公开(公告)号：JP2012197223A

公开(公告)日：2012-10-18

申请号：JP2012115331

申请日：2012-05-21

Applicant: Corning Inc ,  コーニング インコーポレイテッド

Inventor： CORTRIGHT JEFFREY E ,  LAMBERSON LISA A ,  MAUREY PAMELA A ,  MORENA ROBERT M

IPC: C03C8/24 ,  C03C8/02 ,  H01M8/02 ,  H01M8/12 ,  H01M8/24

CPC classification number: C03C3/064 ,  C03C3/091 ,  C03C8/14 ,  C03C8/20

Abstract: PROBLEM TO BE SOLVED: To provide a sealing material resistant to hydrogen gas permeation at a sealing temperature in the intermediate temperature range of 600-900°C.SOLUTION: The sealing material comprises a glass frit in mol% of: 20-30% of Si; 0-15% of SrO; 0-8% of KO; 0-6% of MgO; 20-30% of CaO; 0-10% of AlO; 35-45% of BO; wherein the total amount of alkali is less than 10 mol%.

Abstract translation: 要解决的问题：提供在600-900℃的中间温度范围内的密封温度下耐氢气渗透的密封材料。 解决方案：密封材料包括摩尔％的玻璃料：20-30％的Si 2 ; 0-15％的SrO; 0-8％K 2 O; 0-6％的MgO; 20-30％的CaO; 0 3 的0-10％; 3 的35-45％B 2 O 3 其中碱的总量小于10摩尔％。 版权所有（C）2013，JPO＆INPIT

公开(公告)号：JP2013227217A

公开(公告)日：2013-11-07

申请号：JP2013111531

申请日：2013-05-28

Applicant: Corning Inc ,  コーニング インコーポレイテッド

Inventor： LAMBERSON LISA A ,  MORENA ROBERT M

IPC: C03C8/24 ,  C03C3/21 ,  C03C27/10 ,  G02B1/00

CPC classification number: C03C8/08 ,  C03C3/21 ,  C03C8/16 ,  C03C8/20 ,  C03C8/24 ,  C03C27/06 ,  H01L51/5246

Abstract: PROBLEM TO BE SOLVED: To provide a method for manufacturing a hermetically sealed glass package using a frit that is antimony-free glass.SOLUTION: A hermetically sealed glass package, such as an OLED display device 10, is manufactured by providing a first glass substrate plate 12 and a second glass substrate plate 18 and depositing an antimony-free frit 16 onto the first substrate plate 12. OLEDs 14 may be deposited on the second glass substrate plate 18. An irradiation source 22 (e.g., laser, infrared light) is then used to heat the frit 16 which melts and forms a hermetic seal 20 that connects the first glass substrate plate 12 to the second glass substrate plate 18 and also protects the OLEDs 14. The antimony-free glass has excellent water resistance, good flow, low glass transition temperature and low coefficient of thermal expansion.

Abstract translation: 要解决的问题：提供使用无锑玻璃的玻璃料制造密封玻璃封装的方法。解决方案：通过提供第一玻璃基板来制造气密密封的玻璃封装，例如OLED显示装置10 板12和第二玻璃衬底板18，并将无锑玻璃料16沉积到第一衬底板12上。可以将OLED 14沉积在第二玻璃衬底板18上。照射源22（例如，激光，红外光）是 然后用于加热熔化的玻璃料16，并形成将第一玻璃基板12连接到第二玻璃基板18并且还保护OLED 14的气密密封20.无锑玻璃具有优异的耐水性，良好的流动性， 玻璃化转变温度低，热膨胀系数低。

公开(公告)号：CA2595945A1

公开(公告)日：2006-08-10

申请号：CA2595945

申请日：2006-01-30

Applicant: CORNING INC

Inventor： MORENA ROBERT M ,  MAUREY PAMELA A ,  CORTRIGHT JEFFREY E ,  LAMBERSON LISA A

IPC: H01M2/08 ,  C03C8/02 ,  C03C8/14 ,  C03C8/20 ,  C03C8/24

Abstract: A solid oxide fuel cell device incorporates a sealing material resistant to hydrogen gas permeation at a sealing temperature in the intermediate temperature range of 600° C.-900° C., the seal having a CTE in the 100x10 -7 /° C. to 120x10 -7 /° C., wherein the sealing material comprises in weight %, of: (i) a 80 wt % to 100 wt % glass frit, the glass frit itself having a composition comprising in mole percent of: SiO 2 15-65; Li 2 O 0-5; Na 2 O 0-5; K 2 O 0-10; MgO 0-5; CaO 0-32; Al 2 O 3 0-10; B 2 O 3 0-50; SrO 0 to 25, wherein the total amount of alkalis is less than 10 mole %; and (ii) zirconia or leucite addition 0 wt % to 30 wt.

公开(公告)号：BRPI0606885A2

公开(公告)日：2009-07-21

申请号：BRPI0606885

申请日：2006-01-30

Applicant: CORNING INC

Inventor： CORTRIGHT JEFFREY E ,  LAMBERSON LISA A ,  MAUREY PAMELA A ,  MORENA ROBERT M

IPC: H01M2/08 ,  C03C8/02 ,  C03C8/14 ,  C03C8/20 ,  C03C8/24

Abstract: A solid oxide fuel cell device incorporates a sealing material resistant to hydrogen gas permeation at a sealing temperature in the intermediate temperature range of 600° C.-900° C., the seal having a CTE in the 100x10 -7 /° C. to 120x10 -7 /° C., wherein the sealing material comprises in weight %, of: (i) a 80 wt % to 100 wt % glass frit, the glass frit itself having a composition comprising in mole percent of: SiO 2 15-65; Li 2 O 0-5; Na 2 O 0-5; K 2 O 0-10; MgO 0-5; CaO 0-32; Al 2 O 3 0-10; B 2 O 3 0-50; SrO 0 to 25, wherein the total amount of alkalis is less than 10 mole %; and (ii) zirconia or leucite addition 0 wt % to 30 wt.

公开(公告)号：AU2006210980A1

公开(公告)日：2006-08-10

申请号：AU2006210980

申请日：2006-01-30

Applicant: CORNING INC

Inventor： LAMBERSON LISA A ,  MORENA ROBERT M ,  MAUREY PAMELA A ,  CORTRIGHT JEFFREY E

IPC: H01M2/08 ,  C03C8/02 ,  C03C8/14 ,  C03C8/20 ,  C03C8/24

Abstract: A solid oxide fuel cell device incorporates a sealing material resistant to hydrogen gas permeation at a sealing temperature in the intermediate temperature range of 600° C.-900° C., the seal having a CTE in the 100x10 -7 /° C. to 120x10 -7 /° C., wherein the sealing material comprises in weight %, of: (i) a 80 wt % to 100 wt % glass frit, the glass frit itself having a composition comprising in mole percent of: SiO 2 15-65; Li 2 O 0-5; Na 2 O 0-5; K 2 O 0-10; MgO 0-5; CaO 0-32; Al 2 O 3 0-10; B 2 O 3 0-50; SrO 0 to 25, wherein the total amount of alkalis is less than 10 mole %; and (ii) zirconia or leucite addition 0 wt % to 30 wt.

公开(公告)号：WO2007067402A2

公开(公告)日：2007-06-14

申请号：PCT/US2006045744

申请日：2006-11-28

Applicant: CORNING INC ,  LAMBERSON LISA A ,  MORENA ROBERT M

Inventor： LAMBERSON LISA A ,  MORENA ROBERT M

IPC: C03B23/20

CPC classification number: C03C8/24 ,  C03C1/026 ,  C03C3/21 ,  H01L51/5246

Abstract: A hermetically sealed glass package preform is provided comprising a glass substrate; a frit comprising 65 - 100 wt.% of a base glass and about 0 - 35 wt.% of a filler; wherein the base glass comprises: about 0 - 5 mole % K 2 O; about 0 - 35 mole % Sb 2 O 3 ; about 0 - 20 mole % ZnO; about 10 - 40 mole % P 2 O 5 ; about 10 - 60 mole % V 2 O 5 ; about 0 - 5 mole % TiO 2 ; about 0 - 5 mole % B 2 O 3 ; about 0 - 5 mole % SiO 2 ; about 0 - 5 mole% WO 3 ; and about 1- 10 mole % of a metal oxide selected from the group consisting of Fe 2 O 3 , Nd 2 O 3 , La 2 O 3 , Ce 2 O 4 , Pr 6 O 11 , Er 2 O 3 , and CeO 2 ; wherein the base glass has a mean particle size distribution of less than about 3 µm; and wherein the filler has a mean particle size distribution of between about 3 and 7 µm. The frit is sintered in an atmosphere less oxidizing than air at a temperature of between about 39O °C to 415 °C.

Abstract translation: 提供了一种密封玻璃包装预制件，其包括玻璃基板; 玻璃料，其包含65-100重量％的基础玻璃和约0-35重量％的填料; 其中所述基础玻璃包括：约0-5摩尔％的K 2 O; 约0-35摩尔％Sb 2 O 3 3; 约0-20摩尔％ZnO; 约10-40摩尔％P 2 O 5 O 5; 约10-60摩尔％V 2 O 5; 约0-5摩尔％TiO 2; 约0-5摩尔％B 2 O 3 3; 约0-5摩尔％SiO 2; 约0-5摩尔％WO 3; 和约1-10摩尔％的选自Fe 2 O 3 O 3，N 2 O 3 O 3的金属氧化物 La 2 O 3，Ce 2 O 4，Pr 6，N 2， Er;;; Er Er Er Er Er Er Er Er Er Er Er Er Er Er Er Er Er;;;;;;;;;;;;;;;;;;;;;;;;;;;; 其中所述基础玻璃的平均粒度分布小于约3μm; 并且其中所述填料的平均粒度分布在约3和7μm之间。 玻璃料在约39℃至415℃之间的温度下在比空气氧化较少的气氛中烧结。

公开(公告)号：WO2006078747A2

公开(公告)日：2006-07-27

申请号：PCT/US2006001781

申请日：2006-01-13

Applicant: CORNING INC ,  CORTRIGHT JEFFREY E ,  MORENA ROBERT M ,  LAMBERSON LISA A ,  MAUREY PAMELA A

Inventor： CORTRIGHT JEFFREY E ,  MORENA ROBERT M ,  LAMBERSON LISA A ,  MAUREY PAMELA A

IPC: C03C8/24 ,  C03C14/00

CPC classification number: C03C8/02 ,  C03C8/24 ,  H01M8/0282 ,  H01M2008/1293

Abstract: A solid oxide fuel cell device incorporates a sealing material resistant to hydrogen gas permeation at a sealing temperature in the intermediate temperature range of 600°C -800°C, the seal having a CTE in the 100x10 -7 /°C to 120x10 -7 /°C , wherein the sealing material comprises in weight %, of: (i) a 80 to 95 wt % of glass frit, the glass frit itself having a composition in mole percent of : SiO 2 70-85%; Al 2 O 3 0-5%; Na 2 O 3 0-8%; K 2 O 10-25%; ZnO 0-10%; ZrO 2 0-6%; MgO 0-7%; TiO 2 0-2%; and (ii) and 5wt % to 25wt% of addition comprising at least one of: alumina, zirconia or leucite.

Abstract translation: 固体氧化物燃料电池装置在600℃-800℃的中间温度范围内的密封温度下结合有耐氢气渗透的密封材料，该密封件具有100×10 -7 /℃的CTE， /℃至120×10 -7 /℃，其中所述密封材料以重量百分比计包含：（i）80至95重量％的玻璃料，所述玻璃料本身具有 摩尔百分比：SiO 2 2 70-85％; 人 _{2 0 3 0-5％; Na 2 3 0-8％; K <2> O 10-25％; ZnO 0-10％; ZrO <2> 0-6％; MgO 0-7％; TiO 2 0-2％; 和（ii）以及5重量％至25重量％的包含氧化铝，氧化锆或白榴石中的至少一种的添加剂。}

公开(公告)号：WO2010048044A3

公开(公告)日：2010-07-22

申请号：PCT/US2009060962

申请日：2009-10-16

Applicant: CORNING INC ,  LAMBERSON LISA A ,  MORENA ROBERT M

Inventor： LAMBERSON LISA A ,  MORENA ROBERT M

IPC: C03C3/16

CPC classification number: C03C8/08 ,  C03C3/21 ,  C03C8/16 ,  C03C8/20 ,  C03C8/24 ,  C03C27/06 ,  H01L51/5246

Abstract: An antimony-free glass suitable for use in a frit for producing a hermetically sealed glass package is described. The hermetically sealed glass package, such as an OLED display device, is manufactured by providing a first glass substrate plate and a second glass substrate plate and depositing the antimony-free frit onto the first substrate plate. OLEDs may be deposited on the second glass substrate plate. An irradiation source (e.g., laser, infrared light) is then used to heat the frit which melts and forms a hermetic seal that connects the first glass substrate plate to the second glass substrate plate and also protects the OLEDs. The antimony-free glass has excellent aqueous durability, good flow, low glass transition temperature and low coefficient of thermal expansion.

Abstract translation: 描述适用于玻璃料生产密封玻璃包装的无锑玻璃。 通过提供第一玻璃基板和第二玻璃基板并将无锑玻璃料沉积到第一基板上来制造密封玻璃封装，例如OLED显示装置。 OLED可以沉积在第二玻璃基板上。 然后使用照射源（例如，激光，红外光）来加热熔融物并且形成将第一玻璃衬底板连接到第二玻璃衬底板并且还保护OLED的气密密封件。 无锑玻璃具有优异的水性耐久性，良好的流动性，低的玻璃化转变温度和低的热膨胀系数。

公开(公告)号：WO2008127565A3

公开(公告)日：2009-03-12

申请号：PCT/US2008004341

申请日：2008-04-03

Applicant: CORNING INC ,  LAMBERSON LISA A ,  MORENA ROBERT M ,  SANFORD EARL J ,  THIBAULT YVES ,  WHEATON BRYAN R

Inventor： LAMBERSON LISA A ,  MORENA ROBERT M ,  SANFORD EARL J ,  THIBAULT YVES ,  WHEATON BRYAN R

IPC: H01M8/12 ,  C03B27/012 ,  C03C3/064 ,  C03C8/24 ,  C03C10/00 ,  C03C14/00 ,  C03C29/00 ,  C04B35/195 ,  F16J15/12 ,  H01M8/02

CPC classification number: H04N5/44543 ,  C03C3/064 ,  C03C8/24 ,  C03C10/0036 ,  C04B37/025 ,  C04B2237/10 ,  C04B2237/348 ,  C04B2237/406 ,  H01M8/0282 ,  H01M8/0286 ,  H01M2008/1293 ,  H04N21/4312 ,  H04N21/4314 ,  H04N21/4821 ,  Y02P70/56

Abstract: According to one embodiment a solid oxide fuel cell device incorporates a seal resistant to hydrogen gas permeation at a in the range of 600°C to 9000C, the seal having a CTE in the 100xl0-7/°C to 120xl0-7/°C, wherein the seal includes a sealing material that comprises in weight %, of: (i) 80 to 100 wt % of glass frit, wherein the glass frit includes in mole% MgO, 0-10% CaO, 0-30% BaO, 30-50% B2O3, 0-40% Al2O3, 10-30% SiO2, 10-30%; and (ii) a filler, 0 wt % to 20 wt%.

Abstract translation: 根据一个实施方案，固体氧化物燃料电池装置包含在600℃至9000℃的范围内耐氢气渗透的密封件，密封件具有100×10 -7 /℃至120×10 -7 /℃的CTE ，其中所述密封件包括重量％的密封材料，所述密封材料包含：（i）80至100重量％的玻璃料，其中所述玻璃料包含摩尔％的MgO，0-10％的CaO，0-30％的BaO， 30-50％B2O3，0-40％Al2O3，10-30％SiO2，10-30％; 和（ii）0重量％至20重量％的填料。

公开(公告)号：WO2008039284A2

公开(公告)日：2008-04-03

申请号：PCT/US2007018872

申请日：2007-08-28

Applicant: CORNING INC ,  DEETER LEE E ,  JOHNSON L URDENIS ,  LAMBERSON LISA A ,  MCINTOSH JOSEPH J ,  MEROLA DIANA M ,  MORENA ROBERT M ,  RUMSEY DENNIS F

Inventor： DEETER LEE E ,  JOHNSON L URDENIS ,  LAMBERSON LISA A ,  MCINTOSH JOSEPH J ,  MEROLA DIANA M ,  MORENA ROBERT M ,  RUMSEY DENNIS F

CPC classification number: C03C8/14 ,  B41J3/4073 ,  B41M5/0047 ,  B41M5/007 ,  C04B41/009 ,  C04B41/4572 ,  C04B41/81 ,  C04B2111/00793 ,  C04B2111/0081 ,  F01N3/0222 ,  F01N2260/24 ,  C04B41/4539 ,  C04B41/4578 ,  C04B41/5022 ,  C04B2103/54 ,  C04B35/00 ,  C04B35/195 ,  C04B38/0006

Abstract: A system, method, and ink for printing a data carrying mark on a green ceramic honeycomb structure is provided. The system includes a printer having an ink jet print head that prints a mark, preferably in the form of a two-dimensional data matrix barcode, on a side wall of the green ceramic honeycomb structure. The ink may be a heat resistant ink that comprises a mixture of a glass or glass ceramic frit and a metal oxide colorant. An optical reader is provided for determining if the data is accurately reproduced in the printed mark, as well as any noise factor which may be present due to defective printing. The system includes a turntable that positions the green body for the printing operation, and then rotates the green body to position the printed mark first in front of a dryer, and then in front of the optical reader to determine the quality of the mark. Marked green and ceramic honeycombs are also provided as well as a method for repairing a defective applied bar code on a honeycomb structure.

Abstract translation: 提供了一种用于在绿色陶瓷蜂窝结构上印刷数据携带标记的系统，方法和墨水。 该系统包括具有喷墨打印头的打印机，该喷墨打印头在绿色陶瓷蜂窝结构体的侧壁上以二维数据矩阵条形式打印标记，优选为二维数据矩阵条形码。 油墨可以是包含玻璃或玻璃陶瓷玻璃料和金属氧化物着色剂的混合物的耐热油墨。 提供了一种用于确定数据是否在印刷标记中被准确地再现的光学读取器以及由于打印不良而可能存在的任何噪声因素。 该系统包括一个转盘，用于将生坯定位用于打印操作，然后旋转生坯以将打印标记置于干燥器前面，然后在光学读取器前面以确定标记的质量。 还提供了标记的绿色和陶瓷蜂窝以及用于修复蜂窝状结构上的有缺陷的条形码的方法。