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    2.
    发明专利
    未知

    公开(公告)号：DE3872642D1

    公开(公告)日：1992-08-13

    申请号：DE3872642

    申请日：1988-09-30

    Applicant: HERBERTS GMBH ,  HOECHST AG

    Inventor： SAATWEBER DIETRICH DR ,  HENDRIKX GEORG DR ,  BRINDOEPKE GERHARD DR ,  PLUM HELMUT DR

    IPC: C09D5/44 ,  C09D163/00 ,  C09D175/04

    Abstract: A cathodically separable aq. electrodipping lacquer compsn. contains (A) a synthetic resin binder contg. amino gps., which can be made water-sol. or water-dispersible by protonisation with acids, and a cross-linking agent (B) reacting on baking, as well as opt. pigments, corrosion inhibitors, anti-crater agents, lacquer auxiliaries and binders, plasticisers, catalysts and organic solvents. (A) The component contains 90-50%, w.r.t. total resin binder, of a polycondensation, polymerisation and/or polyaddn. resin, with Mn 700-10,000, 1.2-21.7 x 10 power(23) lateral or terminal C=C bonds w.r.t. 1,000 g, corresp. to a hydrogenation iodine number of 5-90, opt. prim. and/or sec. OH gps., corresp. to OH number of 0-450 mg KOH/g resin, and tert. amino gps. corresp. to 30-450 mg KOH/g resin. (B) The component contains 10-50% of cpds. with methane tricarboxylic acid amide gps. of formula (I) with at least 2 gps. with active H, and derived from a reaction prod. of a mono- or poly-isocyanate and a malonic acid deriv., and contg. as further component (C) 0-10% of capped di- and/or poly-isocyanates.

    3.
    发明专利
    未知

    公开(公告)号：DE3602981A1

    公开(公告)日：1987-08-06

    申请号：DE3602981

    申请日：1986-01-31

    Applicant: HOECHST AG

    Inventor： WALZ GERD DR ,  PLUM HELMUT DR

    IPC: C07C69/52 ,  C08K5/16 ,  C08L5/00 ,  C08L101/00 ,  C09D5/44 ,  C09D163/00 ,  C08J3/24 ,  C08K5/00 ,  C25D13/04

    Abstract: Hardeners are described for synthetic resins which contain groups which are capable of ester or amide formation and, if appropriate, polymerizable double bonds. The new hardeners, which allow lower crosslinking temperatures, are products (A) of the Michael addition of compounds (B), containing Michael addition-capable ester groups, to compounds (C) which contain at least two Michael addition-capable double bonds, the products (A) having an average of at least one polymerization-capable double bond and at least two transesterification- or transamidation-capable ester groups per molecule and the compound (B) representing products of the reaction of (b1) CH-active alkyl esters and (b2) polyisocyanates.

    4.
    发明专利
    未知

    公开(公告)号：DE3229047A1

    公开(公告)日：1984-02-09

    申请号：DE3229047

    申请日：1982-08-04

    Applicant: HOECHST AG

    Inventor： PLUM HELMUT DR

    IPC: C08F8/00 ,  C08F8/12 ,  C08F8/44 ,  C08F20/00 ,  C08F20/34 ,  C08F20/36 ,  C08F22/00 ,  C08F22/22 ,  C08G18/83 ,  C09D133/04 ,  C09D157/06 ,  C09D3/80

    Abstract: Polymers that contain terminal amino groups and moieties of the formula (I) a process for preparing the polymers by (a) reacting in a first step a hydroxyl-containing ester of an alpha , beta -olefinically unsaturated monocarboxylic or dicarboxylic acid and a dihydric alcohol with a diisocyanate, the equivalence ratio of NCO to OH groups being greater than 1:1, (b) polymerizing the reaction product of (a) alone or in mixture with at least one olefinically unsaturated polymerizable monomer by free-radical polymerization, (c) decarboxylating the polymer into the ammonium salt, and then neutralizing the resulting product and their use in 2-component finishes that crosslink by means of crosslinking agents.

    5.
    发明专利
    未知

    公开(公告)号：DE3872826D1

    公开(公告)日：1992-08-20

    申请号：DE3872826

    申请日：1988-10-14

    Applicant: HOECHST AG

    Inventor： BRINDOEPKE GERHARD DR ,  PLUM HELMUT DR

    IPC: C08G18/32 ,  C08G18/30 ,  C08G18/34 ,  C08G18/38 ,  C08G18/50 ,  C08G18/62 ,  C08G18/64 ,  C08G18/80 ,  C09D5/44 ,  C09D175/00

    Abstract: Hardening component (I) for synthetic resins which form amide or ester gps. (II) comprises the reaction prod. of a polyisocyanate, a CH-acidic alkyl ester (III), a polyamine (VI) and possibly other NH- or OH-reactive cpds; (III) has the formula X-CHR2-COOR1 and (VI) is a polyoxy-alkylaneamine. In the formulae, X = COOR1, CN, CONH2, CONHR1, CO(NR1)2, COR1 or NO2; R1 = 1-8C alkyl and R2 = H or R1. Curable mixts. are claimed, comprising (I), binder (II) and possibly a diluent and additives. Polyisocyanate is pref. TDI or IPDI; X = COOR1 (with R1 = 1-6C alkyl) or CN, R2 = H; pref. (III) is dialkyl malonate or alkyl cyanoacetate; (IV) has the formula H2NCHR2CH2O-(CHR2O),-CH2CHR3 NH2 (IVa), H2NCHMeCH (OCHMeCH)m-(OCH2CH2)2-OCH2CHMeNH (VIb) or R1-(COCH2OH -NH) (VIc) with R2 = H or 1-6C alkyl; n = 1-50; m + p = 1-50 and m, p each = 1-49; R4 = trihyaric alcohol residu x, y, z = same as n, m or p); (II) has = M, 1000-30,000 and contains OH and/or amino gps.

    6.
    发明专利
    未知

    公开(公告)号：DE4032751A1

    公开(公告)日：1992-04-23

    申请号：DE4032751

    申请日：1990-10-16

    Applicant: HOECHST AG

    Inventor： BRINDOEPKE GERHARD DR ,  KUBILLUS UWE DR ,  PLUM HELMUT DR

    IPC: A47K3/28 ,  A47K3/30 ,  C08G59/14 ,  C08G59/16 ,  C08G59/40 ,  C08G59/50 ,  C08G59/62 ,  C09D163/00

    Abstract: A liquid coating composition is based on an acetoacetate group-containing polymer and a polyamine in the form of the corresponding aldimine or ketimine, where the acetoacetate group-containing polymer is obtained by reacting a polyepoxide with water, an amine, a hydroxycarboxylic acid and subsequently esterifying or transesterifying the final product using acetoacetic acid. This liquid coating composition is particularly suitable as a binder in two-component automobile repair fillers or as a two-component primer.

    7.
    发明专利
    未知

    公开(公告)号：DE3772782D1

    公开(公告)日：1991-10-17

    申请号：DE3772782

    申请日：1987-01-20

    Applicant: HOECHST AG

    Inventor： PLUM HELMUT DR

    IPC: C09D5/44

    Abstract: The compsns. (I), based on (A) resins contg. amino gps., or OH and amino gps. and gps. capable of forming ester and/or amide gsp. with carboxylic acids and (B) hardeners capable of transesterification and/or transamidation, are prepd. by 1) freeing (A) from solvent 2) diluting residue with water-soluble solvent of b.pt. below 100 deg.C 3) mixing diluted residue with (B) at temp. such that (A) and (B) do not react 4) at least partly neutralising the amino gps. with a water-soluble acid 5) diluting with water and 6) removing the organic solvent from the aq. dispersion under reduced pressure at moderately elevated temp. Pref. (A) is polymer of alpha, beta-unsatd. monomer contg. hydroxy- or amino-ester of olefinically unsatd. carboxylic acid, a polyaminopolyamide from dimerised fatty acid and a polyamine, or an aminopolyether-polyol from an epoxide resin and a prim. or sec. amine, Water-sol. solvent is lower alcohol or ketone, partic. MeOH, EtOH, iso-PrOH, acetone, or ethyl methyl ketone.

    9.
    发明专利
    未知

    公开(公告)号：DE3101887A1

    公开(公告)日：1982-09-02

    申请号：DE3101887

    申请日：1981-01-22

    Applicant: HOECHST AG

    Inventor： PLUM HELMUT DR

    IPC: C08F2/00 ,  C08F2/02 ,  C08F20/10 ,  C08F22/10 ,  C08F212/00 ,  C08F212/06 ,  C08F220/00 ,  C08F220/04 ,  C08F220/10 ,  C08F220/54 ,  C08F222/10 ,  C08F222/14 ,  C09D135/06

    Abstract: Process for preparing copolymers from esters of an unsaturated carboxylic acid with at least one other unsaturated monomer, characterized in that the following components are copolymerized in radical substance polymerization: (A) 5 to 60 parts by weight of at least one diester of an alpha , beta -olefinically unsaturated dicarboxylic acid having 1 to 8 carbon atoms in the ester group, (B) 10 to 70 parts by weight of at least one vinyl aromatic hydrocarbon having one vinyl group, (C) 0 to 30 parts by weight of at least one glycidyl ester of an aliphatic saturated monocarboxylic acid branched in the alpha -position, (D) 0 to 50 parts by weight of at least one ester, amide and/or anhydride of an alpha , beta -olefinically unsaturated mono- and/or dicarboxylic acid, (E) 0 to 40 parts by weight of at least one alpha , beta -olefinically unsaturated monocarboxylic acid, the sum of components (A) to (E) being 100 parts by weight, whilst at least a part of component (A) is at first introduced into the reaction vessel alone or in combination with at least a part of component (C) and a mixture of component (B) with at least one of components (D) and (E) and any remaining parts of components (A) and/or (C) is added in batches at 140 DEG to 200 DEG C. together with a radical initiator, alone or in conjunction with a regulator, and if component (C) is present, at least an equimolar quantity of component (E) is used; and the use of the products thus obtained as binders for the preparation of coating compositions.

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