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    A PROCESS FOR THE PREPARATION OF BRONOPOL
    1.
    发明申请
    A PROCESS FOR THE PREPARATION OF BRONOPOL 审中-公开
    制备BRONOPOL的方法

    公开(公告)号：WO2009107133A1

    公开(公告)日：2009-09-03

    申请号：PCT/IL2009/000218

    申请日：2009-02-26

    Applicant: BROMINE COMPOUNDS LTD. ,  OREN, Jacob

    Inventor： OREN, Jacob

    IPC: C07C201/12 ,  C07C205/15

    CPC classification number: C07C201/10 ,  C07C201/12 ,  C07C205/15

    Abstract: The invention provides a process for preparing bronopol, which process comprises charging a reaction vessel with water, bromopicrin, nitromethane and paraformaldehyde, gradually feeding a base into said reaction vessel under stirring, bringing the reaction to completion and separating bronopol from the aqueous reaction mixture.

    Abstract translation: 本发明提供了一种制备青霉酚的方法，该方法包括向反应容器中加入水，溴氰菊酯，硝基甲烷和多聚甲醛，在搅拌下逐渐向碱性物质中加入碱，使反应完成，并从反应混合物中分离出丙三醇。

    PROCESS FOR THE PREPARATION OF 1.1-CYCLOHEXANE DIACETIC ACID MONOAMIDE
    2.
    发明申请
    PROCESS FOR THE PREPARATION OF 1.1-CYCLOHEXANE DIACETIC ACID MONOAMIDE 审中-公开
    制备1.1环己基二酸单丁酰胺的方法

    公开(公告)号：WO2003002517A1

    公开(公告)日：2003-01-09

    申请号：PCT/IL2002/000473

    申请日：2002-06-17

    Applicant: BROMINE COMPOUNDS LTD. ,  OREN, Jacob

    Inventor： OREN, Jacob

    IPC: C07C231/02

    CPC classification number: C07C233/08 ,  C07C231/02 ,  C07C2601/14

    Abstract: Process for the preparation of 1,1-cyclohexane-diacetic acid monoamide (CHDAAM), by amination of 1,1-Cyclohexane-diacetic anhydride (CDAAn) with aqueous ammonia, neutralization of the reaction mixture, such that crude CHDAAM is precipitated and filtered and by purification of the crude CHDAAM by crystallization from a solvent. The amination is carried out at a temperature kept below 20oC and with aqueous ammonia having a concentration from 25 to 35 wt%, in a molar ratio relative to the CHDAAn from 5 to 10. The neutralization is carried out with an aqueous solution of H2SO4 having a concentration from 30 to 70 wt% and is continued until a slightly acid solution is obtained.

    Abstract translation: 通过用氨水将1,1-环己烷 - 二乙酸酐（CDAAn）胺化，反应混合物中和，制备1,1-环己烷 - 二乙酸单酰胺（CHDAAM）的方法，使粗CHDAAM沉淀并过滤 并通过从溶剂中结晶来纯化粗CHDAAM。 胺化在保持在20℃以下的温度下进行，氨水的浓度为25〜35重量％，相对于CHDAAn为5〜10的摩尔比。中和是用H 2 SO 4水溶液进行的， 浓度为30〜70重量％，并持续直至获得轻微的酸溶液。

    PROCESS FOR THE PREPARATION OF 5-BROMOPHTHALIDE
    3.
    发明申请
    PROCESS FOR THE PREPARATION OF 5-BROMOPHTHALIDE 审中-公开
    制备5-BRMOPHTHALIDE的方法

    公开(公告)号：WO2004089924A1

    公开(公告)日：2004-10-21

    申请号：PCT/IB2003/001450

    申请日：2003-04-11

    Applicant: BROMINE COMPOUNDS LTD. ,  OREN, Jacob

    Inventor： OREN, Jacob

    IPC: C07D307/88

    CPC classification number: C07D307/88 ,  C07D307/87

    Abstract: A process, which comprises reducing 4-bromophthalic anhydride in an organic solvent, to obtain a mixture of 5-bromophthalide and 6-bromophthalide, acidifying the reaction mixture, separating the same into aqueous and organic phases, and selectively crystallizing 5-bromophthalide from the organic phase.

    Abstract translation: 一种方法，其包括在有机溶剂中还原4-溴邻苯二甲酸酐，得到5-溴苯酞和6-溴苯酞的混合物，酸化反应混合物，将其分离成水相和有机相，并从 有机相。

    PROCESS FOR THE PREPARATION OF THE MONOMER PENTABROMOBENZYL ACRYLATE AND POLYMERIZATION THEREOF
    4.
    发明申请
    PROCESS FOR THE PREPARATION OF THE MONOMER PENTABROMOBENZYL ACRYLATE AND POLYMERIZATION THEREOF 审中-公开
    单体戊烯酰基丙烯酸酯的制备方法及其聚合方法

    公开(公告)号：WO2012140649A1

    公开(公告)日：2012-10-18

    申请号：PCT/IL2012/000154

    申请日：2012-04-05

    Applicant: BROMINE COMPOUNDS LTD. ,  OREN, Jacob

    Inventor： OREN, Jacob

    IPC: C08F120/22 ,  C07C69/54

    CPC classification number: C07C67/10 ,  C07C67/14 ,  C08F22/10 ,  C08F120/22 ,  C08F220/22 ,  C08F220/68 ,  C07C69/653

    Abstract: The invention relates to a process for preparing pentabromobenzyl acrylate through the reaction of pentahalobenzyl halide with a salt of acrylic acid in water-immiscible solvent, wherein said salt is in aqueous form and the reaction is carried out in the presence of a phase transfer catalyst. A process for polymerizing the pentabromobenzyl acrylate in halogenated aromatic solvent and the poly (pentabromobenzyl acrylate) obtained are also disclosed.

    Abstract translation: 本发明涉及一种通过五卤代苄基卤化物与丙烯酸盐在水不混溶溶剂中的反应制备丙烯酸五溴苄酯的方法，其中所述盐为水溶液形式，反应在相转移催化剂存在下进行。 还公开了在卤代芳族溶剂中聚合丙烯酸五溴苄酯和获得的聚（五溴苄基丙烯酸酯）的方法。

    PROCESS FOR THE PREPARATION OF 1.1-CYCLOHEXANEDIACETIC ACID
    5.
    发明申请
    PROCESS FOR THE PREPARATION OF 1.1-CYCLOHEXANEDIACETIC ACID 审中-公开
    制备1.1环己基酸的方法

    公开(公告)号：WO2003002504A1

    公开(公告)日：2003-01-09

    申请号：PCT/IL2002/000474

    申请日：2002-06-17

    Applicant: BROMINE COMPOUNDS LTD. ,  OREN, Jacob

    Inventor： OREN, Jacob

    IPC: C07C55/28

    CPC classification number: C07C51/08 ,  C07C51/48 ,  C07C55/28

    Abstract: Process for the preparation of 1,1-cyclohexane-diacetic acid (CHDAA) from 1,5-dicarbonitrile-2,4-dioxo-3-azaspiro[5,5]undecane (the imide), by reacting it with sulfuric acid in two steps. The first step at a temperature lower than 100°C and the second step at a reaction temperature from 160 to 190°C. The first step is carried out by dissolving the imide in aqueous sulfuric acid at temperatures from about 65°to about 85°C and then cooling the solution thus obtained to room temperature. The second step is carried out by reacting said solution with aqueous sulfuric acid at temperatures of about 170°C.

    Abstract translation: 由1,5-二腈-2,4-二氧代-3-氮杂螺[5,5]十一烷（酰亚胺）制备1,1-环己烷二乙酸（CHDAA）的方法，通过与硫酸反应 两步。 在低于100℃的温度下进行第一步，第二步是在160〜190℃的反应温度下进行。第一步是将酰亚胺溶解在硫酸水溶液中，温度约为65-85℃ 然后将由此获得的溶液冷却至室温。 第二步是通过使所述溶液与硫酸水溶液在约170℃的温度下反应来进行。

    A PROCESS FOR THE PREPARATION OF BRONOPOL
    6.
    发明公开
    A PROCESS FOR THE PREPARATION OF BRONOPOL 有权
    用于生产溴硝丙二醇

    公开(公告)号：EP2247568A1

    公开(公告)日：2010-11-10

    申请号：EP09716009.7

    申请日：2009-02-26

    Applicant: Bromine Compounds Ltd.

    Inventor： OREN, Jacob

    IPC: C07C201/12 ,  C07C205/15

    CPC classification number: C07C201/10 ,  C07C201/12 ,  C07C205/15

    Abstract: The invention provides a process for preparing bronopol, which process comprises charging a reaction vessel with water, bromopicrin, nitromethane and paraformaldehyde, gradually feeding a base into said reaction vessel under stirring, bringing the reaction to completion and separating bronopol from the aqueous reaction mixture.

    A PROCESS FOR THE PREPARATION OF BRONOPOL
    7.
    发明授权
    A PROCESS FOR THE PREPARATION OF BRONOPOL 有权
    用于生产溴硝丙二醇

    公开(公告)号：EP2247568B1

    公开(公告)日：2012-04-25

    申请号：EP09716009.7

    申请日：2009-02-26

    Applicant: Bromine Compounds Ltd.

    Inventor： OREN, Jacob

    IPC: C07C201/12 ,  C07C205/15

    CPC classification number: C07C201/10 ,  C07C201/12 ,  C07C205/15

    Abstract: The invention provides a process for preparing bronopol, which process comprises charging a reaction vessel with water, bromopicrin, nitromethane and paraformaldehyde, gradually feeding a base into said reaction vessel under stirring, bringing the reaction to completion and separating bronopol from the aqueous reaction mixture.

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