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    PROCESS FOR WORKING-UP A REACTION MIXTURE COMPRISING POLYETHER POLYOL
    1.
    发明申请
    PROCESS FOR WORKING-UP A REACTION MIXTURE COMPRISING POLYETHER POLYOL 审中-公开
    用于加工包含聚醚多元醇的反应混合物的方法

    公开(公告)号：WO2013087782A2

    公开(公告)日：2013-06-20

    申请号：PCT/EP2012/075411

    申请日：2012-12-13

    Applicant: BASF SE ,  CHILEKAR, Vinit ,  VOß, Hartwig ,  KUHN, Jelan ,  DE COLVANAER, Ann ,  BRODHAGEN, Andreas

    Inventor： CHILEKAR, Vinit ,  VOß, Hartwig ,  KUHN, Jelan ,  DE COLVANAER, Ann ,  BRODHAGEN, Andreas

    IPC: C08G65/00

    CPC classification number: C08G65/30 ,  C08G65/2648

    Abstract: The invention relates to a process for working-up a reaction mixture (5) comprising polyetherol and dissolved alkali metal comprising catalyst, wherein at least alkali metal ions of the dissolved alkali metal comprising catalyst are partially or completely removed from the mixture by a membrane separation process, the process comprising following steps: (a) feeding the reaction mixture (5) comprising polyetherol and dissolved alkali metal comprising catalyst into a first chamber (1) of a separation unit (3), (b) feeding a solvent into a second chamber (7) of the separation unit (3), the first chamber (1) and the second chamber (7) being separated by a membrane (9), (c) transporting at least the alkali metal ions of the alkali metal comprising catalyst from the first chamber (1) into the second chamber by passing through the membrane (9).

    Abstract translation: 本发明涉及一种用于处理包含聚醚醚和包含催化剂的溶解的碱金属的反应混合物（5）的方法，其中至少包含催化剂的溶解的碱金属的碱金属离子通过膜分离部分或完全从混合物中除去 方法包括以下步骤：（a）将包含聚乙烯和包含催化剂的溶解的碱金属的反应混合物（5）进料到分离单元（3）的第一室（1）中，（b）将溶剂进料到第二 分离单元（3）的室（7），第一室（1）和第二室（7）被隔膜（9）隔开，（c）至少输送包含催化剂的碱金属的碱金属离子 从第一腔室（1）通过膜（9）进入第二腔室。

    PROCESS FOR A CONTINUOUS PRODUCTION OF POLYETHEROLS
    6.
    发明申请
    PROCESS FOR A CONTINUOUS PRODUCTION OF POLYETHEROLS 审中-公开
    连续生产聚醚的方法

    公开(公告)号：WO2013010971A1

    公开(公告)日：2013-01-24

    申请号：PCT/EP2012/063866

    申请日：2012-07-16

    Applicant: BASF SE ,  CHILEKAR, Vinit ,  BEY, Oliver ,  BRODHAGEN, Andreas ,  LÖFFLER, Achim ,  AHMADNIAN, Fatemeh ,  BÖHLING, Ralf ,  GROßMANN, Christoph ,  KAMMEL, Ulrich ,  ADELMANN, Ronald ,  OSTROWSKI, Thomas ,  JOSHI, Milind ,  WATERS, Gerrit ,  MECKELNBURG, Dirk

    Inventor： CHILEKAR, Vinit ,  BEY, Oliver ,  BRODHAGEN, Andreas ,  LÖFFLER, Achim ,  AHMADNIAN, Fatemeh ,  BÖHLING, Ralf ,  GROßMANN, Christoph ,  KAMMEL, Ulrich ,  ADELMANN, Ronald ,  OSTROWSKI, Thomas ,  JOSHI, Milind ,  WATERS, Gerrit ,  MECKELNBURG, Dirk

    IPC: C08G65/00

    CPC classification number: C08G65/2609 ,  C08G65/2696

    Abstract: The invention relates to a process for a continuous production of polyetherols comprising the steps of reacting of an alcohol (3) with a starter (5) or an alkoxylated precursor to give a mixture comprising an alcoholate and water, removing the water from the mixture by distillation,if appropriate feeding the alcoholate into a bubble column (23), having an inclination of from 0 to 90 to the horizontal, the bubble column (23)being divided into at least two compartments (25), wherein the compartments (25) are divided from each other by a dividing wall (27), the dividing wall (27) having a height, that liquid can flow over the dividing wall (27) from one compartment (25) into an adjacent compartment, feeding of alkylene oxide into at least one compartment (25) at the bottom of the compartment such that the alkylene oxide rises in the alcoholate, reacting of the alkylene oxide with the alcoholate or a secondary product being formed by the reaction of the alcoholate with alkylene oxide to give the polyetherol, discharging the reaction product from the bubble column (23).

    Abstract translation: 本发明涉及一种连续生产聚醚醚的方法，包括以下步骤：使醇（3）与起始物（5）或烷氧基化前体反应，得到包含醇化物和水的混合物，通过 蒸馏，如果适当地将醇化物进料到气泡塔（23）中，其具有0至90°相对于水平面的倾斜度，气泡塔（23）被分成至少两个室（25），其中隔室（25） 通过分隔壁（27）彼此分开，分隔壁（27）具有高度，液体可以在分隔壁（27）上从一个隔室（25）流到相邻的隔室中，将烯化氧进料到 在室的底部的至少一个隔间（25），使得烯化氧在醇化物中升高，烯化氧与醇化物的反应或通过醇化物与烯化氧的反应形成的次级产物至gi 然后将聚合物从气泡塔（23）排出。

    PROCESS FOR A CONTINUOUS PRODUCTION OF POLYETHEROLS
    10.
    发明公开
    PROCESS FOR A CONTINUOUS PRODUCTION OF POLYETHEROLS 有权
    方法用于连续生产聚醚

    公开(公告)号：EP2734570A1

    公开(公告)日：2014-05-28

    申请号：EP12735146.8

    申请日：2012-07-16

    Applicant: BASF SE

    Inventor： CHILEKAR, Vinit ,  BEY, Oliver ,  BRODHAGEN, Andreas ,  LÖFFLER, Achim ,  AHMADNIAN, Fatemeh ,  BÖHLING, Ralf ,  GROßMANN, Christoph ,  KAMMEL, Ulrich ,  ADELMANN, Ronald ,  OSTROWSKI, Thomas ,  JOSHI, Milind ,  WATERS, Gerrit ,  MECKELNBURG, Dirk

    IPC: C08G65/00

    CPC classification number: C08G65/2609 ,  C08G65/2696

    Abstract: The invention relates to a process for a continuous production of polyetherols comprising the steps of reacting of an alcohol (3) with a starter (5) or an alkoxylated precursor to give a mixture comprising an alcoholate and water, removing the water from the mixture by distillation,if appropriate feeding the alcoholate into a bubble column (23), having an inclination of from 0 to 90 to the horizontal, the bubble column (23)being divided into at least two compartments (25), wherein the compartments (25) are divided from each other by a dividing wall (27), the dividing wall (27) having a height, that liquid can flow over the dividing wall (27) from one compartment (25) into an adjacent compartment, feeding of alkylene oxide into at least one compartment (25) at the bottom of the compartment such that the alkylene oxide rises in the alcoholate, reacting of the alkylene oxide with the alcoholate or a secondary product being formed by the reaction of the alcoholate with alkylene oxide to give the polyetherol, discharging the reaction product from the bubble column (23).

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