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    METHOD FOR PRODUCING ω-HYDROXYCARBOXYLIC ACID ESTER
    1.
    发明专利
    METHOD FOR PRODUCING ω-HYDROXYCARBOXYLIC ACID ESTER 有权
    生产ω-羟基羧酸的方法

    公开(公告)号：JP2005154429A

    公开(公告)日：2005-06-16

    申请号：JP2004318898

    申请日：2004-11-02

    Applicant: Kao Corp ,  花王株式会社

    Inventor： AOKI TAKASHI ,  TSUJII YOSHIAKI

    IPC: C07C67/31 ,  C07B61/00 ,  C07C69/675

    Abstract: PROBLEM TO BE SOLVED: To provide a method for simply producing an ω-hydroxycarboxylic acid ester with high selectivity in a high yield, by using an easily available general-purpose copper-based catalyst and an ester interchange catalyst. SOLUTION: This method for producing the ω-hydroxycarboxylic acid ester comprises making the ester interchange catalyst coexist, when an α,ω-dicarboxylic acid diester is hydrogenated by using the copper-based catalyst. COPYRIGHT: (C)2005,JPO&NCIPI

    Abstract translation: 待解决的问题：通过使用容易获得的通用铜基催化剂和酯交换催化剂，提供以高产率高选择性简单地制备ω-羟基羧酸酯的方法。 解决方案：当通过使用铜基催化剂氢化α，ω-二羧酸二酯时，制备ω-羟基羧酸酯的方法包括使酯交换催化剂共存。 版权所有（C）2005，JPO＆NCIPI

    PREPARATION OF WATER-BASE INK
    2.
    发明专利
    PREPARATION OF WATER-BASE INK 失效

    公开(公告)号：JPH11209666A

    公开(公告)日：1999-08-03

    申请号：JP1230498

    申请日：1998-01-26

    Applicant: KAO CORP

    Inventor： WAKABAYASHI SHIGEMI ,  ISHII MASUKAME ,  SUZUKI SHOICHI ,  TSUJII YOSHIAKI

    IPC: C09D11/00 ,  C09D11/322 ,  C09D11/324 ,  C09D11/326 ,  C09D11/328 ,  C09D11/38

    Abstract: PROBLEM TO BE SOLVED: To obtain a water-base ink which does not gel even at high temps. by causing the surfaces of substantially water-insoluble fine particles to adsorb a polyalkylene glycol before or during mixing and dispersing a colorant, a dispersant, and the fine particles into a water-base medium. SOLUTION: The surface of at least one kind of fine particles selected from among particles of silcon oxide, titanium oxide, and aluminum oxide are caused to adsorb a polyalkylene glycol (e.g. polyethylene glycol) pref. having a wt. average mol.wt. of 2,000-20,000. After the fine particles are mixed and dispersed into the polyalkylene glycol to give a dispersion liquid contg. fine particles having adsorbed the polyalkylene glycol, a colorant (e.g. carbon black), a dispersant (e.g. a formaline condensate of a polynuclear arom. compd. sulfonate), and a water-soluble medium (e.g. diethylene glycol) are mixed and dispersed into the liquid, and the resultant colorant dispersion is further diluted with water to a specified concn., thus giving the objective water-base ink.

    INK FOR INK JET RECORDING
    3.
    发明专利
    INK FOR INK JET RECORDING 失效

    公开(公告)号：JPH10298478A

    公开(公告)日：1998-11-10

    申请号：JP11319897

    申请日：1997-04-30

    Applicant: KAO CORP

    Inventor： ISHII MASUKAME ,  TSUJII YOSHIAKI ,  SUZUKI SHOICHI ,  WAKABAYASHI SHIGEMI ,  SUZUKI ATSUSHI

    IPC: B41J2/01 ,  C09D11/02 ,  C09D11/033 ,  C09D11/037 ,  C09D11/322 ,  C09D11/324 ,  C09D11/326 ,  C09D11/328 ,  C09D11/38

    Abstract: PROBLEM TO BE SOLVED: To obtain an ink excellent in long-term storage stability and environmental stability by forming an ink comprising a water-insoluble or difficulty water-soluble colorant, a dispersant and a water-soluble medium, wherein the dispersant is a polymeric dispersant obtained by condensing a sulfonate of aromatic compound mixture containing polynuclear aromatic compounds with formalin and neutralizing the condensate. SOLUTION: The polynuclear aromatic compounds used are desirably anthracene, phenanthrene, pyrene, acenaphthene and fluorene. The mixing ratio is desirably such that the colorant, the polymeric dispersant and the aqueous medium account for 2-10 wt.%, 0.5-10 wt.% and 80-97.2 wt.%, respectively. The fluid may optionally contain microparticles having a means primary particle diameter of 5-600 m. It is also desirable that the fluid contains polyethylene glycol. It is also desirable that the fluid contains a surfactant selected among nonionic and anionic surfactants.

    INK FOR INK JET RECORDING
    4.
    发明专利
    INK FOR INK JET RECORDING 失效

    公开(公告)号：JPH10298477A

    公开(公告)日：1998-11-10

    申请号：JP11319697

    申请日：1997-04-30

    Applicant: KAO CORP

    Inventor： ISHII MASUKAME ,  TSUJII YOSHIAKI ,  SUZUKI SHOICHI ,  WAKABAYASHI SHIGEMI ,  SUZUKI ATSUSHI

    IPC: B41J2/01 ,  C09D11/02 ,  C09D11/033 ,  C09D11/037 ,  C09D11/322 ,  C09D11/326 ,  C09D11/328 ,  C09D11/38

    Abstract: PROBLEM TO BE SOLVED: To obtain an ink excellent in long-term storage stability and environmental stability by forming an ink comprising a water-insoluble or difficultly water-soluble colorant, a dispersant and a water-soluble medium, wherein the dispersant is a polymeric dispersant obtained by condensing a sulfonate of aromatic compound mixture containing alkyl naphthalenes with formalin and neutrlizing the condensate. SOLUTION: The aromatic compound mixture contains aromatic compounds represented by the formula (wherein R1 and R2 are each H or a 1-5C alkyl). Compounds of the formula are desirably dimethylnaphthalene, methylnaphthalene and butylnaphthalene. The mixing ratio is desirably such that the colorant, the polymeric dispersant and the aqueous medium account for 2-10 wt.%, 0.8-10 wt.% and 80-97.2 wt.%, respectively. The fluid may optionally contain microparticles having a means primary particle diameter of 5-600 nm. It is also desirable that the fluid contains polyethylene glycol and a surfactant selected among nonionic and anionic surfactants.

    Method for producing 1,3-dioxane
    6.
    发明专利
    Method for producing 1,3-dioxane 有权
    生产1,3二氧化硅的方法

    公开(公告)号：JP2009196917A

    公开(公告)日：2009-09-03

    申请号：JP2008038964

    申请日：2008-02-20

    Applicant: Kao Corp ,  花王株式会社

    Inventor： KOTACHI SHINJI ,  TSUJII YOSHIAKI ,  NAGASAWA ATSUSHI

    IPC: C07D319/06

    Abstract: PROBLEM TO BE SOLVED: To provide a process for producing 1,3-dioxane which can efficiently produce 1,3-dioxane with high productivity in a high yield without using the generally used solvent and facilities for reflux and azeotropic dehydration.
    SOLUTION: The process for producing 1,3-dioxane represented by formula (3) (wherein R
    1 is a methyl group or a hydrocarbon group forming a six-membered ring by bonding to R
    2 ; R
    2 is a methyl group or a hydrocarbon group forming a six-membered ring by bonding to R
    1 ; R
    3 is hydrogen or a methyl group; R
    4 is a methyl group or an ethyl group; and R
    5 is a methyl group, an ethyl group, a propyl group, an isopropyl group, a butyl group or a sec-butyl group) comprises substantially reacting a mixture comprising an acid catalyst, an aldehyde compound, and a 1,3-diol compound without substantially removing the water formed during the reaction.
    COPYRIGHT: (C)2009,JPO&INPIT

    Abstract translation: 待解决的问题：提供一种能够以高产率高效率地生产1,3-二恶烷的1,3-二恶烷的制备方法，而不使用通常使用的溶剂和用于回流和共沸脱水的设备。 解决方案：由式（3）表示的1,3-二恶烷的制备方法（其中R 1 SP 1是通过与R 1键合而形成六元环的甲基或烃基， SP> 2 ; R 2 是通过键合到R 1和R 3上的形成六元环的甲基或烃基; / SP>是氢或甲基; R 4是甲基或乙基; R 5是甲基，乙基，丙基 ，异丙基，丁基或仲丁基）包括基本上使包含酸催化剂，醛化合物和1,3-二醇化合物的混合物基本上反应，而基本上不除去反应期间形成的水。 版权所有（C）2009，JPO＆INPIT

    AQUEOUS PIGMENT INK
    8.
    发明专利
    AQUEOUS PIGMENT INK 失效

    公开(公告)号：JPH1053741A

    公开(公告)日：1998-02-24

    申请号：JP21141096

    申请日：1996-08-09

    Applicant: KAO CORP

    Inventor： WAKABAYASHI SHIGEMI ,  ISHII MASUKAME ,  SAKUMA TADASHI ,  YANAGI HIDEKI ,  SUZUKI SHOICHI ,  TSUJII YOSHIAKI ,  AIDA KENJI

    IPC: C09D11/00 ,  C09D11/02 ,  C09D11/023 ,  C09D11/033 ,  C09D11/037 ,  C09D11/10 ,  C09D11/102 ,  C09D11/106 ,  C09D11/107 ,  C09D11/108 ,  C09D11/322 ,  C09D11/324 ,  C09D11/326 ,  C09D11/38

    Abstract: PROBLEM TO BE SOLVED: To provide an aqueous pigment ink suitable for use in ink-jet recording which is excellent in the dispersion stability of a pigment contained therein, by incorporating a specific alkylene glycol derivative in a mixture of a pigment, a polymer-dispersing agent, a water-soluble solvent and water. SOLUTION: This ink is an aqueous pigment ink comprising a pigment, (A) a polymer-dispersing agent, (B) 0.01 to 3wt.% of a compound represented by formula I, wherein AO is a 2-3C oxyalkylene, n is an number of 6 to 80 and XY is H or a sulfonic acid (sulfonate) group, a water-soluble solvent and water. (B) is preferably polyethylene glycol, polypropylene glycol or a polyethylene glycol disulfate, especially preferably a polyethylene glycol having a molecular weight of 400 to 2,000. Though various dispersing agents may be usable as (A), it is especially preferred that (A) is a (meth)acrylic acid derivative which is a copolymer derived from a compound of formula II, wherein each of R1 and R2 is H or a lower alkyl, m is a number of 0 to 2, n is a number of 1 to 300, X is H or a lower alkyl and AO is as defined above, and a compound of formula III, wherein each of R3 , R4 and R5 is H, a lower alkyl or the like, each of M1 and M2 is H, an alkali metal or the like and m1 is a number of 0 to 2.

    INK FOR INK JET RECORDING
    9.
    发明专利
    INK FOR INK JET RECORDING 失效

    公开(公告)号：JPH1053739A

    公开(公告)日：1998-02-24

    申请号：JP21291796

    申请日：1996-08-12

    Applicant: KAO CORP

    Inventor： YANAGI HIDEKI ,  ISHII MASUKAME ,  SAKUMA TADASHI ,  SUZUKI SHOICHI ,  WAKABAYASHI SHIGEMI ,  TSUJII YOSHIAKI ,  AIDA KENJI

    IPC: C09D11/00 ,  C09D11/02 ,  C09D11/033 ,  C09D11/037 ,  C09D11/10 ,  C09D11/102 ,  C09D11/106 ,  C09D11/107 ,  C09D11/108 ,  C09D11/322 ,  C09D11/324 ,  C09D11/326 ,  C09D11/328 ,  C09D11/38

    Abstract: PROBLEM TO BE SOLVED: To obtain an ink for ink jet recording which shows improved frequency response under high-frequency drive conditions by mixing a colorant with a specified water-soluble resin, a surfactant, a water-soluble solvent and water. SOLUTION: A monomer represented by formula I (wherein R1 and R2 are each H or a lower alkyl; m1 is 0-2; AO is a 2 or 3C oxyalkylene; n is 1-300; and X is H or a lower alkyl) is copolymerized with a monomer represented by formula II [wherein R3 to R5 are each H, a lower alkyl or (CH2 )m2 CM2 ; M1 and M2 are each an alkali (alkaline earth) metal, ammonium or an amine; and m2 is 0-2] or its anhydride in a molar ratio of 0.1/100 to 100/100 to obtain a water-soluble resin comprising a copolymer having a weight-average molecular weight of 5,000-200,000. 0.3-10wt.% colorant is mixed with 0.1-10wt.% above water-soluble resin, 0.01-5wt.% anionic surfactant, 0.1-30wt.% water-soluble solvent and 70-98wt.% water to obtain an ink having foam stability after 5min (Ross-Miles tert) of 5-50mm, a surface tension (at 25 deg.C) of 30-60dyn/cm and a viscosity of 0.3-30cP.

    WATER-BASED PIGMENT INK
    10.
    发明专利
    WATER-BASED PIGMENT INK 失效

    公开(公告)号：JPH1046083A

    公开(公告)日：1998-02-17

    申请号：JP21026396

    申请日：1996-08-08

    Applicant: KAO CORP

    Inventor： SAKUMA TADASHI ,  ISHII MASUKAME ,  YANAGI HIDEKI ,  SUZUKI SHOICHI ,  WAKABAYASHI SHIGEMI ,  TSUJII YOSHIAKI ,  AIDA KENJI

    IPC: C09D11/00 ,  C09D11/033 ,  C09D11/037 ,  C09D11/10 ,  C09D11/102 ,  C09D11/106 ,  C09D11/107 ,  C09D11/108 ,  C09D11/322 ,  C09D11/324 ,  C09D11/326 ,  C09D11/38

    Abstract: PROBLEM TO BE SOLVED: To obtain the subject ink high in print denseness, excellent in long- term dispersion stability, and useful for ink jet printing use, comprising a pigment, a dispersant such as an alkylene oxide-added monomer-contg. copolymer, a water-soluble solvent and water. SOLUTION: This water-based pigment ink high in print denseness and excellent in dispersibility under long-term storage, comprises (A) a pigment (e.g. carbon black), (B) a high molecular dispersant consisting of a copolymer of 5,000-200,000 in weight-average molecular weight prepared by copolymerization between 10-50 pts.wt. of an alkylene oxide-added monomer of formula I [X is H, methyl, a group of formula II (R is a 2-3C alkylene; R is H or a 1-3C alkyl: (n) is an integer of 1-300) or a group of formula III ((p) and (q) are each an integer of 1-300); Y is a group of formula IV or formula V] and 50-10 pts.wt. of a 2nd monomer copolymerizable with the 1st monomer, or a copolymer formed by neutralizing the above copolymer, (C) a water-soluble solvent (e.g. diethylene glycol), and (D) water.

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