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    Water-soluble monoazo dyestuffs containing a naphthalene diazo component
    1.
    发明授权
    Water-soluble monoazo dyestuffs containing a naphthalene diazo component 失效
    含有萘二甲酸酯组分的水溶性单稳态脱水剂

    公开(公告)号：US3655642A

    公开(公告)日：1972-04-11

    申请号：US3655642D

    申请日：1969-08-19

    Applicant: HOECHST AG

    Inventor： MEININGER FRITZ ,  HUNGER KLAUS

    IPC: C09B62/006 ,  C09B62/44 ,  C09B62/51 ,  C09B29/16

    CPC classification number: C09B62/51 ,  C09B62/006 ,  C09B62/4413

    Abstract: A WATER-SOLUBLE MONOAZO DYESTUFF HAVING IN FORM OF THE FREE ACID THE FORMULA

    1,5-BIS(X-O2S-),3-(A-N=N-)NAPHTHALENE

    WHEREIN X REPRESENTS-CH=CH2,-CH2-CH2-OH,

    -CH2-CH2-O-SO3H,-CH2-CH2-S-SO3H

    -CH2-CH2-O-PO3H2,-CH2-CH2-C1

    -CH2-CH2-BR,-CH2-CH2-O-SO2-CH3

    PHENYL-SO2-O-CH2-CH2-, -CH2-CH2-OOC-CH3, PHENYL-O-CH2-CH2-

    OR-CH2-CH2-N(LOWER ALKYL)2, AND A REPRESENTS AS A RADICAL OF A COUPLING COMPONENT HYDROXYPHENYLENE, HYDROXYPHENYLENE SUBTITUTED BY LOWER ALKYL, LOWER ALKOXY OR SULFO; HYDROXYNAPHTHYLENE, HYDROXYNAPHTHYLENE SUBSTITUTED BY LOWER ALKYL, LOWER ALKOXY, SULFO, ACETOACETYLAMINO, BENZOYLAMINO, ACRYLOYLAMINO, 2,6-DICHLORO-S-TRIAZINYLAMINO, 2-CHLORO-6-AMINO-S-TRIAZINYLAMINO, 2,6-DIHYDROXYS-TRIAZINYLAMINO, SULFACETYLAMINO OR N-ACETYL-N-METHYLAMINO; AMINOANPHTHYLENE, AMINONAPHTHYLENE SUBSTITUTED BY SULFO OR HYDROXYL; 2-HYDROXY-3-NAPHTHOIC ACID ANILIDE, 2-HYDROXY-3-NAPHTOIC ACID ANILIDE SUBSTITUTED ON THE BENZENE NUCLEUS OF THE SNILIDE RADICAL BY LOWER ALKYL, LOWER ALKOXY OR CHLORINE OR BROMINE; 2-HYDROXY-3-NAPHTHOIC ACID NAPHTHYLIDE, 2-HYDROXY-3-NAPHTHOIC ACID NAPHTHYLIDE SUBSTITUTED ON THE NAPHTHALENE NUCLEUS OF THE NAPHTHYLIDE RADICALS BY LOWER ALKYL, LOWER ALKOXY OR CHLORINE OR BROMINE; 1-PHENYL-5-PYRAZOLONE BEING SUBSTITUTED IN THE 3POSITION BY LOWER ALKYL, LOWER ALKOXY, CARB-LOWER ALKOXY, CARBOXYL OR CARBAMYL; 1-PHENYL-5-PYRAZOLONE BEING SUBSTITUTED IN THE 3-POSITION BY LOWER ALKYL, LOWER ALKOXY, CARB-LOWER ALKOXY, CARBOXYL OR CARBAMYL AND ON THE PHENYL RING THE CHLORINE, BROMINE OR SULFO, 1-NAPHTYL-5PYRAZOLONE BEING SUBSTITUTED IN THE 3-POSITION BY LOWER ALKYL, LOWER ALKOXY, CARB-LOWER ALKOXY, CARBOXYL OR CARBAMYL; 1-NAPHTHYL-5-PYRAZOLONE BEING SUBSTITUTED IN THE 3-POSITION BY LOWER ALKYLY, LOWER ALKOXY, CARB-LOWER ALKOXY, CARBOXYL OR CARBAMYL AND ON THE NAPHTHYL RING BY CHLORINE, BROMINE OR SULFO; SAID DYESTUFFS WHICH HAVE A HIGH TINCTORIAL STRENGTH BEING SUITABLE FOR THE DYEING OR PRINTING OF FIBROUS MATERIALS CONSISTING OF WOOL, SILK, POLYAMIDE FIBERS AND NATIVE OR REGENERATED CELLULOSE FIBERS, THE DYEINGS AND PRINTS OBTAINED ON SAID MATERIALS BEING DISTINGUISHED BY CLEAR SHADES, GOOD STABILITY TOWARDS ALKALINE AGENTS AND DRY CLEANING, HIGH DEGREE OF FIXATION AND GOOD TO VERY GOOD FASTENESS PROPERTIES TO WETTING AND TO LIGHT.

    Process for the dyeing or printing of nitrogen containing textile materials
    2.
    发明授权
    Process for the dyeing or printing of nitrogen containing textile materials 失效
    含氮纺织材料的染色或印花工艺

    公开(公告)号：US3907495A

    公开(公告)日：1975-09-23

    申请号：US40542773

    申请日：1973-10-11

    Applicant: HOECHST AG

    Inventor： MEININGER FRITZ ,  HUNGER KLAUS ,  OSTERLOH FRITZ ,  BERNER KLAUS

    IPC: C09B62/503 ,  D06P3/10 ,  D06P1/06 ,  D06P1/39

    CPC classification number: D06P3/10 ,  Y10S8/917 ,  Y10S8/924

    Abstract: Process for dyeing or printing nitrogen containing native or synthetic fibrous materials, such as wool, silk or fibres of polyamide, which comprises the dyeing or printing of the said fibrous materials with a water-soluble dyestuff of the formula

    IN WHICH F represents the rest of a monoazo- or 1-amino-4phenyl-amino-anthraquinone-2-sulfonic acid dyestuff, Y represents a direct linkage or one of the groups

    OR

    Z represents a hydrogen atom or an alkali metal atom or the ammonium group, and n represents the integer 1, 2 or 3, at a temperature between about 20* and about 115* C and at a pH-value between about 4.0 and about 7.5, the dyeings and prints so prepared being distinguished by very good fastness to processing and fastness to wear, such as fastness to wet and fastness to light.

    Abstract translation: 含有天然或合成纤维材料（如羊毛，丝绸或聚酰胺纤维）的含氮染色或印刷方法，其包括用式IN的水溶性染料染色或印刷所述纤维材料，其中F 单 - 或1-氨基-4-苯基 - 氨基 - 蒽醌-2-磺酸染料，Y表示直接键或基团之一或Z表示氢原子或碱金属原子或铵基，n表示 代表整数1,2或3，在约20至约115℃的温度和约4.0至约7.5的pH值之间，所制备的染色和印花的特征在于非常好的加工牢度和牢度 穿着，如坚牢耐湿，耐光。

    Bis-methylene-amides of phosphoric acids and their thio-derivatives
    3.
    发明授权
    Bis-methylene-amides of phosphoric acids and their thio-derivatives 失效
    磷酸二苯甲酯及其衍生物

    公开(公告)号：US3646134A

    公开(公告)日：1972-02-29

    申请号：US3646134D

    申请日：1969-02-04

    Applicant: HOECHST AG

    Inventor： HUNGER KLAUS

    IPC: C07F9/22 ,  C07F9/24 ,  C07F9/44 ,  C07F9/6533 ,  C08K5/5399

    CPC classification number: C08K5/5399 ,  C07F9/224 ,  C07F9/2458 ,  C07F9/247 ,  C07F9/44 ,  C07F9/6533 ,  C10M2223/02 ,  C10M2223/049 ,  C10M2223/06 ,  C10M2223/061

    Abstract: BIS-METHYLENE AMIDES OF PHOSPHORIC OR PHOSPHORIC ACID, AND THEIR THIO DERIVATIVES, USEFUL AS LUBRICANT ADDITIVES HAVING ANTIOXIDANT AND THERMAL-STABILIZING PROPERTIES, OF THE FORMULA

    R1-C(-R2)=N-P(=Z)(-X)-N=C(-R3)-R4

    TO FORM AN INTERMEDIATE WHICH IS SUBSEQUENTLY OXIDIZED WITH OXYGEN OR SULFUR. SPECIFIC BIS-METHYLENES OF A PHOSPHONIC ACID IN WHICH X IS HYDROCARBYL OR DIALKYLAMINO.

    Y-P(-X)-Y

    WHERE Y IS CHLORINE OR BROMINE, OF WITH A COMPOUND OF THE FORMULA

    Y-P(=Z)(-X)-Y

    WHEREIN R1-R4, TAKEN ALONE, ARE THE SAME OR DIFFERENT AND ARE ALKYL, CYCLOHEXYL, PHENYL, MONO- OR DI-CHLOROOR BROMOPHENYL, OR ALKYLPHENYL; OR R1 AND R2, TAKEN TOGETHER, OR R3 AND R4, TAKEN TOGETHER, ARE ALKYLENE; X IS ALKYL, CYCLOHEXYL, PHENYL, OR ALKYLPHENYL BOND DIRECTLY TO CARBON OR BY WAY OF AN OXYGEN OR SULFUR ATOM, OR MORPHOLINO OR DIALKYLAMINO; AND Z IS OXYGEN OR SULFUR. METHODS OF MAKING SAID COMPOUNDS BY REACTING A KETAMINE OR MIXTURE OF KETAMINES WITH A COMPOUND OF THE FORMULA

    4.
    发明专利
    未知

    公开(公告)号：DK157935B

    公开(公告)日：1990-03-05

    申请号：DK293683

    申请日：1983-06-24

    Applicant: HOECHST AG

    Inventor： HUNGER KLAUS ,  FROELICH HEINRICH ,  LENZ HANS-JOACHIM

    IPC: C09B35/033 ,  C08K5/23 ,  C09B31/11 ,  C09B35/10 ,  C09B41/00 ,  C09B67/22

    Abstract: Diaryl pigments having an excellent stability to heat are obtained by carrying out the coupling of bis-diazotized 3,3'-dichloro-4,4'-diaminobiphenyl with acetoacetanilides in the presence of an added quantity of acetoacetanilides which are monosubstituted or disubstituted in the 3-position or 4-position of the nucleus. As a result of their good heat stability, these pigments are particularly suitable for pigmenting plastics having processing temperatures above 200 DEG C.

    PROCESS FOR THE PREPARATION OF 4,4'-DIAZO COMPOUNDS OF 3,3'-DIALKOXYBIPHENYLS
    5.
    发明专利
    PROCESS FOR THE PREPARATION OF 4,4'-DIAZO COMPOUNDS OF 3,3'-DIALKOXYBIPHENYLS 未知

    公开(公告)号：IN164898B

    公开(公告)日：1989-07-01

    申请号：IN242CA1986

    申请日：1986-03-25

    Applicant: HOECHST AG

    Inventor： HERTEL HASSO ,  HUNGER KLAUS ,  FROELICH HEINRICH

    IPC: C09B35/02 ,  C09B35/08 ,  C09B35/00

    Abstract: bis-Diazo compounds of the formula (1) in which R is a straight-chain or branched alkyl or alkoxyalkyl radical of 3 to 5 carbon atoms and Y is an anti-diazotate radical -N=N-O ME , in which ME represents a potassium atom or sodium atom, or is the radical -N=N-Z, in which Z represents the radical of a water-soluble aliphatic or aromatic amine containing a sulpho and/or carboxyl group are prepared by bisdiazotising a diamine of the formula (2) in which R has the abovementioned meaning in an aqueous, strong, non-oxidising inorganic or organic acid with an alkali metal nitrite at temperatures of about -10 DEG C to about +40 DEG C and converting the bisdiazonium compound formed either into the anti-bisdiazotate of the formula (1) mentioned where Y is -N=N-O ME or into a bisdiazoamino compound of the formula (1) where Y is -N=N-Z in a manner known per se, followed by precipitation.

    7.
    发明专利
    未知

    公开(公告)号：BR8601373A

    公开(公告)日：1986-12-02

    申请号：BR8601373

    申请日：1986-03-26

    Applicant: HOECHST AG

    Inventor： HERTEL HASSO ,  HUNGER KLAUS ,  FROLICH HEINRICH

    IPC: D06P1/12 ,  C09B35/14 ,  D06P3/68 ,  C09B35/037 ,  D06P3/60

    Abstract: Using the method of azoic dyeing, fast blue dyeings are obtained when the bis-diazotable diazo component used is a compound of the general formula (1) (1) in which R is a straight-chain or branched alkyl group of 3 to 5 carbon atoms or a (C1-C3)-alkoxy-(C2-C4)-alkyl group having straight-chain and/or branched alkyl groups of in total 3 to 5 carbon atoms, and the coupling component used is a compound conforming to the general formula (2) (2) in which Z stands for a hydrogen atom or a halogen atom or an alkoxy group of 1 to 4 carbon atoms and Aryl denotes a phenyl radical or a 1-naphthyl radical which can be substituted by 1, 2 or 3 substituents from the group consisting of halogen, nitro, alkyl of 1 to 4 carbon atoms and alkoxy of 1 to 4 carbon atoms, and the coupling reaction and dye formation on the fiber are carried out at a pH value between 4 and 10.

    9.
    发明专利
    未知

    公开(公告)号：MX144087A

    公开(公告)日：1981-08-26

    申请号：MX16746176

    申请日：1976-12-16

    Applicant: HOECHST AG

    Inventor： HUNGER KLAUS ,  WEDER KIETER

    IPC: C08K5/00 ,  C08K5/22 ,  C08L7/00 ,  C08L21/00 ,  C08L33/00 ,  C08L33/02 ,  C08L67/00 ,  C08L77/00 ,  C09B35/34 ,  C09D7/00 ,  C09D7/12 ,  C09B31/10

    Abstract: 1527009 Disazo pigments HOECHST AG 17 Dec 1976 [20 Dec 1975] 52818/76 Heading C4P Novel disazo pigments having the formula (where each K independently is the radical of a coupling component which does not contain watersolubilizing groups) are prepared by tetraazotizing 3,8-diamino-phenanthridone and coupling with 2 mols. of a coupling component, or a mixture of coupling components of formula K-H. The coupling is preferably carried out in the presence of a surfactant and organic solvent. The product is preferably heated in an aqueous, aqueous organic or organic medium at 100-200‹ C. to modify the physical form. The pigments are used in spin dyeing and also to colour printing inks, lacquers, dispersion paints, rubbers, plastics materials and natural or synthetic resins and paper.

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