PRODUCTION OF PALLADIUM TETRAAMINE SULFATE

    公开(公告)号:JP2001026427A

    公开(公告)日:2001-01-30

    申请号:JP2000160159

    申请日:2000-05-30

    Abstract: PROBLEM TO BE SOLVED: To obtain a replenishing agent for electroplating bath, which is low in corrosive properties by distillating a palladium nitrate solution formed from palladium and an excess amount of a nitrate solution at a specified temp. and then adding palladium sulfate and ammonium hydroxide. SOLUTION: A palladium nitrate solution is prepared by washing a prescribed amount of metal palladium with HCl of about 40 to 60 deg.C to activate the palladium and bringing the palladium into contact with an excess amount of a nitrate solution. The nitrate solution is prepared using nitric acid and the nitrate solution is used preferably in the range of about 15 to 50 g/l. The palladium nitrate solution is distilled at a low temp. of

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