公开(公告)号：JP2002284516A

公开(公告)日：2002-10-03

申请号：JP2001391814

申请日：2001-12-25

Applicant: DEGUSSA

Inventor： LORTZ WOLFGANG DR ,  BATZ-SOHN CHRISTOPH DR ,  MANGOLD HELMUT ,  PERLET GABRIELE ,  WILL WERNER

IPC: A61K8/18 ,  A61K8/25 ,  A61Q1/02 ,  C01B33/141 ,  C01B33/18 ,  C03C17/25 ,  C09C1/68 ,  C09G1/02 ,  C09K3/14 ,  D21H19/40 ,  H01L21/304 ,  H01L21/306 ,  A61K7/02

Abstract: PROBLEM TO BE SOLVED: To provide an aqueous dispersion containing silica that is produced by a thermal decomposition method and advantageous when used in a chemical mechanical polishing(CMP) process. SOLUTION: This purpose is achieved by the aqueous dispersion containing silica that is produced by the thermal decomposition method using aerosol by which the silica is doped with alkali. Regarding the silica in the dispersion, an average particle diameter of its second particles is =0.7.

公开(公告)号：JP2003238944A

公开(公告)日：2003-08-27

申请号：JP2003027530

申请日：2003-02-04

Applicant: DEGUSSA

Inventor： LORTZ WOLFGANG DR ,  BATZ-SOHN CHRISTOPH DR ,  PERLET GABRIELE ,  WILL WERNER

IPC: B24B37/00 ,  C01B33/18 ,  C09G1/02 ,  C09K3/14 ,  H01L21/304 ,  H01L21/3105

Abstract: PROBLEM TO BE SOLVED: To provide a dispersion in which an oxide surface can be removed with a high rate during the chemical-mechanical polishing without leaving scratches on the surface to be polished. SOLUTION: The aqueous dispersion contains a silicon dioxide powder prepared by a thermal decomposition process doped with an aluminum oxide in the form of aerosol. The powder has the aluminum oxide content in an amount of 0.01-3 mass%, advantageously 0.2-1.5 mass% relative to the total amount of the powder. The dispersion has an average particle diameter of maximum 0.1 μm. COPYRIGHT: (C)2003,JPO

公开(公告)号：JP2002211915A

公开(公告)日：2002-07-31

申请号：JP2001336247

申请日：2001-11-01

Applicant: DEGUSSA

Inventor： LORTZ WOLFGANG DR ,  BATZ-SOHN CHRISTOPH DR ,  PERLET GABRIELE ,  WILL WERNER

IPC: C03B8/02 ,  C01B33/141 ,  C03B20/00 ,  C03C19/00 ,  C09C1/68 ,  C09G1/02 ,  C09K3/14 ,  D21H19/38 ,  H01L21/306 ,  H01L21/3105 ,  H01L21/321

Abstract: PROBLEM TO BE SOLVED: To provide an easily obtainable aqueous dispersion containing cerium oxide, having a very low impurity content and capable of giving a particle diameter in a reproducible manner. SOLUTION: The aqueous dispersion contains pyrolytic silicon dioxide doped with cerium oxide and this cerium oxide is introduced by aerosol comprising a cerium salt solution or a cerium suspension and has

公开(公告)号：WO2009095141A3

公开(公告)日：2010-09-23

申请号：PCT/EP2008068344

申请日：2008-12-30

Applicant: EVONIK DEGUSSA GMBH ,  LORTZ WOLFGANG ,  SCHEFFLER JOCHEN ,  PERLET GABRIELE

Inventor： LORTZ WOLFGANG ,  SCHEFFLER JOCHEN ,  PERLET GABRIELE

IPC: A01N25/04 ,  A01N25/06 ,  A01N59/00 ,  A01P7/00

CPC classification number: A01N25/04 ,  A01N59/00 ,  A01N61/00 ,  A01N25/06 ,  A01N2300/00

Abstract: Dispersion comprising hydrophobic pyrogenically prepared silicon dioxide, alcohol and at least one additive which promotes the dispersion and, as additional component, at least one insecticide and/or acaricide. The dispersion can be canned in spray cans and used as insecticide.

Abstract translation: 分散体包含疏水性热解法制备的二氧化硅，醇和促进分散的至少一种添加剂，以及作为另外的组分的至少一种杀虫剂和/或杀螨剂。 分散体可以在喷雾罐中罐装并用作杀虫剂。

公开(公告)号：WO2005104851A3

公开(公告)日：2006-01-26

申请号：PCT/EP2005004069

申请日：2005-04-18

Applicant: DEGUSSA

Inventor： LORTZ WOLFGANG ,  SCHEFFLER JOCHEN ,  PERLET GABRIELE

IPC: A01N25/04 ,  A01N59/00 ,  A61K33/00 ,  C01B33/141

CPC classification number: A01N59/00 ,  A01N25/30 ,  A01N25/10 ,  A01N2300/00

Abstract: Dispersion comprising, in addition to water, 0.5 to 20 wt.% of hydrophobic silica, 0.01 to 10 wt.% of a gelling or viscosity-increasing additive, 0.1 to 1 wt.% of a preservative and 0 to 1 wt.% of a surface-active substance. It is prepared by a procedure in which the individual components are dispersed successively or together into the water and in this procedure the individual components are deaerated before and/or during the addition or the dispersion is deaerated during the individual dispersing steps. The dispersion can be employed as an insecticide.

Abstract translation: 分散体除了含有0.5-20重量％的疏水性二氧化硅，0.01至10重量％的胶凝或增粘添加剂，0.1-1重量％的防腐剂和0-1重量％的防腐剂 表面活性物质。 其通过以下步骤制备，其中各个组分相继或一起分散在水中，并且在该步骤中，在各个分散步骤之前和/或加入期间或分散体脱气时，各个组分脱气。 分散体可以用作杀虫剂。

公开(公告)号：WO2010006839A2

公开(公告)日：2010-01-21

申请号：PCT/EP2009056802

申请日：2009-06-03

Applicant: EVONIK DEGUSSA GMBH ,  LORTZ WOLFGANG ,  PERLET GABRIELE ,  DIENER UWE ,  REITZ SASCHA

Inventor： LORTZ WOLFGANG ,  PERLET GABRIELE ,  DIENER UWE ,  REITZ SASCHA

IPC: C09C1/30 ,  C09D7/12

CPC classification number: C09C1/3018 ,  B82Y30/00 ,  C01P2004/64 ,  C01P2006/12 ,  C01P2006/22 ,  C08K3/36 ,  C08K9/06 ,  C09C1/3063 ,  C09C1/3081 ,  C09C1/309 ,  C09D7/62 ,  C09D7/67 ,  Y10T428/2995

Abstract: Process for preparing a dispersion of surface-modified silicon dioxide particles having an average particle diameter of not more than 100 nm by high-pressure milling of a preliminary dispersion comprising a) 10% to 50% by weight of surface-modified silicon dioxide particles, b) at least one glycol monoether of the general formula (A): H3C(CH2)m-O-(CH2)n-[O-(CH2)o]p-OH, c) at least one carboxylic ester of the general formula (B): H2x+1Cx-O-CH2-(CHR)-[O-CHR]y-O-C(=O)-CzH2z+1, d) the molar ratio A/B being 10:90 to 40:60 and m, n, o, p, x, y and z being independent of one another. Dispersion obtainable by this process. Process for producing granules of surface-modified silicon dioxide particles by separating off the liquid phase of the dispersion. Granules obtainable by this process. Use of dispersion and granules in coating materials.

Abstract translation: 通过高压研磨预分散体制备平均粒径不超过100nm的表面改性的二氧化硅颗粒的分散体的方法，所述预分散体包含a）10重量％至50重量％的表面改性的二氧化硅颗粒， b）至少一种通式（A）的二醇单醚：H 3 C（CH 2）m -O-（CH 2）n - [O-（CH 2）o] p -OH，c）至少一种通式 B）：H2x + 1Cx-O-CH2-（CHR） - [O-CHR] yOC（= O）-CzH2z + 1，d）A / B的摩尔比为10:90至40:60，m，n ，o，p，x，y和z彼此独立。 通过该过程可获得分散体。 通过分离分散体的液相来生产表面改性的二氧化硅颗粒的颗粒的方法。 通过该过程可获得的颗粒。 在涂料中使用分散剂和颗粒剂。

公开(公告)号：WO2010006837A2

公开(公告)日：2010-01-21

申请号：PCT/EP2009056733

申请日：2009-06-02

Applicant: EVONIK DEGUSSA GMBH ,  LORTZ WOLFGANG ,  PERLET GABRIELE ,  DIENER UWE ,  REITZ SASCHA

Inventor： LORTZ WOLFGANG ,  PERLET GABRIELE ,  DIENER UWE ,  REITZ SASCHA

IPC: C09C1/30 ,  C08K3/36 ,  C09D7/12 ,  C09J11/02 ,  G03G9/097

CPC classification number: C09C1/3018 ,  B82Y30/00 ,  C01P2004/64 ,  C01P2006/12 ,  C01P2006/22 ,  C08K3/36 ,  C08K9/06 ,  C09C1/3081 ,  C09C1/309 ,  C09D7/62 ,  C09D7/67 ,  G03G9/09716 ,  G03G9/09725 ,  Y10T428/2995

Abstract: Process for preparing surface-modified silicon dioxide particles with a mean particle diameter of at most 100 nm, comprising the steps of: a) providing a predispersion b) high-pressure grinding of the predispersion to form a dispersion c) removing the liquid phase of the dispersion, the predispersion comprising al) surface-modified silicon dioxide particles which are at least partly aggregated, are bonded to the surface-modifying component via Si-O-Si bonds and still have reactive groups on their surface, a2) one or more organosilicon compounds which have at least one silicon-carbon bond and at least one functional group which can react with the reactive groups to form a covalent Si-O-Si bond, and a3) one or more solvents. Redispersible, surface-modified silicon dioxide particles obtainable by this process. Use of these in toner powders, silicone rubber, adhesives and scratch-resistance surface coatings.

Abstract translation: 制备平均粒径为至多100nm的表面改性二氧化硅颗粒的方法，包括以下步骤：a）提供预分散体b）预分散体的高压研磨以形成分散体c）除去 分散体，包含a1）至少部分聚集的表面改性二氧化硅颗粒的预分散体通过Si-O-Si键与表面改性组分键合，并且在其表面上仍具有反应性基团，a2）一个或多个 具有至少一个硅 - 碳键的有机硅化合物和至少一个可与反应性基团反应形成共价Si-O-Si键的官能团，和a）一种或多种溶剂。 可通过该方法获得的可再分散的表面改性二氧化硅颗粒。 在调色剂粉末，硅橡胶，粘合剂和耐刮擦表面涂层中使用这些。

公开(公告)号：WO2006010438A3

公开(公告)日：2006-10-12

申请号：PCT/EP2005007210

申请日：2005-07-05

Applicant: DEGUSSA ,  PERLET GABRIELE ,  LORTZ WOLFGANG ,  BATZ-SOHN CHRISTOPH ,  WILL WERNER ,  REITZ SASCHA

Inventor： PERLET GABRIELE ,  LORTZ WOLFGANG ,  BATZ-SOHN CHRISTOPH ,  WILL WERNER ,  REITZ SASCHA

IPC: C09C1/36 ,  C04B41/50 ,  C09D17/00

CPC classification number: C03C17/256 ,  B82Y30/00 ,  C01P2004/64 ,  C01P2006/12 ,  C03C2217/212 ,  C03C2218/113 ,  C04B41/009 ,  C04B41/5041 ,  C04B41/87 ,  C04B2111/00586 ,  C04B2111/2061 ,  C04B2111/60 ,  C09C1/3669 ,  C09D17/008 ,  C04B41/4539 ,  C04B33/00

Abstract: Aqueous dispersion obtainable by placing in water an aggregated titanium dioxide powder having a specific surface area of from 20 to 150 m 2 /g in such an amount that the desired dispersion comprises at least 20 wt.% titanium dioxide, and at least one amino alcohol having from 1 to 6 carbon atoms, and at least one carboxylic acid from the group comprising dibasic carboxylic acids and/or hydroxycarboxylic acids having from 2 to 6 carbon atoms, - the amino alcohol being present in the dispersion in an amount of from 2.5 to 7.0 µmol./m 2 specific surface area TiO 2 and the carboxylic acid being present in an amount of from 1.0 to 3.5 µmol./m 2 specific surface area TiO 2 , - producing a pre-dispersion by introducing energy in an amount of less than 200 kJ/m 3 and then producing a dispersion in which the aggregated titanium dioxide powder has a mean, volume-related aggregate diameter of less than 150 nm by grinding the pre-dispersion by means of a high-energy mill at a pressure of at least 500 bar. The dispersion can be used in the coating of glass, ceramics and metal surfaces.

Abstract translation: 通过将具有20至150m 2 / g的比表面积的聚集的二氧化钛粉末放置在水中而获得的水溶液，其量使得所需的分散体包含至少20重量％的二氧化钛 和至少一种具有1至6个碳原子的氨基醇，和至少一种含有二元羧酸和/或具有2至6个碳原子的羟基羧酸的羧酸， - 氨基醇存在于分散体 其量为2.5至7.0μmol/ m 2比表面积TiO 2，羧酸的存在量为1.0-3.5μmol/ m 2 比表面积TiO 2 2，通过引入少于200kJ / m 3的量的能量产生预分散，然后 产生其中聚集的二氧化钛粉末通过研磨预分散剂具有小于150nm的平均体积相关聚集体直径的分散体 通过在至少500巴的压力下的高能磨机。 分散体可用于玻璃，陶瓷和金属表面的涂层。

公开(公告)号：WO2009074440A3

公开(公告)日：2010-04-22

申请号：PCT/EP2008065917

申请日：2008-11-20

Applicant: EVONIK DEGUSSA GMBH ,  LORTZ WOLFGANG ,  WILL WERNER ,  REITZ SASCHA ,  PERLET GABRIELE

Inventor： LORTZ WOLFGANG ,  WILL WERNER ,  REITZ SASCHA ,  PERLET GABRIELE

IPC: C01B33/141

CPC classification number: C01B33/1417 ,  C01B33/1415

Abstract: Process for preparing an alkaline dispersion of aggregated silicon dioxide particles by dividing a preliminary dispersion within a pH of 3 to 5 into at least two streams, placing these streams under a pressure of at least 50 bar and depressurizing them to a collision point, each via one nozzle, in a grinding chamber, and admixing the dispersion that runs off at the bottom, while still in the grinding chamber, with an alkaline substance in an amount such that the dispersion overall has a pH of more than 7.

Abstract translation: 通过将3至5的pH范围内的预分散体分成至少两股流，将这些物流放置在至少50巴的压力下并将其减压至碰撞点，从而制备聚集的二氧化硅颗粒的碱性分散体的方法， 一个喷嘴，在研磨室中，并且在仍然在研磨室中的底部上分散的分散体与碱性物质混合，使得分散体总体上具有大于7的pH。

公开(公告)号：WO2009030587A3

公开(公告)日：2010-03-11

申请号：PCT/EP2008060663

申请日：2008-08-14

Applicant: EVONIK DEGUSSA GMBH ,  SCHEFFLER JOCHEN ,  SCHAEFFNER DIRK ,  PERLET GABRIELE ,  LORTZ WOLFGANG

Inventor： SCHEFFLER JOCHEN ,  SCHAEFFNER DIRK ,  PERLET GABRIELE ,  LORTZ WOLFGANG

IPC: A01N59/00 ,  A01N65/00 ,  A01P7/04

CPC classification number: A01N59/00 ,  A01N65/00 ,  A01N25/04 ,  A01N2300/00

Abstract: Dispersion containing, in addition to water, 0.5 to 20% by weight of hydrophobic silica, 0.01 to 10% by weight of a gelling additive, or viscosity-increasing additive, 0.1 to 1% by weight of a preservative, 0 to 1% by weight of a surface -active substance, which, as further component, contains organic insecticides. It is produced by dispersing the individual components successively or together into the water and in this process deaerating the individual components before and/or during the addition or deaerating the dispersion during the individual dispersion steps. The dispersion can be used as insecticide.

Abstract translation: 含水0.5〜20重量％的疏水性二氧化硅，0.01〜10重量％的凝胶化添加剂或粘度增加添加剂的分散液，0.1〜1重量％的防腐剂，0〜1重量％ 表面活性物质的重量，其作为另外的组分含有有机杀虫剂。 它是通过将各个组分连续地或一起分散在水中而产生的，并且在该过程中，在各个分散步骤期间，在加入或脱气分散体之前和/或期间使各个组分脱气。 分散体可用作杀虫剂。