1.
    发明专利
    未知

    公开(公告)号:DE1792567A1

    公开(公告)日:1971-11-25

    申请号:DE1792567

    申请日:1968-09-20

    Applicant: DEGUSSA

    Abstract: 1277592 Germanium dioxide DEUTSCHE GOLDUND SILBER-SCHEIDEANSTALT 4 Sept 1969 [20 Sept 1968] 43879/69 Heading C1A Amorphous highly dispersed germanium dioxide is prepared by reacting a volatile tetravalent germanium compound or a sprayable solution thereof under hydrolysing or oxidizing conditions in the gas phase or as an aerosol at a temperature above 1300‹ C., allowing the germanium dioxide formed to coagulate at a temperature of from 200‹ to 1000‹ C., and separating the gaseous reaction products. The germanium compound is preferably a halide or a volatile organo-germanium compound. The reaction is preferably carried out at a temperature of from 1400‹ to 1700‹ C. using a fuel gas of high calorific value with a free oxygen containing gas or pure oxygen, the mixture being reacted after passage through a nozzle. The germanium dioxide formed is preferably coagulated and separated at a temperature of from 400‹ to 700‹ C.

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