanol content of the methanol-containing methyl formate is reduced in a distillation column, this distillation column simultaneously being employed for other separation functions during work-up of the formic acid.

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