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    Sizing agent for glass fibers
    1.
    发明授权
    Sizing agent for glass fibers 失效
    玻璃纤维施胶剂

    公开(公告)号：US3920596A

    公开(公告)日：1975-11-18

    申请号：US47844174

    申请日：1974-06-12

    Applicant: KAO CORP

    Inventor： FURUKAWA JUN-ICHI ,  KONO YOSHINAO

    IPC: C08L67/00 ,  C03C25/10 ,  C03C25/32 ,  C08J5/08 ,  C08L7/00 ,  C08L21/00 ,  C08L67/06 ,  D06M13/02 ,  D06M13/325 ,  D06M13/328 ,  D06M15/507 ,  D06M101/00 ,  C08L67/08

    CPC classification number: C03C25/323 ,  Y10S260/16 ,  Y10T428/2938 ,  Y10T428/2958 ,  Y10T428/2964 ,  Y10T442/2402

    Abstract: A sizing agent composition comprising a film-forming material, a lubricant for glass fibers, a coupling agent and an antistatic agent, in which the film-forming material is an oil-in-water type emulsion of an unsaturated polyester obtained by reacting under heating (a) 1 mole of a dibasic acid component containing at least 50 mole percent of fumaric acid or maleic anhydride and (b) 1 to 1.5 moles of a diol component containing at least 30 mole percent of an adduct of 2 to 10 moles of an alkylene oxide to bisphenol A, with (c) an emulsifier selected from an adduct of 5 to 200 moles of an alkylene oxide to castor oil, an adduct of 5 to 200 moles of an alkylene oxide to hydrogenated castor oil and a polyethyleneglycol having an average molecular weight of 1000 to 6000, the amount of said emulsifier (c) being 5 to 30 parts by weight per 100 parts by weight of the sum of the polyester starting materials (a) and (b), and incorporating the resulting unsaturated polyester into water, and that the antistatic agent is a triethanolamine salt of an oxyacid of a metal selected from the group consisting of titanium, antimony, molybdenum, vanadium, aluminum, zinc, tin, germanium, zirconium, tungsten, boron and tellurium.

    Abstract translation: 包含成膜材料，玻璃纤维用润滑剂，偶联剂和抗静电剂的施胶剂组合物，其中成膜材料是通过在加热下反应而获得的不饱和聚酯的水包油型乳液 （a）1摩尔含有至少50摩尔％的富马酸或马来酸酐的二元酸组分和（b）1至1.5摩尔含有至少30摩尔％的2-10摩尔的 环氧烷与双酚A，其中（c）选自5至200摩尔烯化氧与蓖麻油的加合物的乳化剂，5至200摩尔环氧烷烃与氢化蓖麻油的加合物和具有平均值的聚乙二醇 分子量为1000〜6000，所述乳化剂（c）的量相对于100重量份聚酯原料（a）和（b）的总和为5〜30重量份，并将得到的不饱和聚酯加入到 水，那个 抗静电剂是选自钛，锑，钼，钒，铝，锌，锡，锗，锆，钨，硼和碲的金属的含氧酸的三乙醇胺盐。

    Sizing agent for glass fibers
    2.
    发明授权
    Sizing agent for glass fibers 失效
    玻璃纤维施胶剂

    公开(公告)号：US3923708A

    公开(公告)日：1975-12-02

    申请号：US47843274

    申请日：1974-06-12

    Applicant: KAO CORP

    Inventor： FURUKAWA JUN-ICHI ,  KONO YOSHINAO

    IPC: C08L67/00 ,  C03C25/10 ,  C03C25/32 ,  C08J5/08 ,  C08L7/00 ,  C08L21/00 ,  C08L67/06 ,  D06M13/02 ,  D06M13/325 ,  D06M13/328 ,  D06M15/507 ,  D06M101/00 ,  C08L67/08

    CPC classification number: C03C25/323 ,  Y10S260/15 ,  Y10T428/2938 ,  Y10T428/2964 ,  Y10T442/2402

    Abstract: A sizing agent composition comprising a film-forming material, a lubricant for glass fibers, a coupling agent and an antistatic agent, in which the film-forming material is an oil-in-water type emulsion of an unsaturated polyester obtained by reacting under heating (a) 1 mole of a dibasic acid component containing at least 50 mole percent of fumaric acid or maleic anhydride and (b) 1 to 1.5 moles of a diol component containing at least 30 mole percent of an adduct of 2 to 10 mols of an alkylene oxide to bisphenol A, with (c) an emulsifier selected from an adduct of 5 to 200 moles of an alkylene oxide to castor oil, an adduct of 5 to 200 moles of an alkylene oxide to hydrogenated castor oil and a polyethyleneglycol having an average molecular weight of 1000 to 6000, the amount of said emulsifier (c) being 5 to 30 parts by weight per 100 parts by weight of the sum of the polyester starting materials (a) and (b), and incorporating the resulting unsaturated polyester into water, and that the antistatic agent is a compound having the formulae RSO3H.N(CH2CH2OH)3 or ROSO3H.N(CH2CH2OH)3 wherein R stands for alkyl having 8 to 20 carbon atoms or an univalent organic radical obtained from alkylbenzene, alkylnaphthalene, polyoxyethylene alkyl ether, polyoxyethylene alkylphenyl ether, naphthalene-formaldehyde condensate, dialkyl succinate or alkyldiphenyl oxide.

    Abstract translation: 包含成膜材料，玻璃纤维用润滑剂，偶联剂和抗静电剂的施胶剂组合物，其中成膜材料是通过在加热下反应而获得的不饱和聚酯的水包油型乳液 （a）1摩尔含有至少50摩尔％的富马酸或马来酸酐的二元酸组分和（b）1至1.5摩尔含有至少30摩尔％的2至10摩尔的加成物的二醇组分 环氧烷与双酚A，其中（c）选自5至200摩尔烯化氧与蓖麻油的加合物的乳化剂，5至200摩尔环氧烷烃与氢化蓖麻油的加合物和具有平均值的聚乙二醇 分子量为1000〜6000，所述乳化剂（c）的量相对于100重量份聚酯原料（a）和（b）的总和为5〜30重量份，并将得到的不饱和聚酯加入到 水，那个 他的抗静电剂是具有式RSO 3 HN（CH 2 CH 2 OH）3或ROSO 3 HN（CH 2 CH 2 OH）3的化合物，其中R代表具有8-20个碳原子的烷基或由烷基苯，烷基萘，聚氧乙烯烷基醚，聚氧乙烯 烷基苯基醚，萘 - 甲醛缩合物，琥珀酸二烷基酯或烷基二苯醚。

    4.
    发明专利
    未知

    公开(公告)号：AT52908T

    公开(公告)日：1990-06-15

    申请号：AT84112727

    申请日：1984-10-22

    Applicant: KAO CORP

    Inventor： TAKEMA YOSHINORI ,  TSUSHIMA RIKIO ,  YASUDA YUTAKA ,  KONO YOSHINAO

    IPC: C08F16/00 ,  A61K8/00 ,  A61K8/02 ,  A61K8/04 ,  A61K8/72 ,  A61K8/81 ,  A61Q3/02 ,  A61Q19/00 ,  C08F16/02 ,  C08F216/06 ,  A61K7/00

    Abstract: A film-forming cosmetic composition useful as a facial pack, nail enamel, eye liner etc., which comprises a copolymer of vinyl alcohol and alkyl vinyl ether, being referred to simply as PVA/AVE, consisting of 98 to 80 mole% of vinyl alcohol monomer units and 2 to 20 mole% of linear or branched alkyl vinyl monomer units having from 1 to 6 carbon atoms.The molar ratio of the vinyl alcohol monomer units to the alkyl vinyl ether monomer units is in the range of from 95/5 to 85/15.The PVA/AVE according to the invention has no acetic groups with ester bonds in a molecule. Instead, there are alkyl or alkenyl groups having ether bonds which serve for steric hindrance for preventing gelation of an aqueous solution of such copolymer. From this reason, the PVA/AVE does not undergo any hydrolysis as time passes and is thus excellent in storage stability.

    5.
    发明专利
    未知

    公开(公告)号：DE2713535A1

    公开(公告)日：1977-10-27

    申请号：DE2713535

    申请日：1977-03-26

    Applicant: KAO CORP

    Inventor： TAKAMORI SHIGERU ,  YAMASHITA KAZUTAKA ,  KONO YOSHINAO

    IPC: C09D5/03 ,  C08G59/00 ,  C08G59/18 ,  C08L63/00 ,  C08L67/00 ,  C09D163/00 ,  C09D3/58

    Abstract: A thermosetting resin composition useful in a powder coating composition comprising a polyepoxy compound and a polycarboxylic acid obtained by reacting (1) one mole of a polycarboxylic acid obtained by reacting (i) one mole of a polyoxyalkylene ether of a dihydric phenol, with (ii) 1 to 4 moles of trimellitic acid or anhydride thereof, (2) from 0.1 to 0.5 moles of a diepoxy compound.

    METODO PARA PRODUCIR POLIMERO DE FOSFATO.
    7.
    发明专利
    METODO PARA PRODUCIR POLIMERO DE FOSFATO. 未知

    公开(公告)号：ES2356259T3

    公开(公告)日：2011-04-06

    申请号：ES06797751

    申请日：2006-09-04

    Applicant: KAO CORP

    Inventor： SHIMODA MASAAKI ,  KONO YOSHINAO ,  TANISHO YOSHIAKI ,  HAMAI TOSHIMASA ,  HAMADA DAISUKE ,  MORII YOSHIKAZU ,  NAKA YOSHIHITO

    IPC: C08F290/06 ,  C04B22/16 ,  C04B24/26 ,  C04B28/02 ,  C08F2/04

    Abstract: Método para producir un polímero a base de éster de ácido fosfórico, que comprende una etapa de mezclado de preparar una disolución mixta que comprende un monómero 1 representado por la siguiente fórmula (1), un monómero 2 representado por la siguiente fórmula (2), y un monómero 3 representado por la siguiente fórmula (3) y una etapa de copolimerización de copolimerizar el monómero 1, monómero 2 y monómero 3, en el que la etapa de mezclado es mezclar los monómeros 1, 2 y 3 a una temperatura de 10 a 50ºC, la etapa de copolimerización es copolimerizar los monómeros a pH 7 o inferior, en un disolvente de polimerización que tiene una concentración de oxígeno disuelto a 25ºC de 0,01 a 4,0 mg/kg, en presencia de un agente quelante de ácido fosfónico, la etapa de copolimerización se inicia en el plazo de 72 horas tras la etapa de mezclado y la temperatura de la disolución mixta se mantiene en el intervalo de 10 a 50ºC hasta que se inicia la etapa de copolimerización: **(Ver fórmula)** en la que R1 y R2 representan cada uno un átomo de hidrógeno o un grupo metilo; y R3 representa un átomo de hidrógeno o -COO(AO)nX [en el que AO representa un grupo oxialquileno o grupo oxiestireno que tiene de 2 a 4 átomos de carbono; n representa un número promedio de moles añadidos de AO, y es un número desde 3 hasta 200; y X representa un átomo de hidrógeno o un grupo alquilo que tiene de 1 a 18 átomos de carbono], **(Ver fórmula)** en la que R4 representa un átomo de hidrógeno o un grupo metilo; R5 representa un grupo alquileno que tiene de 2 a 12 átomos de carbono; m1 representa un número desde 1 hasta 30; y M representa un átomo de hidrógeno, un metal alcalino o un metal alcalinotérreo, y **(Ver fórmula)** en la que R6 y R8 representan cada uno un átomo de hidrógeno o un grupo metilo; R7 y R9 representan cada uno un grupo alquileno que tiene de 2 a 12 átomos de carbono; m2 y m3 representan cada uno un número desde 1 hasta 30; y M representa un átomo de hidrógeno, un metal alcalino o un metal alcalinotérreo.

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