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    WOOD HEATER WITH ALTERNATING MICROWAVE LAUNCH LOCATIONS AND ENHANCED HEATING CYCLES
    1.
    发明申请
    WOOD HEATER WITH ALTERNATING MICROWAVE LAUNCH LOCATIONS AND ENHANCED HEATING CYCLES 审中-公开
    木质加热器，配有微波启动位置和增强加热循环

    公开(公告)号：WO2012087874A2

    公开(公告)日：2012-06-28

    申请号：PCT/US2011/065732

    申请日：2011-12-19

    Applicant: EASTMAN CHEMICAL COMPANY

    Inventor： KIMREY, Harold, Dall ,  ATTRIDE, David, Carl ,  OVERTURF, Brad, William ,  SHELTON, Mark, Robert

    IPC: B27K5/00 ,  B27M1/00 ,  H05B6/64 ,  F26B3/347

    CPC classification number: B27K5/0055 ,  B27K3/346 ,  C08H8/00 ,  F26B3/347 ,  F26B5/048 ,  F26B2210/16 ,  H05B6/707 ,  H05B6/763 ,  H05B6/80 ,  H05B2206/046 ,  Y02P20/124

    Abstract: An optimized system and process for heating wood using a microwave heater. The optimized system/process directs microwave energy towards different regions of the wood at different times during heating. In certain situations, microwave energy is introduced into the heater using microwave launchers and the system includes one or more microwave switches that control distribution of microwave energy to the microwave launchers so that two adjacent and/or opposing microwave launchers do not simultaneously introduce microwave energy into the heater. The optimized heating process also includes heating wood using a plurality of sequential heating cycles carried out at different conditions. For example, at least one of the heating cycles can be carried out at a lower input rate of microwave energy and/or at a lower pressure than one of the previous heating cycles.

    Abstract translation: 使用微波加热器加热木材的优化系统和工艺。 优化的系统/过程在加热期间的不同时间将微波能量引导到木材的不同区域。 在某些情况下，使用微波发射器将微波能量引入加热器，并且该系统包括一个或多个微波开关，其控制微波能量向微波发射器的分布，使得两个相邻和/或相对的微波发射器不同时将微波能量引入 加热器。 优化的加热过程还包括使用在不同条件下进行的多个连续加热循环加热木材。 例如，至少一个加热循环可以以较低的微波能量输入速率和/或比之前的加热循环之一更低的压力进行。

    MICROWAVE WOOD HEATER WITH ENHANCED SPATIAL USAGE EFFICIENCY AND UNIFORMITY OF HEAT DISTRIBUTION
    2.
    发明申请
    MICROWAVE WOOD HEATER WITH ENHANCED SPATIAL USAGE EFFICIENCY AND UNIFORMITY OF HEAT DISTRIBUTION 审中-公开
    具有增强空间使用效率和散热均匀性的微波炉加热器

    公开(公告)号：WO2012087883A2

    公开(公告)日：2012-06-28

    申请号：PCT/US2011/065745

    申请日：2011-12-19

    Applicant: EASTMAN CHEMICAL COMPANY

    Inventor： OVERTURF, Brad, William ,  KIMREY, Harold, Dail, Jr. ,  ATTRIDE, David, Carl ,  SHELTON, Mark, Robert

    IPC: B27K5/00 ,  B27M1/00

    CPC classification number: B27K5/0055 ,  B27K3/346 ,  C08H8/00 ,  F26B3/347 ,  F26B5/048 ,  F26B2210/16 ,  H05B6/707 ,  H05B6/763 ,  H05B6/80 ,  H05B2206/046 ,  Y02P20/124

    Abstract: A commercial scale microwave system that includes a heater having enhanced heat distribution and minimized void space. The enhanced heat distribution can be provided by a unique launcher and/or reflector configuration disposed in the interior of the microwave heater. The microwave system can be operated to prevent the wood from both overheating (which results in scorching) and under-heating (which results in inadequate drying and/or inadequate thermal- modification). The microwave heating system can provide enhanced microwave energy distribution for large quantities of wood, even large quantities of wood heated under vacuum and/or in the presence of one or more chemical reagents.

    Abstract translation: 一种商业规模的微波系统，其包括具有增强的热分布和最小化空隙空间的加热器。 可以通过设置在微波加热器内部的独特的发射器和/或反射器配置来提供增强的热分布。 可以操作微波系统以防止木材过热（导致焦化）和欠热（导致不充分的干燥和/或不适当的热改性）。 微波加热系统可以为大量木材提供增强的微波能量分布，甚至在真空下和/或在一种或多种化学试剂存在下加热大量的木材。

    WOOD HEATER WITH ENHANCED MICROWAVE DISPERSING AND TM-MODE MICROWAVE LAUNCHERS
    5.
    发明申请
    WOOD HEATER WITH ENHANCED MICROWAVE DISPERSING AND TM-MODE MICROWAVE LAUNCHERS 审中-公开
    增强型微波分散木质加热器和TM型微波发射器

    公开(公告)号：WO2012087880A2

    公开(公告)日：2012-06-28

    申请号：PCT/US2011/065741

    申请日：2011-12-19

    Applicant: EASTMAN CHEMICAL COMPANY

    Inventor： KIMREY, Harold, Dail, Jr. ,  ATTRIDE, David, Carl ,  OVERTURF, Brad, William ,  SHELTON, Mark, Robert

    IPC: B27K5/00

    CPC classification number: B27K5/0055 ,  B27K3/346 ,  C08H8/00 ,  F26B3/347 ,  F26B5/048 ,  F26B2210/16 ,  H05B6/707 ,  H05B6/763 ,  H05B6/80 ,  H05B2206/046 ,  Y02P20/124

    Abstract: A microwave heater capable of heating a bundle of wood and equipped with an optimized system for introducing microwave energy into the heater is provided. Also provided is an enhanced system for launching and dispersing within the heater. The system uses one or more TM ab microwave launchers to emit microwave energy in the interior of the microwave heater in a TM ab mode, where a is 0 and b is an integer between 1 and 5. The TM ab launchers can be configured to emit microwave energy through an open outlet that faces generally parallel to the nearest wall of the heater. In certain situations, it can be advantageous to use at least two TM ab microwave launchers having open outlets that face towards one another. In certain situations, it can be advantageous to use at least two TM ab microwave launchers located on generally opposite sides of the microwave heater. In certain situations, the system can also include one or more moving reflectors for dispersing microwave energy emitted from the TM ab microwave launchers.

    Abstract translation: 提供了一种微波加热器，其能够加热一捆木材并配备有用于将微波能量引入加热器的优化系统。 还提供了一个用于在加热器内启动和分散的增强系统。 该系统使用一个或多个TM微波发射器以微波加热器的内部以TM模式发射微波能量，其中a为0且b为整数 在1和5之间。TM发射器可以被配置成通过面向大致平行于加热器的最近的壁的开口出口发射微波能量。 在某些情况下，使用至少两个具有面向彼此的开口出口的微波发射器可能是有利的。 在某些情况下，使用位于微波加热器的大体相对侧上的至少两个TM微波发射器可能是有利的。 在某些情况下，该系统还可以包括一个或多个移动反射器，用于分散从微波发射器发射的微波能量。

    PROCESS FOR THE PREPARATION OF ALKYL 1-METHYLCYCLOPROPANECARBOXYLATE
    10.
    发明公开
    PROCESS FOR THE PREPARATION OF ALKYL 1-METHYLCYCLOPROPANECARBOXYLATE 审中-公开
    制备1-甲基环丙烷羧酸烷基酯的方法

    公开(公告)号：EP1305277A2

    公开(公告)日：2003-05-02

    申请号：EP01959006.6

    申请日：2001-07-19

    Applicant: EASTMAN CHEMICAL COMPANY

    Inventor： HUBBS, John, Clark ,  ATTRIDE, David, Carl ,  BOAZ, Neil, Warren ,  CIULA, James, Charles ,  MADDOX, John, Thorton ,  NABIH, Thomas ,  NOTTINGHAM, William, Dell ,  SPENCER, David, Chris

    IPC: C07C69/74 ,  C07C69/63 ,  C07C67/317 ,  C07C67/307 ,  C07C67/00 ,  C07C209/56 ,  C07C211/35

    CPC classification number: C07C209/56 ,  C07C67/00 ,  C07C67/307 ,  C07C67/317 ,  C07C2601/02 ,  C07C69/74 ,  C07C69/63 ,  C07C211/35

    Abstract: Disclosed is a 4-step process for the preparation of alkyl esters of 1-methylcyclopropanecarboxylic acid which comprises the steps of (1) converting η-butyrolactone to α-methyl-η-butyrolactone; (2) converting the α-methyl-η-butyrolactone from step (1) to an alkyl 4-halo-2-methyl-butyrate; (3) producing a xylene solution of the alkyl 4-halo-2-methyl-butyrate; and (4) contacting the xylene solution of the alkyl 4-halo-2-methylbutyrate from step (3) with an alkali metal alkoxide under conditions to temperature and pressure which causes vaporization of (i) an alkanol as it is fomred and (ii) an alkyl 1-methylcyclopropanecarboxylate as it si formed from the alkyl 4-halo-2-methylbutyrate. Also disclosed are processes whereby the alkyl 1-methylcyclopropanecarboxylate, prepared as described above, is converted to 1-methylcyclopropylamine.

    Abstract translation: 公开了制备1-甲基环丙烷羧酸烷基酯的四步方法，其包括以下步骤：（1）将η-丁内酯转化为α-甲基-η-丁内酯; （2）将来自步骤（1）的α-甲基-η-丁内酯转化成4-卤代-2-甲基丁酸烷基酯; （3）制备4-卤代-2-甲基丁酸烷基酯的二甲苯溶液; （4）使得来自步骤（3）的4-卤代-2-甲基丁酸烷基酯的二甲苯溶液与碱金属醇盐在导致（i）成链烷醇汽化的温度和压力条件下接触，并且（ii） ）由4-卤代-2-甲基丁酸烷基酯形成的1-甲基环丙烷羧酸烷基酯。 还公开了将如上所述制备的1-甲基环丙烷羧酸烷基酯转化为1-甲基环丙胺的方法。

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