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公开(公告)号:DE3662257D1
公开(公告)日:1989-04-13
申请号:DE3662257
申请日:1986-05-16
Applicant: HOECHST AG
Inventor: SCHWARZMAIER PETER , FROHLICH WALTER DR , KUHN WENZEL DR , RIEDL JOSEF DR , SCHAFFELHOFER IWO DR , MITTERMAIER ERICH , KRUMBOCK REINHARD
IPC: C07C17/04 , C07C17/00 , C07C17/38 , C07C17/383 , C07C19/045 , C07C67/00
Abstract: A process for the purification of 1,2-dichloroethane is described, in which the crude product, containing not more than 3% by weight of high-boilers, is distilled in a first column at 125 DEG to 180 DEG C. in such a way that the bottom product contains not more than 7% by weight of high-boilers. The purified, vaporous 1,2-dichloroethane discharged at the head of this column is used to heat product streams containing 1,2-dichloroethane. The bottom product from the first column is distilled in a second column, advantageously at a pressure of 5 to 40 kPa, together with a feed composed of vaporous 1,2-dichloroethane obtained from the reaction of ethylene with chlorine. The process makes it possible to purify 1,2-dichloroethane with a saving in energy.
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公开(公告)号:DE3460268D1
公开(公告)日:1986-08-07
申请号:DE3460268
申请日:1984-08-03
Applicant: HOECHST AG
Inventor: FELIX BERND DR , FROHLICH WALTER DR , KATZENBERGER HEINER
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公开(公告)号:ES2054710T3
公开(公告)日:1994-08-16
申请号:ES88100904
申请日:1988-01-22
Applicant: HOECHST AG , UHDE GMBH
Inventor: LINK GERHARD , FROHLICH WALTER DR , KRUMBOCK REINHARD , PRANTL GEORG , SCHAFFELHOFER IWO DR
Abstract: Gaseous 1,2-dichloroethane which has been produced in a variety of ways is heated indirectly by the hot, vinyl chloride-containing gases which are led away from the radiation zone of the pyrolysis furnace. This allows the heat of the pyrolysis gases to be utilised in a favourable manner, pyrolysis rates to be increased, and operation times of the pyrolysis furnace to be prolonged.
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