4.
    发明专利
    未知

    公开(公告)号:BR9107188A

    公开(公告)日:1994-09-27

    申请号:BR9107188

    申请日:1991-12-10

    Applicant: HOECHST AG

    Abstract: In a method for continuous nitration of a nitrable aromatic compound, which forms an azeotrope with water, by treating with nitric acid in the presence of nitrating acids, the reaction is carried out with a molar ratio of nitric acid to the aromatic compound of at least 1:1, the temperature and the pressure being coordinated so that the reaction mixture boils, the nitrating acid is recycled without further intermediate treatment, the resulting mixture is extracted with water and the eluate is returned to the reaction to restore the nitrating acid.

    METHOD FOR THE CONTINUOUS NITRATION OF NITRABLE AROMATIC COMPOUNDS

    公开(公告)号:CA2099108A1

    公开(公告)日:1992-06-25

    申请号:CA2099108

    申请日:1991-12-10

    Applicant: HOECHST AG

    Abstract: HOE 90/F 390 Process for the continuous nitration of nitratable aromatic compounds A process for the continuous nitration of a nitratable aromatic compound, which forms an azeotrope with water, by treatment with nitric acid in the presence of nitrating acids, which comprises carrying out the reaction using a molar ratio of nitric acid to the aromatic compound of at least 1.1, the temperature and the pressure being coordinated with one another in such a way that the reaction mixture boils, recycling the nitrating acid in the circulation without further intermediate treatment, extracting the product mixture with water and recycling the eluate, to return nitrating acid. to the reaction.

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