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公开(公告)号:IN153152B
公开(公告)日:1984-06-09
申请号:IN891CA1979
申请日:1979-08-29
Applicant: DEGUSSA
Inventor: GOEDECKE RALF DR , LIEBERT MARTIN , NISCHK WOLFGANG DR , PLOTZ WOLFGANG DR , PUSCHNER KURT
IPC: C07D251/28 , C07D55/42
Abstract: There is provided a process for the recovery of cyanuric chloride in solid or liquid form from the reaction mixture which results from the trimerization of cyanogen chloride wherein to recover the cyanuric chloride in liquid or solid form the gaseous reaction mixture is introduced into an apparatus combination consisting essentially of a stripping column and a condenser connected at the outlet side, preferably a head condenser, preferably above the stripping column, and in which the sump of the stripping column is held to the boiling temperature of the cyanuric chloride whereupon the cyanuric chloride contained in the gaseous reaction mixture depending on the regulation of the temperature at the outlet of the condenser in the range of 146 DEG to 190 DEG C. is partially condensed, after which to recover the liquid cyanuric chloride in liquid form it is removed as such at the lower end of the stripping column while the residual gas leaving the condenser and still containing cyanuric chloride, which amount of cyanuric chloride is controlled by the temperature at the outlet of the condenser, is led to a separating chamber and the residual cyanuric chloride is recovered there by known process.
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公开(公告)号:CH641784A5
公开(公告)日:1984-03-15
申请号:CH895879
申请日:1979-10-04
Applicant: DEGUSSA
Inventor: GOEDECKE RALF DR , LIEBERT MARTIN , NISCHK WOLFGANG DR , PUSCHNER KURT , PLOETZ WOLFGANG DR
IPC: C07D251/28
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公开(公告)号:CH643659A5
公开(公告)日:1984-06-15
申请号:CH1027179
申请日:1979-11-16
Applicant: DEGUSSA
Inventor: DAHM FRANZ-LUDWIG , DIEHL HERBERT , EIERMANN KURT DR , LAMBERTY REINHOLD , NISCHK WOLFGANG DR
IPC: G01N27/416 , G01N27/28 , G01N27/52
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公开(公告)号:DE2843382A1
公开(公告)日:1980-04-17
申请号:DE2843382
申请日:1978-10-05
Applicant: DEGUSSA
Inventor: GOEDECKE RALF DR ING DR , LIEBERT MARTIN , NISCHK WOLFGANG DR , PLOETZ WOLFGANG DR , PUSCHNER KURT
IPC: C07D251/28
Abstract: There is provided a process for the recovery of cyanuric chloride in solid or liquid form from the reaction mixture which results from the trimerization of cyanogen chloride wherein to recover the cyanuric chloride at will in liquid or solid form the gaseous reaction mixture is introduced into an apparatus combination consisting essentially of a stripping column and a condenser connected at the outlet side, preferably a head condenser, preferably above the stripping column, and in which the sump of the stripping column is held to the boiling temperature of the cyanuric chloride whereupon the cyanuric chloride contained in the gaseous reaction mixture depending on the regulation of the temperature at the outlet of the condenser in the range of 146 DEG to 190 DEG C. is partially condensed, after which to recover the liquid cyanuric chloride in liquid form it is removed as such at the lower end of the stripping column and is either directly or, in a given case, after an intermediate storage led to a spray tower and is sprayed whereupon the solid, fine-grained cyanuric chloride is withdrawn at the bottom of the spray tower while the residual gas leaving the condenser and still containing cyanuric chloride, which amount of cyanuric chloride is controlled by the temperature at the outlet of the condenser, is led preferably to a separating chamber and the residual cyanuric chloride is recovered there by known process.
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公开(公告)号:CH641788A5
公开(公告)日:1984-03-15
申请号:CH896579
申请日:1979-10-04
Applicant: DEGUSSA
Inventor: GOEDECKE RALF DR , KURANDT UWE , LIEBERT MARTIN , MEWES DIETER DR , NISCHK WOLFGANG DR
IPC: B01J2/02 , C07D251/28
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公开(公告)号:CH641787A5
公开(公告)日:1984-03-15
申请号:CH896479
申请日:1979-10-04
Applicant: DEGUSSA
Inventor: GOEDECKE RALF DR , LIEBERT MARTIN , NISCHK WOLFGANG DR , PUSCHNER KURT , PLOETZ WOLFGANG DR
IPC: C07D251/28
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公开(公告)号:IN153151B
公开(公告)日:1984-06-09
申请号:IN890CA1979
申请日:1979-08-29
Applicant: DEGUSSA
Inventor: GOEDECKE RALF DR , LIEBERT MARTIN , NISCHK WOLFGANG DR , PLOTZ WOLFGANG DR , PUSCHNER KURT
IPC: C07D251/28 , C07D55/42
Abstract: There is provided a process for the recovery of cyanuric chloride in solid or liquid form from the reaction mixture which results from the trimerization of cyanogen chloride wherein to recover the cyanuric chloride at will in liquid or solid form the gaseous reaction mixture is introduced into an apparatus combination consisting essentially of a stripping column and a condenser connected at the outlet side, preferably a head condenser, preferably above the stripping column, and in which the sump of the stripping column is held to the boiling temperature of the cyanuric chloride whereupon the cyanuric chloride contained in the gaseous reaction mixture depending on the regulation of the temperature at the outlet of the condenser in the range of 146 DEG to 190 DEG C. is partially condensed, after which to recover the liquid cyanuric chloride in liquid form it is removed as such at the lower end of the stripping column and is either directly or, in a given case, after an intermediate storage led to a spray tower and is sprayed whereupon the solid, fine-grained cyanuric chloride is withdrawn at the bottom of the spray tower while the residual gas leaving the condenser and still containing cyanuric chloride, which amount of cyanuric chloride is controlled by the temperature at the outlet of the condenser, is led preferably to a separating chamber and the residual cyanuric chloride is recovered there by known process.
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公开(公告)号:CH641785A5
公开(公告)日:1984-03-15
申请号:CH895979
申请日:1979-10-04
Applicant: DEGUSSA
Inventor: GOEDECKE RALF DR , LIEBERT MARTIN , NISCHK WOLFGANG DR , PUSCHNER KURT , PLOETZ WOLFGANG DR
IPC: C07D251/28
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公开(公告)号:DE2850137A1
公开(公告)日:1980-06-12
申请号:DE2850137
申请日:1978-11-18
Applicant: DEGUSSA
Inventor: DAHM FRANZ-LUDWIG DIPL ING , DIEHL HERBERT , EIERMANN KURT DIPL PHYS DR , LAMBERTY REINHOLD , NISCHK WOLFGANG DR
IPC: G01N27/416 , G01N27/28 , G01N27/52
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公开(公告)号:DE2843381A1
公开(公告)日:1980-04-17
申请号:DE2843381
申请日:1978-10-05
Applicant: DEGUSSA
Inventor: GOEDECKE RALF DR ING DR , LIEBERT MARTIN , NISCHK WOLFGANG DR , PLOETZ WOLFGANG DR , PUSCHNER KURT
IPC: C07D251/28
Abstract: There is provided a process for the recovery of cyanuric chloride in solid or liquid form from the reaction mixture which results from the trimerization of cyanogen chloride wherein to recover the cyanuric chloride in liquid or solid form the gaseous reaction mixture is introduced into an apparatus combination consisting essentially of a stripping column and a condenser connected at the outlet side, preferably a head condenser, preferably above the stripping column, and in which the sump of the stripping column is held to the boiling temperature of the cyanuric chloride whereupon the cyanuric chloride contained in the gaseous reaction mixture depending on the regulation of the temperature at the outlet of the condenser in the range of 146 DEG to 190 DEG C. is partially condensed, after which to recover the liquid cyanuric chloride in liquid form it is removed as such at the lower end of the stripping column while the residual gas leaving the condenser and still containing cyanuric chloride, which amount of cyanuric chloride is controlled by the temperature at the outlet of the condenser, is led to a separating chamber and the residual cyanuric chloride is recovered there by known process.
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