公开(公告)号：JP2007051057A

公开(公告)日：2007-03-01

申请号：JP2006218474

申请日：2006-08-10

Applicant: Degussa Ag ,  デグサ アクチエンゲゼルシャフトDegussa AG

Inventor： KATUSIC STIPAN ,  KROELL MICHAEL ,  KRAEMER MICHAEL ,  HEBERER STEFAN ,  STAAB EDWIN ,  MICHAEL GUENTHER

IPC: C01F17/00 ,  C09K3/14

CPC classification number: C09K3/1463 ,  B82Y30/00 ,  C01F17/0043 ,  C01F17/005 ,  C01P2004/64 ,  C01P2004/86 ,  C01P2006/12 ,  C09K3/1409

Abstract: PROBLEM TO BE SOLVED: To provide a cerium oxide powder, a method for producing the same, and a dispersion liquid containing the powder.
SOLUTION: The cerium oxide powder has a BET surface area of 25-150 m
2 /g and contains primary particles having an average diameter of 5-50 nm. The layer close to the surface of each primary particle has a depth of about 5 nm, and the carbonate concentration in the layer close to the surface is decreased toward inside from the surface. The content of carbon deriving from carbonate groups is 5-50% by area percentage on the surface and 0-30% by area percentage at a depth of about 5 nm in the layer close to the surface. The content of cerium oxide is at least 99.5 mass% based on powder. Further, the content of carbon is 0.01-0.3 mass% based on powder. The dispersion liquid is sufficiently stable even when an additive is not added additionally and can be used for chemical and mechanical polishing within a range from neutrality to weak alkalinity.
COPYRIGHT: (C)2007,JPO&INPIT

Abstract translation: 待解决的问题：提供氧化铈粉末，其制备方法和含有该粉末的分散液。 解决方案：氧化铈粉末的BET表面积为25-150m 2 / SP / g，并且含有平均直径为5-50nm的一次粒子。 靠近每个初级颗粒表面的层具有约5nm的深度，并且靠近表面的层中的碳酸盐浓度从表面向内减小。 来自碳酸酯基团的碳的含量在表面附近的层中为面积百分比为5-50％，在约5nm的深度为0-30％的面积百分比。 氧化铈的含量相对于粉末为99.5质量％以上。 此外，基于粉末，碳的含量为0.01-0.3质量％。 即使不添加添加剂也能够分散液充分稳定，可以在中性至弱碱性的范围内用于化学和机械抛光。 版权所有（C）2007，JPO＆INPIT

公开(公告)号：JP2006213591A

公开(公告)日：2006-08-17

申请号：JP2005345055

申请日：2005-11-30

Applicant: Degussa Ag ,  デグサ アクチエンゲゼルシャフトDegussa AG

Inventor： KATUSIC STIPAN ,  KRAEMER MICHAEL ,  KROELL MICHAEL ,  KRESS PETER ,  STAAB EDWIN

IPC: C01B13/34 ,  B01J2/04 ,  C01F17/00 ,  C01G27/00 ,  C01G99/00

CPC classification number: B01J23/10 ,  B01J37/082 ,  B82Y30/00 ,  C01B13/20 ,  C01B13/34 ,  C01F17/0043 ,  C01G1/02 ,  C01G25/00 ,  C01G25/02 ,  C01P2004/50 ,  C01P2004/52 ,  C01P2004/64 ,  C01P2006/12 ,  C01P2006/80 ,  C01P2006/90 ,  C09G1/02 ,  Y10T428/2982

Abstract: PROBLEM TO BE SOLVED: To provide a method of making metal oxide powder by which uniform powders having high BET surface area and narrow particle size distribution can be obtained and suitable for making the metal oxide powder in a range of quantity of kg/hr order. SOLUTION: In the method of making the metal oxide powder having at least 20 m 2 /g BET surface area by reacting aerosol with oxygen in a reaction space at a reaction temperature higher than 700°C and successively separating the resultant powder from a gaseous material, the aerosol is produced by spraying at least one kind of a starting material in a liquid form or a solution and at least one kind of a spray gas using a multi-component nozzle so that the average liquid particle diameter D 30 of the aerosol to the volume is 30-100 μm and the number of aerosol small droplets having a particle diameter larger than 100 μm is ≤10% of the total number of droplets. COPYRIGHT: (C)2006,JPO&NCIPI

Abstract translation: 要解决的问题：提供一种制备金属氧化物粉末的方法，通过该方法可以获得具有高BET表面积和窄粒度分布的均匀粉末，并且适于使金属氧化物粉末的量为kg / 小时订单。 解决方案：在反应温度高于700℃的反应空间中通过气溶胶与氧气反应制备具有至少20m 2 / SP / g BET表面积的金属氧化物粉末的方法中， 并将所得粉末从气态物质中分离出来，通过使用多组分喷嘴将至少一种起始材料以液体形式或溶液喷射至少一种喷雾气体喷射而制成气雾剂， 气溶胶的体积的平均液体粒径D 30 为30-100μm，粒径大于100μm的气溶胶小液滴的数量为液滴总数的10％。 版权所有（C）2006，JPO＆NCIPI

公开(公告)号：JP2007161580A

公开(公告)日：2007-06-28

申请号：JP2006340375

申请日：2006-12-18

Applicant: Degussa Gmbh ,  デグサ ゲーエムベーハーDegussa GmbH

Inventor： ZIMMERMANN GUIDO ,  KATUSIC STIPAN ,  KRAEMER MICHAEL ,  MIESS HORST ,  NUH YILMAZ ,  MICHAEL GUENTHER

IPC: C01G9/03

CPC classification number: C01G9/03 ,  C01P2006/12 ,  C09C1/043

Abstract: PROBLEM TO BE SOLVED: To provide an improved method for producing a zinc oxide powder without generating a cake-like material in an evaporation zone and an oxidation zone.
SOLUTION: In the evaporation zone, a gas flow of an inert gas and a fuel gas is passed through a melt of zinc having a temperature of 780-850°C while forming zinc vapor. In this case, the content of the fuel gas is 1-50 vol.% based on the total volume of the inert gas and the fuel gas, and the molar ratio of the zinc vapor to the fuel gas is 0.01-50. In the oxidation zone, a second gas flow containing an oxygen-containing gas and steam is added to a gas flow of the zinc vapor, the fuel gas, and the inert gas in such an amount that the temperature in the oxidation zone is kept within a range of 500-1,000°C.
COPYRIGHT: (C)2007,JPO&INPIT

Abstract translation: 要解决的问题：提供一种在蒸发区和氧化区中不产生饼状材料的氧化锌粉末的制造方法。 解决方案：在蒸发区中，惰性气体和燃料气体的气流在形成锌蒸气的同时通过温度为780-850℃的锌熔体。 在这种情况下，基于惰性气体和燃料气体的总体积，燃料气体的含量为1-50体积％，锌蒸气与燃料气体的摩尔比为0.01-50。 在氧化区中，将含有含氧气体和蒸汽的第二气流加入到锌蒸汽，燃料气体和惰性气体的气流中，其量使得氧化区中的温度保持在 范围500-1,000℃。 版权所有（C）2007，JPO＆INPIT

公开(公告)号：JP2009184923A

公开(公告)日：2009-08-20

申请号：JP2009129226

申请日：2009-05-28

Applicant: Evonik Degussa Gmbh ,  エボニック デグサ ゲーエムベーハーEvonik Degussa GmbH

Inventor： GUTSCH ANDREAS DR ,  HENNIG THOMAS DR ,  KATUSIC STIPAN ,  KRAEMER MICHAEL ,  MICHAEL GUENTHER ,  VARGA GOEFFREY J

IPC: A61K8/19 ,  C01F7/02 ,  A61K8/26 ,  A61K8/29 ,  C01B13/18 ,  C01B13/34 ,  C01F7/30 ,  C01G1/02 ,  C01G23/047 ,  C01G23/07 ,  C01G25/02 ,  C09K3/00 ,  C09K3/14

CPC classification number: B82Y30/00 ,  C01B13/34 ,  C01F7/304 ,  C01G23/07 ,  C01G25/02 ,  C01P2002/02 ,  C01P2002/30 ,  C01P2004/32 ,  C01P2004/61 ,  C01P2004/62 ,  C01P2004/64 ,  C01P2006/12 ,  C01P2006/80

Abstract: PROBLEM TO BE SOLVED: To provide a method of manufacturing an approximately nano-degree thermal decomposition method oxide having a minimal chloride content and a BET surface area of 1-600 m
2 /g without necessitating an extremely high vaporization temperature.
SOLUTION: This oxide is obtained by dissolving an organic metal material in a solvent and converting it into an oxide in a flame at a temperature over 200°C.
COPYRIGHT: (C)2009,JPO&INPIT

Abstract translation: 要解决的问题：提供一种制造具有最小氯化物含量和1-600m 2 / SP / g的BET表面积的近似纳米级热分解方法氧化物的方法，而不需要 极高的汽化温度。 解决方案：该氧化物通过将有机金属材料溶解在溶剂中并在200℃以上的温度下将其转化为火焰中的氧化物而获得。 版权所有（C）2009，JPO＆INPIT

公开(公告)号：JP2005060222A

公开(公告)日：2005-03-10

申请号：JP2004233631

申请日：2004-08-10

Applicant: Degussa Ag ,  デグサ アクチエンゲゼルシャフト

Inventor： KATUSIC STIPAN ,  HEBERER STEFAN ,  KRAEMER MICHAEL ,  KRESS PETER ,  KROELL MICHAEL ,  STAAB EDWIN

IPC: B01J23/10 ,  B01J35/02 ,  B01J35/10 ,  B01J37/00 ,  B01J37/02 ,  C01F17/00 ,  C09K3/14

CPC classification number: B82Y30/00 ,  B01J23/10 ,  B01J35/023 ,  B01J35/1014 ,  B01J35/1019 ,  B01J37/0238 ,  C01F17/0043 ,  C01P2002/60 ,  C01P2002/76 ,  C01P2004/04 ,  C01P2004/50 ,  C01P2004/64 ,  C01P2006/10 ,  C01P2006/11 ,  C01P2006/12 ,  C01P2006/14 ,  C01P2006/17 ,  C01P2006/80 ,  C09K3/1409 ,  C09K3/1463 ,  Y10S977/773 ,  Y10S977/775 ,  Y10S977/811

Abstract: PROBLEM TO BE SOLVED: To prepare a cerium oxide powder suitable as a component of a dispersion for grinding a semiconductor substrate, easily incorporated and having high stability to precipitation.
SOLUTION: The polycrystalline cerium oxide powder in a form of primary particle aggregate has 70-150 m
2 /g specific surface area, 5-20 nm average primary particle diameter and 20-100 nm projected average aggregate diameter.
COPYRIGHT: (C)2005,JPO&NCIPI

Abstract translation: 要解决的问题：为了制备适合作为用于研磨半导体衬底的分散体的组分的二氧化铈粉末，容易并入并具有高的沉淀稳定性。 解决方案：一次粒子聚集体形式的多晶氧化铈粉末具有比表面积70-150μm，平均一次粒径为5-20nm，投影时为20-100nm 平均骨料直径。 版权所有（C）2005，JPO＆NCIPI

公开(公告)号：JP2004315362A

公开(公告)日：2004-11-11

申请号：JP2004118825

申请日：2004-04-14

Applicant: Degussa Ag ,  デグサ アクチエンゲゼルシャフト

Inventor： GOTTFRIED HEIKO ,  KATUSIC STIPAN ,  KRAEMER MICHAEL ,  PRIDOEHL MARKUS ,  WOMBACHER WILLIBALD ,  ZIMMERMANN GUIDO

IPC: C01B13/24 ,  C01B13/34 ,  C01B33/18 ,  C01F7/30 ,  C01G1/02 ,  C01G19/00 ,  C01G23/07 ,  C01G25/02

CPC classification number: B82Y30/00 ,  C01G1/02 ,  C01G19/00 ,  C01P2002/72 ,  C01P2002/85 ,  C01P2004/64 ,  C01P2006/12 ,  Y10T428/12146 ,  Y10T428/298 ,  Y10T428/2982

Abstract: PROBLEM TO BE SOLVED: To provide composite powder having a matrix domain structure. SOLUTION: The composite powder has the matrix domain structure in which the matrix is a metal oxide and is present in the form of three dimensional aggregate having ≤250 nm diameter at least in one dimension and the domains consist of metal oxides and/or nobel metals in the matrix of individual metal oxide. In such a case, the domains consist of at least two metal oxides, at least two noble metals or a mixture of at least one metal oxide with at least one noble metal and are nano scale and the composite powder has 60-1,200 m 2 /cm 3 volume-specific surface area. The composite powder is produced by mixing the precursors of the matrix and of the domains corresponding to the subsequently desired ratio with a gaseous mixture containing a combustible gas and oxygen, reacting in the reactor consisting of a combustion zone and a reaction zone, cooling the hot gas and a solid product and separating from the gas. The composite powder is used as a material for magnetic, electronic or optical applications. COPYRIGHT: (C)2005,JPO&NCIPI

公开(公告)号：JP2001342011A

公开(公告)日：2001-12-11

申请号：JP2001103978

申请日：2001-04-02

Applicant: DEGUSSA

Inventor： GUTSCH ANDREAS DR ,  HENNIG THOMAS DR ,  KATUSIC STIPAN ,  KRAEMER MICHAEL ,  MICHAEL GUENTHER ,  VARGA GEOFFREY J

IPC: A61K8/19 ,  A61K8/26 ,  A61K8/29 ,  C01B13/18 ,  C01B13/34 ,  C01F7/30 ,  C01G1/02 ,  C01G23/047 ,  C01G23/07 ,  C01G25/02 ,  C09K3/00 ,  C09K3/14 ,  A61K7/00

Abstract: PROBLEM TO BE SOLVED: To provide nano size oxide with a slight amount of chloride and BET specific surface area of 1-600 m2/g through a thermo-decomposition method which does not need an extremely high evaporation temperature. SOLUTION: In manufacturing through a thermo-decomposition of metal and/or metalloid, oxide and/or mixed oxide in nano size is controlled to become 1-600 m2/g in BET specific surface area and less than 0.05 mass % in total chloride content.

公开(公告)号：JP2001327849A

公开(公告)日：2001-11-27

申请号：JP2001076687

申请日：2001-03-16

Applicant: DEGUSSA

Inventor： TASSILO MORITZ ,  REETZ TEJA ,  DELLER KLAUS ,  GUTSCH ANDREAS DR ,  KRAEMER MICHAEL ,  MICHAEL GUENTHER

IPC: B01J2/02 ,  B01J20/06 ,  B01J20/10 ,  C01B33/12 ,  C01G23/04 ,  C04B35/626 ,  C09B67/00 ,  C09B67/06 ,  C09C1/28 ,  C09C1/36 ,  C09C3/00

Abstract: PROBLEM TO BE SOLVED: To provide the almost spherical and excellently flowable grains, each of which has a homogeneous structure and which are completely redispersed under the condition necessary to disperse the starting solids. SOLUTION: The discrete granules are almost spherical grains having a uniform density distribution and can be completely redispersed under the condition used in the starting solids. The granule consists of the dispersible fine solids having

公开(公告)号：WO2007144237A3

公开(公告)日：2008-10-30

申请号：PCT/EP2007054479

申请日：2007-05-09

Applicant: EVONIK DEGUSSA GMBH ,  KATUSIC STIPAN ,  ZIMMERMANN GUIDO ,  KRAEMER MICHAEL ,  KRESS PETER ,  MIESS HORST

Inventor： KATUSIC STIPAN ,  ZIMMERMANN GUIDO ,  KRAEMER MICHAEL ,  KRESS PETER ,  MIESS HORST

IPC: C01G1/02 ,  C01G9/00 ,  C01G9/03

CPC classification number: C01G1/02 ,  C01G9/00 ,  C01G9/03 ,  C01P2002/52 ,  C01P2002/54 ,  C01P2006/12 ,  C04B35/01 ,  C04B35/053 ,  C04B35/057 ,  C04B35/453 ,  C04B35/457 ,  C04B35/62665 ,  C04B35/6325 ,  C04B2235/3201 ,  C04B2235/3206 ,  C04B2235/3217 ,  C04B2235/3229 ,  C04B2235/3232 ,  C04B2235/3262 ,  C04B2235/3279 ,  C04B2235/3281 ,  C04B2235/3284 ,  C04B2235/40 ,  C04B2235/401 ,  C04B2235/405 ,  C04B2235/449 ,  C04B2235/5409 ,  C04B2235/5436

Abstract: Process for preparing a mixed metal oxide powder, in which oxidizable starting materials are evaporated and oxidized, the reaction mixture is cooled after the reaction and the pulverulent solids are removed from gaseous substances, wherein as starting materials, at least one pulverulent metal and at least one metal compound, the metal and the metal component of the metal compound being different and the proportion of metal being at least 80% by weight based on the sum of metal and metal component from metal compound, together with one or more combustion gases, are fed to an evaporation zone of a reactor, where metal and metal compound are evaporated completely under nonoxidizing conditions, subsequently, the mixture flowing out of the evaporation zone is reacted in the oxidation zone of this reactor with a stream of a supplied oxygen-containing gas whose oxygen content is at least sufficient to oxidize the starting materials and combustion gases completely.

Abstract translation: 制备混合金属氧化物粉末的方法，其中可氧化原料被蒸发和氧化，反应混合物在反应后冷却，并从气态物质中除去粉状固体，其中作为原料，至少一种粉状金属和至少 一种金属化合物，金属化合物的金属和金属组分不同，并且金属比例为至少80重量％，基于来自金属化合物的金属和金属组分的总和与一种或多种燃烧气体一起是 进料到反应器的蒸发区，其中金属和金属化合物在非氧化条件下完全蒸发，随后将从蒸发区流出的混合物在该反应器的氧化区中与供给的含氧气体流 其氧含量至少足以使原料和燃烧气体完全氧化。

公开(公告)号：WO2007144242A3

公开(公告)日：2008-04-03

申请号：PCT/EP2007054760

申请日：2007-05-16

Applicant: EVONIK DEGUSSA GMBH ,  KATUSIC STIPAN ,  ZIMMERMANN GUIDO ,  KRAEMER MICHAEL ,  GOTTFRIED HEIKO ,  KRESS PETER

Inventor： KATUSIC STIPAN ,  ZIMMERMANN GUIDO ,  KRAEMER MICHAEL ,  GOTTFRIED HEIKO ,  KRESS PETER

IPC: C01B13/20 ,  C01F5/04 ,  C01G9/00 ,  C01G9/03

CPC classification number: C01G9/02 ,  C01B13/20 ,  C01F5/04 ,  C01F17/0043 ,  C01G1/02 ,  C01G9/03 ,  C01P2002/52 ,  C01P2006/12

Abstract: Process for preparing a metal oxide powder, in which starting materials are evaporated and oxidized, wherein a metal melt in the form of droplets and one or more combustion gases are fed to the evaporation zone of a reactor, where the metal melt is evaporated completely under nonoxidizing conditions, subsequently, the mixture flowing out of the evaporation zone is reacted in the oxidation zone of this reactor with a stream of a supplied oxygen-containing gas whose oxygen content is at least sufficient to oxidize the metal and the combustion gases completely.

Abstract translation: 制备金属氧化物粉末的方法，其中起始材料被蒸发和氧化，其中将液滴形式的一种或多种燃烧气体的金属熔体进料到反应器的蒸发区，其中金属熔体完全蒸发 非氧化条件下，从蒸发区流出的混合物在该反应器的氧化区中与供氧的气体气流反应，氧气含量至少足以使金属和燃烧气体完全氧化。