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    PRODUCTION OF FATTY ACID ESTER, AND PRODUCTION OF SOAP USING THE FATTY ACID ESTER
    7.
    发明专利
    PRODUCTION OF FATTY ACID ESTER, AND PRODUCTION OF SOAP USING THE FATTY ACID ESTER 失效

    公开(公告)号：JPH0641578A

    公开(公告)日：1994-02-15

    申请号：JP19507592

    申请日：1992-07-22

    Applicant: KAO CORP

    Inventor： MATSUMURA YOSHIHISA ,  DOBASHI KIYOSHI

    IPC: C07C67/03 ,  C11B3/12 ,  C11C3/10 ,  C11C3/12 ,  C11D9/02 ,  C11D13/00

    Abstract: PURPOSE:To obtain the fatty acid ester giving soaps extremely good in their smells by ester-exchanging palm oil, etc., with a lower alcohol, hydrogenating the product, and subsequently distilling to obtain the fraction. CONSTITUTION:For example, palm oil, palm nuclear oil or their mixture is ester-exchanged with a lover alcohol to produce a palm oil fatty acid lower alcohol ester, a palm oil nuclear fatty acid lower alcohol ester or their mixture. The ester or ester mixture is hydrogenated in the presence of a hydrogenation catalyst to reduce the linolic acid ester content of the ester in an amount of 10wt.% or more based on the linolic acid content of the non-hydrogenated ester, followed by distilling the hydrogenation product to provide a fraction for the objective ester.

    METHOD AND APPARATUS FOR PREPARATION OF SOAP
    8.
    发明专利
    METHOD AND APPARATUS FOR PREPARATION OF SOAP 失效

    公开(公告)号：JPH03265696A

    公开(公告)日：1991-11-26

    申请号：JP6572690

    申请日：1990-03-16

    Applicant: KAO CORP

    Inventor： UESUNA AKIHIKO ,  MATSUMURA YOSHIHISA ,  DOBASHI KIYOSHI ,  SHIMOJIYOU YOSHIO

    IPC: C11D13/04

    Abstract: PURPOSE:To improve the rate of reaction and to make an apparatus for preparing soap compact in size by adding a monoglyceride and/or a diglyceride to a reaction mixture in the saponification step in the production of soap by ester saponification. CONSTITUTION:A monoglyceride and/or a diglyceride is added to a reaction mixture in the saponification step in the production of soap by saponification of fatty acid/lower alcohol esters. It is preferable to add 1-20wt.% monoglyceride and/or diglyceride to the esters. The esters used are those of a 1-5C alcohol with a fatty acid having an 8-24C alkyl or alkenyl group. Any glycerides derived from long-chain fatty acids may be used for the above glycerides. However, those monoglycerides and diglycerides which have fatty acid compositions corresponding to the fatty acid/lower alcohol esters as the raw material of soap are preferable in terms of physical properties of the soap to be obtained.

    Novel 2-(alpha-substituted alkyl)-2-imidazoline and its preparation
    9.
    发明专利
    Novel 2-(alpha-substituted alkyl)-2-imidazoline and its preparation 失效
    新2-（ALPHA-取代的烷基）-2-咪唑啉及其制备

    公开(公告)号：JPS5781468A

    公开(公告)日：1982-05-21

    申请号：JP15783880

    申请日：1980-11-10

    Applicant: Kao Corp

    Inventor： YASUDA YUTAKA ,  DOBASHI KIYOSHI ,  NISHIMURA TOSHIROU

    IPC: C07D233/22 ,  B01F17/32 ,  C07D233/26 ,  C08K5/3445

    CPC classification number: C08K5/3445 ,  C07D233/26

    Abstract: NEW MATERIAL:2-(α-Substituted alkyl)-2-imidazoline of formulaI(R
    1 is 6W 20C alkyl, alkenyl; R
    2 is 1W4C alkyl).
    EXAMPLE: 1-(2-Hydroxyethyl)-2-(α-methoxycarbonylethylundecyl)-2-imidazoline.
    USE: Synthetic intermediate of amphoteric surfactant: the amphoteric surfactant is less colored, when stored at high temperature.
    PREPARATION: An acrylic ester of CH
    2 =CH-CO
    2 R is made to act on an imidazoline of formula II under substantially anhydrous conditions.
    COPYRIGHT: (C)1982,JPO&Japio

    Abstract translation: 新材料：式Ⅰ的2-（α-取代烷基）-2-咪唑啉（R1为6-20C烷基，烯基; R2为1-4C烷基）。 实施例：1-（2-羟乙基）-2-（α-甲氧基羰基乙基十一烷基）-2-亚氨基二唑啉。 用途：两性表面活性剂的合成中间体：两性表面活性剂在高温储存时颜色较少。 制备：使CH 2 = CH-CO 2 R的丙烯酸酯在基本无水的条件下作用于式II的咪唑啉。

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