公开(公告)号：DE2231148A1

公开(公告)日：1974-01-31

申请号：DE2231148

申请日：1972-06-26

Applicant: HOECHST AG

Inventor： DIERY HELMUT DR ,  HESS PETER DR ,  SCHNEIDER KARL-HEINZ ,  SCHNEIDER GERHART DR

IPC: D06M11/00 ,  D06B7/00 ,  D06M11/38 ,  D06M11/40 ,  D06M13/288 ,  D06M23/00 ,  D06M101/00 ,  D06M101/02 ,  D06M101/06 ,  D06M1/14

Abstract: Aqueous mercerizing solutions containing alkali metal hydroxide and 0.1 to 5 g/l of a phosphonic acid derivative of the formula 2/6 IN WHICH R is aliphatic hydrocarbon radical and X and Y each is hydrogen, an alkali metal ion or a lower aliphatic radical, and the use of these solutions in a process for mercerizing cellulose fibrous material..

公开(公告)号：DE3839004A1

公开(公告)日：1990-05-31

申请号：DE3839004

申请日：1988-11-18

Applicant: HOECHST AG

Inventor： TRONICH WOLFGANG DR ,  HESS PETER DR

IPC: C07C209/22 ,  C07C209/00 ,  C07C209/10 ,  C07C211/56

Abstract: Process for the preparation of 4,4'-dinitrodiphenylamine which comprises reacting 1 mole of 4-halonitrobenzene with about 1 to about 3 moles of an alkali metal cyanate in the presence of about 0.5 to about 5 moles of water in dimethylsulfoxide at temperatures of about 150 DEG to about 170 DEG C.

公开(公告)号：DE3560678D1

公开(公告)日：1987-10-29

申请号：DE3560678

申请日：1985-08-29

Applicant: HOECHST AG

Inventor： HESS PETER DR ,  KOHLHAAS FOLKER DR ,  PAPENFUHS THEODOR DR

IPC: C07C315/00 ,  C07C67/00 ,  C07C313/00 ,  C07C315/04 ,  C07C317/36 ,  C07C317/40 ,  C07C147/12

Abstract: A process for the preparation of 3-(acyl)amino-4-alkoxy-phenyl- beta -hydroxyethyl-sulfone (sulfates) of the formula (1) (1) in which R1 is alkyl having 1-4 carbon atoms and R2 is hydrogen or one of the groupings +TR with the proviso that n=1 if R2=H and n=0 if R2=acyl, by converting 2-alkoxyacylanilines of the formula (2) (2) in which R1 and R2 have the meanings given, in a known manner to the corresponding sulfochlorides substituted in the p-position relative to the alkoxy group, reducing the sulfochlorides with an alkali metal sulfite or ammonium sulfite in an aqueous medium at pH 7.0-8.5 and at -5 to +40 DEG C. to give the corresponding sulfinates, alkoxylating the latter with ethylene oxide in an aqueous medium at pH 6.0-8.5 and 40 DEG -80 DEG C. to give the 3-acylamino-4-alkoxyphenyl- beta -hydroxyethyl-sulfones of the formula (1) (with R2=acyl and n=0) and, if appropriate, esterifying the latter, with deacylation, with concentrated sulfuric acid at 70 DEG -150 DEG C. to give the compounds of the said formula (1) (with R2H and n=1).

公开(公告)号：CH527282A

公开(公告)日：1972-10-13

申请号：CH1662771

申请日：1971-11-15

Applicant: HOECHST AG

Inventor： SMERZ OTTO DR ,  WERNER LINKE ,  SCHARF ALBERT DR ,  HESS PETER DR

IPC: D06M13/217 ,  D01F6/62 ,  D06M15/53 ,  D01F7/06

公开(公告)号：DE3432891A1

公开(公告)日：1986-03-20

申请号：DE3432891

申请日：1984-09-07

Applicant: HOECHST AG

Inventor： HESS PETER DR ,  KOHLHAAS FOLKER DR ,  PAPENFUHS THEODOR DR

IPC: C07C315/00 ,  C07C67/00 ,  C07C313/00 ,  C07C315/04 ,  C07C317/36 ,  C07C317/40 ,  C07C147/12

Abstract: A process for the preparation of 3-(acyl)amino-4-alkoxy-phenyl- beta -hydroxyethyl-sulfone (sulfates) of the formula (1) (1) in which R1 is alkyl having 1-4 carbon atoms and R2 is hydrogen or one of the groupings +TR with the proviso that n=1 if R2=H and n=0 if R2=acyl, by converting 2-alkoxyacylanilines of the formula (2) (2) in which R1 and R2 have the meanings given, in a known manner to the corresponding sulfochlorides substituted in the p-position relative to the alkoxy group, reducing the sulfochlorides with an alkali metal sulfite or ammonium sulfite in an aqueous medium at pH 7.0-8.5 and at -5 to +40 DEG C. to give the corresponding sulfinates, alkoxylating the latter with ethylene oxide in an aqueous medium at pH 6.0-8.5 and 40 DEG -80 DEG C. to give the 3-acylamino-4-alkoxyphenyl- beta -hydroxyethyl-sulfones of the formula (1) (with R2=acyl and n=0) and, if appropriate, esterifying the latter, with deacylation, with concentrated sulfuric acid at 70 DEG -150 DEG C. to give the compounds of the said formula (1) (with R2H and n=1).

公开(公告)号：DE2301437A1

公开(公告)日：1974-08-08

申请号：DE2301437

申请日：1973-01-12

Applicant: FARRWERKE HOECHST AG VORMALS M

Inventor： BUEKING HANS-WALTER DR ,  HESS PETER DR ,  KOENIG FRANZ ,  SAHM WILFRIED DR ,  SCHNEIDER GERHART DR

IPC: C11D3/32 ,  C11D3/39 ,  C11D3/42

Abstract: Peracylated aliphatic polyamines are useful as activators for inorganic peroxo compounds, i.e., they set free the available oxygen of the peroxo compounds in aqueous solutions at temperatures below 80 DEG C and are thus useful as additives to detergents especially inasmuch as they are compatible with usual detergent brighteners.

公开(公告)号：DE58903809D1

公开(公告)日：1993-04-22

申请号：DE58903809

申请日：1989-11-15

Applicant: HOECHST AG

Inventor： TRONICH WOLFGANG DR ,  HESS PETER DR

IPC: C07C209/22 ,  C07C209/00 ,  C07C209/10 ,  C07C211/56

Abstract: Process for the preparation of 4,4'-dinitrodiphenylamine which comprises reacting 1 mole of 4-halonitrobenzene with about 1 to about 3 moles of an alkali metal cyanate in the presence of about 0.5 to about 5 moles of water in dimethylsulfoxide at temperatures of about 150 DEG to about 170 DEG C.

公开(公告)号：DE2301235A1

公开(公告)日：1974-07-25

申请号：DE2301235

申请日：1973-01-11

Applicant: HOECHST AG

Inventor： HESS PETER DR ,  BUECKING HANS-WALTER DR ,  SCHNEIDER GERHART DR

IPC: C11D3/39 ,  D06L3/02