-
公开(公告)号：JP2014141494A
公开(公告)日：2014-08-07
申请号：JP2014031217
申请日：2014-02-21
Applicant: Basf Se , ビーエーエスエフ ソシエタス・ヨーロピアBasf Se
Inventor： HEIDI EMILIA SAXELL , ERK PETER , CLAUDE TARANTA , KROEHL THOMAS , COX GERHARD , MARTIN SUKOPP , STEFAN SCHERER , ANTTI OJALA , GAUTAM R DESIRAJU , RAHUL BANERJEE , PRASHANT M BHATT
IPC: C07D231/38 , A01N47/02 , A01P7/04 , A61K9/10 , A61K31/415 , A61P33/00 , A61P33/10 , A61P33/14
CPC classification number: A01N43/56 , A01N47/02 , A01N2300/00
Abstract: PROBLEM TO BE SOLVED: To provide a fipronyl crystal allowing easy filtration and drying with less dust in a production procedure and a composition which is blended with the crystal, has formulation stability and is for insecticidal and parasiticidal mixtures.SOLUTION: A solid fipronyl is present as a monoclinic system having a center-symmetry space group C2/c, shows a specific reflection in an X-ray powder diffraction diagram recorded at 25°C by using Cu-Kα radiation rays and contains at least 85 wt.% of a crystal transformation I of fipronyl. A method of producing the crystal transformation I comprises dissolving a solid fipronyl different from the crystal transformation I in a solvent selected from one or more of alcohols, acetonitrile(AN), dimethylsulfoxide(DMSO), one or more of benzene derivatives, etc. and crystallizing from the resultant solution. When the solvent is AN, crystallization is carried out at 40°C or lower. When the solvent is DMSO, crystallization is carried out at 80°C or lower.
Abstract translation: 要解决的问题：提供一种氟虫腈基晶体，其允许在制备方法中容易地过滤和干燥较少的粉尘，并且与晶体混合的组合物具有制剂的稳定性，并且是杀虫剂和杀寄生虫剂的混合物。解决方案：存在固体氟虫基 作为具有中心对称空间群C2 / c的单斜晶系，通过使用Cu-Kα射线在25℃记录的X射线粉末衍射图中显示特定的反射，并含有至少85重量％的结晶 氟吡酮的转化I。 制造晶体转变I的方法包括将不同于晶体转变I的固体氟虫酰基溶解在选自醇，乙腈（AN），二甲基亚砜（DMSO），一种或多种苯衍生物等中的一种或多种的溶剂中，以及 从所得溶液中结晶。 当溶剂为AN时，在40℃或更低温度下进行结晶。 当溶剂为DMSO时，在80℃或更低温度下进行结晶。
-
公开(公告)号：JP2014139189A
公开(公告)日：2014-07-31
申请号：JP2014031222
申请日：2014-02-21
Applicant: Basf Se , ビーエーエスエフ ソシエタス・ヨーロピアBasf Se
Inventor： HEIDI EMILIA SAXELL , ERK PETER , CLAUDE TARANTA , KROEHL THOMAS , COX GERHARD , MARTIN SUKOPP , DESIRAJU GAUTAM R , RAHUL BANERJEE , BHATT PRASHANT M
IPC: C07D231/44 , A01N25/04 , A01N25/12 , A01N47/02 , A01P5/00 , A01P7/04 , A61K31/415 , A61P33/10 , A61P33/14
CPC classification number: A01N47/02 , A01N2300/00
Abstract: PROBLEM TO BE SOLVED: To provide a novel crystal-transformed fipronil and an insecticidal and a parasiticidal composition.SOLUTION: A fipronil of a triclinic-system crystal transformation V is obtained by crystallizing a solid-form fipronil of formula (I) with dimethylsulfoxide at 100-150°C or acetonitrile at 60-81°C as solvent. A combination of the fipronil with an other insecticidal or parasiticidal compound provides an insecticidal or a parasiticidal composition having a synergistic effect against a specified target of an insect, an acarid or a parasite. The fipronil can be used as a mixture with a fungicidal compound.
Abstract translation: 要解决的问题：提供新型晶体转化的氟虫腈和杀虫剂和杀寄生虫剂组合物。解决方案：通过用二甲基亚砜结晶式（I）的固体形式的氟虫腈获得三斜晶系的晶体转变V的氟虫腈 100-150℃或乙腈在60-81℃作为溶剂。 氟虫腈与其他杀虫剂或杀寄生虫化合物的组合提供对昆虫，螨虫或寄生虫的特定靶标具有协同效应的杀虫剂或杀寄生虫剂组合物。 氟虫腈可以与杀真菌化合物混合使用。
-
公开(公告)号：BRPI0718222A2
公开(公告)日：2018-09-04
申请号：BRPI0718222
申请日：2007-11-02
Applicant: BASF SE
Inventor： JAN KLAAS LOHMANN , JOACHIM RHEINHEIMER , JOCHEN DIETZ , MARTIN SUKOPP , MICHAEL KEIL , MICHAEL RACK , SANDRA LÖHR , SEBASTIAN PEER SMIDT , THOMAS GROTE , THOMAS ZIERKE
IPC: C07D237/04 , C07F7/04
-
公开(公告)号：BR122019011580B1
公开(公告)日：2020-10-13
申请号：BR122019011580
申请日：2007-11-05
Applicant: BASF SE
Inventor： ANTTI OJALA , CLAUDE TARANTA , GAUTAM R DESIRAJU , GERHARD COX , HEIDI EMILIA SAXELL , MARTIN SUKOPP , PETER ERK , PRASHANT M BHATT , RAHUL BANERJEE , STEFAN SCHERER , THOMAS KRÖHL
Abstract: a presente invenção diz respeito a uma modificação cristalina inédita de fipronil, a um processo para a preparação do mesmo, a misturas e composições pesticidas e parasiticidas compreendendo a dita modificação cristalina e a seu uso para combater pragas e parasitas.
-
-
-
Search Results
4
records
(took 0.024 seconds)
