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    Sizing agent for glass fibers
    1.
    发明授权
    Sizing agent for glass fibers 失效
    玻璃纤维施胶剂

    公开(公告)号：US3920596A

    公开(公告)日：1975-11-18

    申请号：US47844174

    申请日：1974-06-12

    Applicant: KAO CORP

    Inventor： FURUKAWA JUN-ICHI ,  KONO YOSHINAO

    IPC: C08L67/00 ,  C03C25/10 ,  C03C25/32 ,  C08J5/08 ,  C08L7/00 ,  C08L21/00 ,  C08L67/06 ,  D06M13/02 ,  D06M13/325 ,  D06M13/328 ,  D06M15/507 ,  D06M101/00 ,  C08L67/08

    CPC classification number: C03C25/323 ,  Y10S260/16 ,  Y10T428/2938 ,  Y10T428/2958 ,  Y10T428/2964 ,  Y10T442/2402

    Abstract: A sizing agent composition comprising a film-forming material, a lubricant for glass fibers, a coupling agent and an antistatic agent, in which the film-forming material is an oil-in-water type emulsion of an unsaturated polyester obtained by reacting under heating (a) 1 mole of a dibasic acid component containing at least 50 mole percent of fumaric acid or maleic anhydride and (b) 1 to 1.5 moles of a diol component containing at least 30 mole percent of an adduct of 2 to 10 moles of an alkylene oxide to bisphenol A, with (c) an emulsifier selected from an adduct of 5 to 200 moles of an alkylene oxide to castor oil, an adduct of 5 to 200 moles of an alkylene oxide to hydrogenated castor oil and a polyethyleneglycol having an average molecular weight of 1000 to 6000, the amount of said emulsifier (c) being 5 to 30 parts by weight per 100 parts by weight of the sum of the polyester starting materials (a) and (b), and incorporating the resulting unsaturated polyester into water, and that the antistatic agent is a triethanolamine salt of an oxyacid of a metal selected from the group consisting of titanium, antimony, molybdenum, vanadium, aluminum, zinc, tin, germanium, zirconium, tungsten, boron and tellurium.

    Abstract translation: 包含成膜材料，玻璃纤维用润滑剂，偶联剂和抗静电剂的施胶剂组合物，其中成膜材料是通过在加热下反应而获得的不饱和聚酯的水包油型乳液 （a）1摩尔含有至少50摩尔％的富马酸或马来酸酐的二元酸组分和（b）1至1.5摩尔含有至少30摩尔％的2-10摩尔的 环氧烷与双酚A，其中（c）选自5至200摩尔烯化氧与蓖麻油的加合物的乳化剂，5至200摩尔环氧烷烃与氢化蓖麻油的加合物和具有平均值的聚乙二醇 分子量为1000〜6000，所述乳化剂（c）的量相对于100重量份聚酯原料（a）和（b）的总和为5〜30重量份，并将得到的不饱和聚酯加入到 水，那个 抗静电剂是选自钛，锑，钼，钒，铝，锌，锡，锗，锆，钨，硼和碲的金属的含氧酸的三乙醇胺盐。

    Sizing agent for glass fibers
    2.
    发明授权
    Sizing agent for glass fibers 失效
    玻璃纤维施胶剂

    公开(公告)号：US3923708A

    公开(公告)日：1975-12-02

    申请号：US47843274

    申请日：1974-06-12

    Applicant: KAO CORP

    Inventor： FURUKAWA JUN-ICHI ,  KONO YOSHINAO

    IPC: C08L67/00 ,  C03C25/10 ,  C03C25/32 ,  C08J5/08 ,  C08L7/00 ,  C08L21/00 ,  C08L67/06 ,  D06M13/02 ,  D06M13/325 ,  D06M13/328 ,  D06M15/507 ,  D06M101/00 ,  C08L67/08

    CPC classification number: C03C25/323 ,  Y10S260/15 ,  Y10T428/2938 ,  Y10T428/2964 ,  Y10T442/2402

    Abstract: A sizing agent composition comprising a film-forming material, a lubricant for glass fibers, a coupling agent and an antistatic agent, in which the film-forming material is an oil-in-water type emulsion of an unsaturated polyester obtained by reacting under heating (a) 1 mole of a dibasic acid component containing at least 50 mole percent of fumaric acid or maleic anhydride and (b) 1 to 1.5 moles of a diol component containing at least 30 mole percent of an adduct of 2 to 10 mols of an alkylene oxide to bisphenol A, with (c) an emulsifier selected from an adduct of 5 to 200 moles of an alkylene oxide to castor oil, an adduct of 5 to 200 moles of an alkylene oxide to hydrogenated castor oil and a polyethyleneglycol having an average molecular weight of 1000 to 6000, the amount of said emulsifier (c) being 5 to 30 parts by weight per 100 parts by weight of the sum of the polyester starting materials (a) and (b), and incorporating the resulting unsaturated polyester into water, and that the antistatic agent is a compound having the formulae RSO3H.N(CH2CH2OH)3 or ROSO3H.N(CH2CH2OH)3 wherein R stands for alkyl having 8 to 20 carbon atoms or an univalent organic radical obtained from alkylbenzene, alkylnaphthalene, polyoxyethylene alkyl ether, polyoxyethylene alkylphenyl ether, naphthalene-formaldehyde condensate, dialkyl succinate or alkyldiphenyl oxide.

    Abstract translation: 包含成膜材料，玻璃纤维用润滑剂，偶联剂和抗静电剂的施胶剂组合物，其中成膜材料是通过在加热下反应而获得的不饱和聚酯的水包油型乳液 （a）1摩尔含有至少50摩尔％的富马酸或马来酸酐的二元酸组分和（b）1至1.5摩尔含有至少30摩尔％的2至10摩尔的加成物的二醇组分 环氧烷与双酚A，其中（c）选自5至200摩尔烯化氧与蓖麻油的加合物的乳化剂，5至200摩尔环氧烷烃与氢化蓖麻油的加合物和具有平均值的聚乙二醇 分子量为1000〜6000，所述乳化剂（c）的量相对于100重量份聚酯原料（a）和（b）的总和为5〜30重量份，并将得到的不饱和聚酯加入到 水，那个 他的抗静电剂是具有式RSO 3 HN（CH 2 CH 2 OH）3或ROSO 3 HN（CH 2 CH 2 OH）3的化合物，其中R代表具有8-20个碳原子的烷基或由烷基苯，烷基萘，聚氧乙烯烷基醚，聚氧乙烯 烷基苯基醚，萘 - 甲醛缩合物，琥珀酸二烷基酯或烷基二苯醚。

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