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    A PROCESS FOR THE PREPARATION OF PROPYLENE OXIDE
    3.
    发明申请
    A PROCESS FOR THE PREPARATION OF PROPYLENE OXIDE 审中-公开
    一种制备环氧丙烷的方法

    公开(公告)号：WO2017140774A1

    公开(公告)日：2017-08-24

    申请号：PCT/EP2017/053492

    申请日：2017-02-16

    Applicant: BASF SE

    Inventor： RIEDEL, Dominic ,  TELES, Joaquim H. ,  SCHELLING, Heiner ,  WEGERLE, Ulrike ,  MÜLLER, Ulrich ,  PARVULESCU, Andrei-Nicolae ,  MANNWEILER, Jochen ,  HENN, Timo ,  LÜDERITZ, Thomas ,  WÖRZ, Nicolai Tonio ,  MÜLLER, Christian ,  WEBER, Markus ,  URBANCZYK, Daniel

    IPC: C07D301/12 ,  C07D301/36

    CPC classification number: C07D301/12 ,  C07D301/36

    Abstract: A continuous process for the preparation of propylene oxide, comprising a start-up stage and normal run stage, wherein the normal run stage comprises (i) continuously providing a liquid feed stream comprising propene, hydrogen peroxide, acetonitrile, a formate salt, water and optionally propane, wherein in the liquid feed stream, the molar amount of the formate salt relative to the molar amount of hydrogen peroxide at a given point of time during the normal run stage is a N (Fo/H 2 O 2 ); (ii) continuously passing the liquid feed stream provided in (i) into an epoxidation zone comprising a catalyst comprising a titanium zeolite having framework type MWW, and subjecting the liquid feed stream to epoxidation reaction conditions in the epoxidation zone, obtaining a reaction mixture comprising propylene oxide, acetonitrile, water, the formate salt, optionally propene, and optionally propane; (iii) continuously removing an effluent stream from the epoxidation zone, the effluent stream comprising propylene oxide, acetonitrile, water, at least a portion of the formate salt, optionally propene, and optionally propane; wherein the normal run stage is characterized in an average rate of change of a N (Fo/H 2 O 2 ) of less than 0 h -1 .

    Abstract translation: 一种用于制备环氧丙烷的连续方法，其包括启动阶段和正常运行阶段，其中正常运行阶段包括（i）连续提供包含丙烯，过氧化氢， 乙腈，甲酸盐，水和任选的丙烷，其中在液体进料流中，相对于在正常运行阶段期间的给定时间点的过氧化氢的摩尔量，甲酸盐的摩尔量是N （F0 / H <子> 2 0 <子> 2 ）; （ii）将（i）中提供的液体进料流连续通入包含催化剂的环氧化区中，所述催化剂包含具有骨架型MWW的钛沸石，并使液体进料流在环氧化区中经受环氧化反应条件，获得反应混合物，所述反应混合物包含 环氧丙烷，乙腈，水，甲酸盐，任选的丙烯和任选的丙烷; （iii）连续地从环氧化区中除去流出物流，所述流出物流包含环氧丙烷，乙腈，水，至少一部分甲酸盐，任选的丙烯和任选的丙烷; 其中所述正常运行阶段的特征在于小于0小时的αN（Fo / H2θO 2）的平均变化率 -1

    CHA TYPE ZEOLITIC MATERIALS AND METHODS FOR THEIR PREPARATION USING COMBINATIONS OF CYCLOALKYL- AND TETRAALKYLAMMONIUM COMPOUNDS
    6.
    发明申请
    CHA TYPE ZEOLITIC MATERIALS AND METHODS FOR THEIR PREPARATION USING COMBINATIONS OF CYCLOALKYL- AND TETRAALKYLAMMONIUM COMPOUNDS 审中-公开
    CHA类型的ZEOLITIC材料及其使用环己基 - 和四氨基亚甲基化合物的组合制备方法

    公开(公告)号：WO2015185625A2

    公开(公告)日：2015-12-10

    申请号：PCT/EP2015/062377

    申请日：2015-06-03

    Applicant: BASF SE

    Inventor： FEYEN, Mathias ,  YANG, Jeff ,  RUETZ, Roger ,  MÜLLER, Ulrich

    IPC: C01B39/48

    CPC classification number: C01B39/48 ,  B01J20/18 ,  B01J20/3057 ,  B01J20/3085 ,  B01J29/7015 ,  B01J29/763 ,  B01J35/002 ,  B01J35/023 ,  B01J37/0018 ,  B01J37/0246 ,  B01J39/02 ,  B01J39/14 ,  B01J2229/186 ,  B01J2229/42

    Abstract: The present invention relates to a process for the preparation of a zeolitic material having a CHA-type framework structure comprising YO 2 and X 2 O 3 , wherein said process comprises the steps of: (1) providing a mixture comprising one or more sources for YO 2 , one or more sources for X 2 O 3 , one or more tetraalkylammonium cation R 1 R 2 R 3 R 4 N + -containing compounds, and one or more tetraalkylammonium cation R 5 R 6 R 7 R 8 N + -containing compounds as structure directing agent; (2) crystallizing the mixture obtained in step (1) for obtaining a zeolitic material having a CHA-type framework structure; wherein Y is a tetravalent element and X is a trivalent element, wherein R 1 , R 2 , R 3 , R 4 , R 5 , R 6 , and R 7 independently from one another stand for alkyl, and wherein R 8 stands for cycloalkyl, as well as to zeolitic materials which may be obtained according to the inventive process and to their use.

    Abstract translation: 本发明涉及一种制备具有包含YO 2和X 2 O 3的CHA型骨架结构的沸石材料的方法，其中所述方法包括以下步骤：（1）提供包含一种或多种YO 2， 更多的X2O3，一种或多种四烷基铵阳离子R1R2R3R4N +的化合物来源，以及一种或多种四烷基铵阳离子R5R6R7R8N +化合物作为结构导向剂; （2）使步骤（1）中得到的混合物结晶得到具有CHA型骨架结构的沸石材料; 其中Y是四价元素，X是三价元素，其中R 1，R 2，R 3，R 4，R 5，R 6和R 7彼此独立地代表烷基，并且其中R8代表环烷基，以及沸石材料， 可以根据本发明的方法和它们的用途获得。

    METHOD AND USE FOR THE TERTIARY MINERAL OIL PRODUCTION BY MEANS OF METAL-ORGANIC FRAMEWORK MATERIALS
    7.
    发明申请
    METHOD AND USE FOR THE TERTIARY MINERAL OIL PRODUCTION BY MEANS OF METAL-ORGANIC FRAMEWORK MATERIALS 审中-公开
    方法和使用金属有机框架材料的初步矿物油生产

    公开(公告)号：WO2015083113A1

    公开(公告)日：2015-06-11

    申请号：PCT/IB2014/066586

    申请日：2014-12-04

    Applicant: BASF SE ,  BASF CHINA COMPANY LIMITED

    Inventor： MAURER, Stefan ,  KIMURA, Riichiro ,  PARVULESCU, Andrei-Nicolae ,  REINHARDT, Caroline ,  SIGGEL, Lorenz ,  MÜLLER, Ulrich

    IPC: C09K8/58 ,  C07D233/58

    CPC classification number: C07D233/58 ,  C09K8/58

    Abstract: The invention relates to a method for tertiary mineral oil production, in which an aqueous suspension, comprising at least one porous metal-organic framework material,is injected through at least one injection borehole into a mineral oil deposit, and crude oil is withdrawn from the deposit through at least one production borehole. The invention further relates to the use of an aqueous suspension, comprising at least one porous metal-organic framework material. The invention further relates to the use of at least one porous metal-organic framework material or an aqueous suspension for tertiary mineral production.

    Abstract translation: 本发明涉及一种用于三次矿物油生产的方法，其中包含至少一种多孔金属 - 有机骨架材料的水性悬浮液通过至少一个注入孔注入矿物油沉积物中，并将原油从 通过至少一个生产井眼沉积。 本发明还涉及包含至少一种多孔金属 - 有机骨架材料的水性悬浮液的用途。 本发明还涉及至少一种多孔金属 - 有机骨架材料或水性悬浮液用于三次矿物生产的用途。

    METHOD FOR UPTAKING A SPILLED LIQUID
    8.
    发明申请
    METHOD FOR UPTAKING A SPILLED LIQUID 审中-公开
    一种溢出液体的方法

    公开(公告)号：WO2015025250A1

    公开(公告)日：2015-02-26

    申请号：PCT/IB2014/063911

    申请日：2014-08-14

    Applicant: BASF SE ,  BASF CHINA COMPANY LIMITED

    Inventor： MAURER, Stefan ,  KIMURA, Riichiro ,  PARVULESCU, Andrei-Nicolae ,  PETRY, Julia ,  SIGGEL, Lorenz ,  MÜLLER, Ulrich

    IPC: C02F1/28 ,  B01J20/26 ,  B01D15/00

    CPC classification number: B01J20/28042 ,  B01J20/226 ,  C02F1/285 ,  C02F1/40 ,  C02F2101/32 ,  C02F2103/365

    Abstract: The present invention relates to a method for at least partly uptaking a spilled liquid comprising at least one liquid hydrocarbon, the method comprising the step of contacting the at least one liquid hydrocarbon with a binder agent comprising at least one porous metal-organic framework material, wherein the at least one metal-organic framework material comprises at least one organic compound coordinated to at least one metal ion, wherein the at least one organic com- pound is based on imidazole, which is unsubstituted or substituted with one or more substituents independently selected from the group consisting of C 1-6 alkyl, phenyl and benzyl. The invention further relates to the use of such a binder agent for at least partly uptaking the liquid.

    Abstract translation: 本发明涉及至少部分吸收包含至少一种液体烃的溢出液体的方法，该方法包括使至少一种液态烃与包含至少一种多孔金属 - 有机骨架材料的粘合剂接触的步骤， 其中所述至少一种金属 - 有机骨架材料包含与至少一种金属离子配位的至少一种有机化合物，其中所述至少一种有机化合物是基于咪唑，其是未取代的或被一个或多个独立选择的取代基取代的取代基 由C1-6烷基，苯基和苄基组成。 本发明还涉及这种粘合剂用于至少部分吸收液体的用途。

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