公开(公告)号：WO0152976A9

公开(公告)日：2002-10-24

申请号：PCT/US0101939

申请日：2001-01-22

Applicant: LUBRIZOL CORP

Inventor： FILIPPINI BRIAN B ,  LANGE RICHARD M ,  GRISSO BRYAN A ,  HIRD BRYN

IPC: B01F17/52 ,  B01F17/00 ,  C05G3/00 ,  C05G5/00 ,  C06B47/00 ,  C06B47/14 ,  C10L1/32 ,  C10M129/74 ,  C10M129/76 ,  C10M129/95 ,  C10M133/04 ,  C10M133/16 ,  C10M133/56 ,  C10M159/12 ,  C10M173/00 ,  C10N30/04 ,  C10N40/08 ,  C10N40/20 ,  C10N40/22 ,  A01N25/04 ,  A01N25/30 ,  C05G3/06 ,  C06B23/00 ,  E21B43/27

CPC classification number: C10L1/328 ,  B01F17/0021 ,  B01F17/0028 ,  B01F17/0042 ,  B01F17/005 ,  C06B47/145

Abstract: The disclosed invention relates to a composition comprising a partially dehydrated product made by: (I) reacting (A) a hydrocarbyl substituted succinic acid or anhydride with (B) a polyol, a polyamine, a hydroxyamine, or a mixture of two or more thereof, to form a first intermediate product comprising: an ester, partial ester or mixture thereof when (B) is a polyol; an amide, imide, salt, amide/salt, partial amide or mixture of two or more thereof when (B) is a polyamine; or an ester, partial ester, amide, partial amide, amide/salt, imide, ester/salt, salt or a mixture of two or more thereof when (B) is a hydroxyamine, a mixture of a polyol and a polyamine, a mixture of a polyol and a hydroxyamine, or a mixture of a polyamine and a hydroxyamine, or a mixture of a polyol, a polyamine and a hydroxyamine; the hydrocarbyl substituent of said acid or anhydride having an average of about 8 to about 200 carbon atoms; and (II) heating said first intermediate product at an effective temperature to form a second intermediate product with water of reaction being formed, and separating a portion of said water of reaction from said second intermediate product, when (A) is said succinic anhydride the amount of water of reaction that is separated is from about 0.2 to about 0.9 equivalents of said water of reaction per equivalent of said succinic anhydride, when (A) is said succinic acid the amount of water of reaction that is separated is from about 1.2 to about 1.9 moles of said water of reaction per equivalent of said succinic acid, said partially dehydrated product having a total acid number in the range of about 20 to about 100 mg of KOH/g.

Abstract translation: 所公开的发明涉及包含部分脱水产物的组合物，其通过以下步骤制备：（I）使（A）烃基取代的琥珀酸或酸酐与（B）多元醇，多胺，羟胺或其两种或更多种的混合物 形成第一中间产物，其包含：（B）为多元醇时的酯，偏酯或其混合物; 当（B）是多胺时，酰胺，酰亚胺，盐，酰胺/盐，部分酰胺或其两种或更多种的混合物; 或（B）为羟基胺，多元醇和多胺的混合物，混合物或其混合物时，可以使用酯，酯，酯，酰胺，部分酰胺，酰胺/盐，酰亚胺，酯/盐，盐或其两种或多种的混合物 的多元醇和羟胺，或多胺和羟胺的混合物，或多元醇，多胺和羟胺的混合物; 所述酸或酸酐的烃基取代基具有约8至约200个碳原子的平均值; 和（II）在有效温度下加热所述第一中间产物以形成具有反应水的第二中间产物，并且当（A）是所述琥珀酸酐时，将所述反应水的一部分与所述第二中间产物分离 当（A）是所述琥珀酸时，分离的反应水的量为约0.2至约0.9当量的所述反应水反应当量的所述琥珀酸酐时，分离的反应水的量为约1.2至 每当量所述琥珀酸约1.9摩尔所述反应水，所述部分脱水产物的总酸值在约20至约100mg KOH / g的范围内。

公开(公告)号：CA2398108C

公开(公告)日：2008-12-23

申请号：CA2398108

申请日：2001-01-22

Applicant: LUBRIZOL CORP

Inventor： GRISSO BRYAN A ,  HIRD BRYN ,  LANGE RICHARD M ,  FILIPPINI BRIAN B

IPC: C09K23/52 ,  C05G3/00 ,  C05G3/70 ,  C05G5/00 ,  C06B23/00 ,  C06B47/00 ,  C06B47/14 ,  C09K23/00 ,  C10L1/32 ,  C10M129/74 ,  C10M129/76 ,  C10M129/95 ,  C10M133/04 ,  C10M133/16 ,  C10M133/56 ,  C10M159/12 ,  C10M173/00 ,  C10N30/04 ,  C10N40/08 ,  C10N40/20 ,  C10N40/22

Abstract: An emulsifier composition comprising a partially deyhdrated product made by: (I) reacting (A) a hydrocarbyl substituted succinic acid or anhydride wi th (B) a polyol, a polyamine, a hydroxyamine, or a mixture of two or more thereof, to form a first intermediate product comprising: an ester, partial ester or mixture thereof when (B) is a polyol; an amide, imide, salt, amide/salt, partial ami de or mixture when (B) is a polyamine; or an ester, partial ester, amide, partial amide, amide/salt, imide, ester/salt, salt or a mixture when (B) is a hydroxyamine, a mixture of a polyol and a polyamine, a mixture of a polyol and a hydroxyamin e, or a mixture of a polyamine and a hydroxyamine, or a mixture of a polyol, a polyamine and a hydroxyamine; the hydrocarbyl substituent of the acid or anhydride having an average of about 8 to about 200 carbon atoms; and (II) heating the first intermediate product to form a second intermediate product with water of reaction being formed, and separating a portion of the water of reaction from the second intermediate product, when (A) is the succinic anhydride the amount of water of reaction that is separated is from about 0.2 to about 0.9 equivalents of said water of reaction per equivalent of the succinic anhydride, when (A) is one succinic acid the amountof water of reaction that is separated is from about 1.2 to about 1.9 moles of said water of reaction per equivalent o f the succinic acid, the partially dehydrated product having a total acid number i n the range of about 20 to about 100 mg of KOH/g. The emulsifier composition can b e used for making emulsions, for example explosive emulsions, emulsion fertilizers, water-blended fuels and lubricants.

公开(公告)号：AU782124B2

公开(公告)日：2005-07-07

申请号：AU3449701

申请日：2001-01-22

Applicant: LUBRIZOL CORP

Inventor： FILIPPINI BRIAN B ,  LANGE RICHARD M ,  GRISSO BRYAN A ,  HIRD BRYN

IPC: C09K23/52 ,  C05G3/00 ,  C05G3/70 ,  C05G5/00 ,  C06B47/00 ,  C06B47/14 ,  C09K23/00 ,  C10L1/32 ,  C10M129/74 ,  C10M129/76 ,  C10M129/95 ,  C10M133/04 ,  C10M133/16 ,  C10M133/56 ,  C10M159/12 ,  C10M173/00 ,  C10N30/04 ,  C10N40/08 ,  C10N40/20 ,  C10N40/22 ,  B01F17/00

Abstract: The disclosed invention relates to a composition comprising a partially dehydrated product made by: (I) reacting (A) a hydrocarbyl substituted succinic acid or anhydride with (B) a polyol, a polyamine, a hydroxyamine, or a mixture of two or more thereof, to form a first intermediate product comprising: an ester, partial ester or mixture thereof when (B) is a polyol; an amide, imide, salt, amide/salt, partial amide or mixture of two or more thereof when (B) is a polyamine; or an ester, partial ester, amide, partial amide, amide/salt, imide, ester/salt, salt or a mixture of two or more thereof when (B) is a hydroxyamine, a mixture of a polyol and a polyamine, a mixture of a polyol and a hydroxyamine, a mixture of a polyamine and a hydroxyamine, or a mixture of a polyol, a polyamine and a hydroxyamine; the hydrocarbyl substituent of said acid or anhydride having an average of about 8 to about 200 carbon atoms; and (II) heating said first intermediate product at an effective temperature to form a second intermediate product with water of reaction being formed, and separating a portion of said water of reaction from said second intermediate product, when (A) is said succinic anhydride the amount of water of reaction that is separated is from about 0.2 to about 0.9 equivalents of said water of reaction per equivalent of said succinic anhydride, when (A) is said succinic acid the amount of water of reaction that is separated is from about 1.2 to about 1.9 moles of said water of reaction per equivalent of said succinic acid, said partially dehydrated product having a total acid number in the range of about 20 to about 100 mg of KOH/g. A process for making the foregoing partially dehydrated product is also disclosed. Emulsions comprising an organic phase, an aqueous phase, and an emulsifying amount of the foregoing partially dehydrated product are disclosed.

公开(公告)号：DE60110044T2

公开(公告)日：2006-01-26

申请号：DE60110044

申请日：2001-01-22

Applicant: LUBRIZOL CORP

Inventor： FILIPPINI B ,  LANGE M ,  GRISSO A ,  HIRD BRYN

IPC: C09K23/52 ,  C05G3/00 ,  C05G3/70 ,  C05G5/00 ,  C06B47/00 ,  C06B47/14 ,  C09K23/00 ,  C10L1/32 ,  C10M129/74 ,  C10M129/76 ,  C10M129/95 ,  C10M133/04 ,  C10M133/16 ,  C10M133/56 ,  C10M159/12 ,  C10M173/00 ,  C10N30/04 ,  C10N40/08 ,  C10N40/20 ,  C10N40/22

Abstract: The disclosed invention relates to a composition comprising a partially dehydrated product made by: (I) reacting (A) a hydrocarbyl substituted succinic acid or anhydride with (B) a polyol, a polyamine, a hydroxyamine, or a mixture of two or more thereof, to form a first intermediate product comprising: an ester, partial ester or mixture thereof when (B) is a polyol; an amide, imide, salt, amide/salt, partial amide or mixture of two or more thereof when (B) is a polyamine; or an ester, partial ester, amide, partial amide, amide/salt, imide, ester/salt, salt or a mixture of two or more thereof when (B) is a hydroxyamine, a mixture of a polyol and a polyamine, a mixture of a polyol and a hydroxyamine, a mixture of a polyamine and a hydroxyamine, or a mixture of a polyol, a polyamine and a hydroxyamine; the hydrocarbyl substituent of said acid or anhydride having an average of about 8 to about 200 carbon atoms; and (II) heating said first intermediate product at an effective temperature to form a second intermediate product with water of reaction being formed, and separating a portion of said water of reaction from said second intermediate product, when (A) is said succinic anhydride the amount of water of reaction that is separated is from about 0.2 to about 0.9 equivalents of said water of reaction per equivalent of said succinic anhydride, when (A) is said succinic acid the amount of water of reaction that is separated is from about 1.2 to about 1.9 moles of said water of reaction per equivalent of said succinic acid, said partially dehydrated product having a total acid number in the range of about 20 to about 100 mg of KOH/g. A process for making the foregoing partially dehydrated product is also disclosed. Emulsions comprising an organic phase, an aqueous phase, and an emulsifying amount of the foregoing partially dehydrated product are disclosed.

公开(公告)号：DE60110044D1

公开(公告)日：2005-05-19

申请号：DE60110044

申请日：2001-01-22

Applicant: LUBRIZOL CORP

Inventor： FILIPPINI B ,  LANGE M ,  GRISSO A ,  HIRD BRYN

IPC: C09K23/52 ,  C05G3/00 ,  C05G3/70 ,  C05G5/00 ,  C06B47/00 ,  C06B47/14 ,  C09K23/00 ,  C10L1/32 ,  C10M129/74 ,  C10M129/76 ,  C10M129/95 ,  C10M133/04 ,  C10M133/16 ,  C10M133/56 ,  C10M159/12 ,  C10M173/00 ,  C10N30/04 ,  C10N40/08 ,  C10N40/20 ,  C10N40/22 ,  B01F17/00

Abstract: The disclosed invention relates to a composition comprising a partially dehydrated product made by: (I) reacting (A) a hydrocarbyl substituted succinic acid or anhydride with (B) a polyol, a polyamine, a hydroxyamine, or a mixture of two or more thereof, to form a first intermediate product comprising: an ester, partial ester or mixture thereof when (B) is a polyol; an amide, imide, salt, amide/salt, partial amide or mixture of two or more thereof when (B) is a polyamine; or an ester, partial ester, amide, partial amide, amide/salt, imide, ester/salt, salt or a mixture of two or more thereof when (B) is a hydroxyamine, a mixture of a polyol and a polyamine, a mixture of a polyol and a hydroxyamine, a mixture of a polyamine and a hydroxyamine, or a mixture of a polyol, a polyamine and a hydroxyamine; the hydrocarbyl substituent of said acid or anhydride having an average of about 8 to about 200 carbon atoms; and (II) heating said first intermediate product at an effective temperature to form a second intermediate product with water of reaction being formed, and separating a portion of said water of reaction from said second intermediate product, when (A) is said succinic anhydride the amount of water of reaction that is separated is from about 0.2 to about 0.9 equivalents of said water of reaction per equivalent of said succinic anhydride, when (A) is said succinic acid the amount of water of reaction that is separated is from about 1.2 to about 1.9 moles of said water of reaction per equivalent of said succinic acid, said partially dehydrated product having a total acid number in the range of about 20 to about 100 mg of KOH/g. A process for making the foregoing partially dehydrated product is also disclosed. Emulsions comprising an organic phase, an aqueous phase, and an emulsifying amount of the foregoing partially dehydrated product are disclosed.

公开(公告)号：AU3449701A

公开(公告)日：2001-07-31

申请号：AU3449701

申请日：2001-01-22

Applicant: LUBRIZOL CORP

Inventor： FILIPPINI BRIAN B ,  LANGE RICHARD M ,  GRISSO BRYAN A ,  HIRD BRYN

IPC: C05G3/00 ,  C05G3/70 ,  C05G5/00 ,  C06B47/00 ,  C06B47/14 ,  C10L1/32 ,  C10M129/74 ,  C10M129/76 ,  C10M129/95 ,  C10M133/04 ,  C10M133/16 ,  C10M133/56 ,  C10M159/12 ,  C10M173/00 ,  C10N30/04 ,  C10N40/08 ,  C10N40/20 ,  C10N40/22 ,  B01F17/00

Abstract: The disclosed invention relates to a composition comprising a partially dehydrated product made by: (I) reacting (A) a hydrocarbyl substituted succinic acid or anhydride with (B) a polyol, a polyamine, a hydroxyamine, or a mixture of two or more thereof, to form a first intermediate product comprising: an ester, partial ester or mixture thereof when (B) is a polyol; an amide, imide, salt, amide/salt, partial amide or mixture of two or more thereof when (B) is a polyamine; or an ester, partial ester, amide, partial amide, amide/salt, imide, ester/salt, salt or a mixture of two or more thereof when (B) is a hydroxyamine, a mixture of a polyol and a polyamine, a mixture of a polyol and a hydroxyamine, a mixture of a polyamine and a hydroxyamine, or a mixture of a polyol, a polyamine and a hydroxyamine; the hydrocarbyl substituent of said acid or anhydride having an average of about 8 to about 200 carbon atoms; and (II) heating said first intermediate product at an effective temperature to form a second intermediate product with water of reaction being formed, and separating a portion of said water of reaction from said second intermediate product, when (A) is said succinic anhydride the amount of water of reaction that is separated is from about 0.2 to about 0.9 equivalents of said water of reaction per equivalent of said succinic anhydride, when (A) is said succinic acid the amount of water of reaction that is separated is from about 1.2 to about 1.9 moles of said water of reaction per equivalent of said succinic acid, said partially dehydrated product having a total acid number in the range of about 20 to about 100 mg of KOH/g. A process for making the foregoing partially dehydrated product is also disclosed. Emulsions comprising an organic phase, an aqueous phase, and an emulsifying amount of the foregoing partially dehydrated product are disclosed.

公开(公告)号：CA2398108A1

公开(公告)日：2001-07-26

申请号：CA2398108

申请日：2001-01-22

Applicant: LUBRIZOL CORP

Inventor： HIRD BRYN ,  LANGE RICHARD M ,  GRISSO BRYAN A ,  FILIPPINI BRIAN B

IPC: C09K23/52 ,  C05G3/00 ,  C05G3/70 ,  C05G5/00 ,  C06B47/00 ,  C06B47/14 ,  C09K23/00 ,  C10L1/32 ,  C10M129/74 ,  C10M129/76 ,  C10M129/95 ,  C10M133/04 ,  C10M133/16 ,  C10M133/56 ,  C10M159/12 ,  C10M173/00 ,  C10N30/04 ,  C10N40/08 ,  C10N40/20 ,  C10N40/22 ,  B01F17/00 ,  C06B23/00 ,  A01N25/04 ,  C05G3/06 ,  E21B43/27 ,  A01N25/30

Abstract: The disclosed invention relates to a composition comprising a partially dehydrated product made by: (I) reacting (A) a hydrocarbyl substituted succinic acid or anhydride with (B) a polyol, a polyamine, a hydroxyamine, o r a mixture of two or more thereof, to form a first intermediate product comprising: an ester, partial ester or mixture thereof when (B) is a polyol; an amide, imide, salt, amide/salt, partial amide or mixture of two or more thereof when (B) is a polyamine; or an ester, partial ester, amide, partial amide, amide/salt, imide, ester/salt, salt or a mixture of two or more there of when (B) is a hydroxyamine, a mixture of a polyol and a polyamine, a mixture of a polyol and a hydroxyamine, or a mixture of a polyamine and a hydroxyamine, or a mixture of a polyol, a polyamine and a hydroxyamine; the hydrocarbyl substituent of said acid or anhydride having an average of about 8 to about 200 carbon atoms; and (II) heating said first intermediate product at an effective temperature to form a second intermediate product with water of reaction being formed, and separating a portion of said water of reaction fr om said second intermediate product, when (A) is said succinic anhydride the amount of water of reaction that is separated is from about 0.2 to about 0.9 equivalents of said water of reaction per equivalent of said succinic anhydride, when (A) is said succinic acid the amount of water of reaction th at is separated is from about 1.2 to about 1.9 moles of said water of reaction per equivalent of said succinic acid, said partially dehydrated product havi ng a total acid number in the range of about 20 to about 100 mg of KOH/g.