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    PROCESS FOR OBTAINING CYCLIC SULPHATS
    1.
    发明专利
    PROCESS FOR OBTAINING CYCLIC SULPHATS 未知

    公开(公告)号：YU47589A

    公开(公告)日：1990-10-31

    申请号：YU47589

    申请日：1989-03-07

    Applicant: RHONE POULENC SA

    Inventor： LE ROY P ,  MANDARD CAZIN B

    IPC: B01J23/46 ,  B01J27/13 ,  C07B61/00 ,  C07D327/10

    Abstract: Process for the preparation of cyclic sulphates of general formula (I) by oxidation of a cyclic sulphite of general formula (II) by means of an alkali metal or alkaline-earth metal hypohalite and of a catalytic quantity of a ruthenium derivative (RuO2, RuCl3). In the general formulae (I) and (II), R1, R2, R3, R4, R5 and R6, which are identical or different, denote hydrogen, halogen, alkyl, alkoxy, aryl, aryloxy or alkoxycarbonyl.

    6-TRICHLOROACETAMIDO-PENICILLANIC ACID DERIVATIVES AND THEIR PREPARATION
    2.
    发明专利
    6-TRICHLOROACETAMIDO-PENICILLANIC ACID DERIVATIVES AND THEIR PREPARATION 未知

    公开(公告)号：ZA745656B

    公开(公告)日：1975-10-29

    申请号：ZA745656

    申请日：1974-09-05

    Applicant: RHONE POULENC SA

    Inventor： BOUCHAUDON J ,  LE ROY P ,  MESSER M

    IPC: A61K31/43 ,  C07D499/00 ,  C07D499/04 ,  C07D499/46 ,  C07D499/48 ,  C07D499/58 ,  C07D501/10 ,  C07D

    Abstract: 1454587 6-Trichloroacetamido-penicillanic acid derivatives RHONE-POULENC SA 5 Sept 1974 [6 Sept 1973] 38881/74 Heading C2C The invention comprises compounds of the formula wherein R is an ester radical. They may be obtained by either oxidizing the S-atom of a compound of the formula to a sulphoxide group, with, e.g. H 2 O 2 , NaIO 4 or an organic per-acid; or reacting a compound of the formula wherein R 1 is PhCH 2 or PhOCH 2 , with or a derivative thereof. Compounds of Formula II may be obtained either by reacting a compound of the formula with Cl 3 CCOOH or a derivative thereof or by reacting an imino-chloride of the above compound with an alkali metal salt of Cl 3 CCOOH. Compounds of Formula III may be obtained either by oxidation of a compound of Formula IV or by esterification of a compound of the formula

    4.
    发明专利
    未知

    公开(公告)号：NO743200L

    公开(公告)日：1975-04-01

    申请号：NO743200

    申请日：1974-09-05

    Applicant: RHONE POULENC SA

    Inventor： BOUCHAUDON J ,  LE ROY P ,  MESSER M N

    IPC: C07D501/04 ,  A61K31/545 ,  C07D499/00 ,  C07D501/10 ,  C07D501/18 ,  C07D501/22 ,  C07D

    Abstract: 1454588 7-Chloroacetamido-3-desacetoxycephalosporanic acid derivatives RHONEPOULENC SA 5 Sept 1974 [6 Sept 1973] 38882/74 Heading C2C The invention comprises compounds of the formula wherein R is an ester radical, e.g. C 1 -C 4 alkyl or benzyl which may be substituted by C 1 -C 4 alkoxy. They may be obtained by (a) heating a compound of the formula in an anhydrous acid medium, or (b) treating a compound of the formula with Zn in acetic acid. 7 - Amino - 3 - desacetoxy - cephalosporanic acid is obtained by hydrolysis or hydrogenolysis of a compound of Formula I to give a compound of the formula and treating this compound with thiourea in aqueous solution.

    6.
    发明专利
    未知

    公开(公告)号：NO743197L

    公开(公告)日：1975-04-01

    申请号：NO743197

    申请日：1974-09-05

    Applicant: RHONE POULENC SA

    Inventor： BOUCHAUDON J ,  LE ROY P ,  MESSER M N

    IPC: A61K31/43 ,  C07D499/00 ,  C07D499/04 ,  C07D499/46 ,  C07D499/48 ,  C07D499/58 ,  C07D501/10 ,  C07D

    Abstract: 1454587 6-Trichloroacetamido-penicillanic acid derivatives RHONE-POULENC SA 5 Sept 1974 [6 Sept 1973] 38881/74 Heading C2C The invention comprises compounds of the formula wherein R is an ester radical. They may be obtained by either oxidizing the S-atom of a compound of the formula to a sulphoxide group, with, e.g. H 2 O 2 , NaIO 4 or an organic per-acid; or reacting a compound of the formula wherein R 1 is PhCH 2 or PhOCH 2 , with or a derivative thereof. Compounds of Formula II may be obtained either by reacting a compound of the formula with Cl 3 CCOOH or a derivative thereof or by reacting an imino-chloride of the above compound with an alkali metal salt of Cl 3 CCOOH. Compounds of Formula III may be obtained either by oxidation of a compound of Formula IV or by esterification of a compound of the formula

    7.
    发明专利
    未知

    公开(公告)号：SE7411228L

    公开(公告)日：1975-03-07

    申请号：SE7411228

    申请日：1974-09-05

    Applicant: RHONE POULENC SA

    Inventor： BOUCHAUDON J ,  LE ROY P ,  MESSER M N

    IPC: C07D501/04 ,  A61K31/545 ,  C07D499/00 ,  C07D501/10 ,  C07D501/18 ,  C07D501/22 ,  C07D99/24

    Abstract: 1454588 7-Chloroacetamido-3-desacetoxycephalosporanic acid derivatives RHONEPOULENC SA 5 Sept 1974 [6 Sept 1973] 38882/74 Heading C2C The invention comprises compounds of the formula wherein R is an ester radical, e.g. C 1 -C 4 alkyl or benzyl which may be substituted by C 1 -C 4 alkoxy. They may be obtained by (a) heating a compound of the formula in an anhydrous acid medium, or (b) treating a compound of the formula with Zn in acetic acid. 7 - Amino - 3 - desacetoxy - cephalosporanic acid is obtained by hydrolysis or hydrogenolysis of a compound of Formula I to give a compound of the formula and treating this compound with thiourea in aqueous solution.

    9.
    发明专利
    未知

    公开(公告)号：SE7411225L

    公开(公告)日：1975-03-07

    申请号：SE7411225

    申请日：1974-09-05

    Applicant: RHONE POULENC SA

    Inventor： BOUCHADON J ,  LE ROY P ,  MESSER M N

    IPC: A61K31/43 ,  C07D499/00 ,  C07D499/04 ,  C07D499/46 ,  C07D499/48 ,  C07D499/58 ,  C07D501/10 ,  C07D99/22

    Abstract: 1454587 6-Trichloroacetamido-penicillanic acid derivatives RHONE-POULENC SA 5 Sept 1974 [6 Sept 1973] 38881/74 Heading C2C The invention comprises compounds of the formula wherein R is an ester radical. They may be obtained by either oxidizing the S-atom of a compound of the formula to a sulphoxide group, with, e.g. H 2 O 2 , NaIO 4 or an organic per-acid; or reacting a compound of the formula wherein R 1 is PhCH 2 or PhOCH 2 , with or a derivative thereof. Compounds of Formula II may be obtained either by reacting a compound of the formula with Cl 3 CCOOH or a derivative thereof or by reacting an imino-chloride of the above compound with an alkali metal salt of Cl 3 CCOOH. Compounds of Formula III may be obtained either by oxidation of a compound of Formula IV or by esterification of a compound of the formula

    POSTUPAK ZA DOBIJANJE CIKLIČNIH SULFATA
    10.
    发明专利
    POSTUPAK ZA DOBIJANJE CIKLIČNIH SULFATA 未知

    公开(公告)号：YU46890B

    公开(公告)日：1994-06-24

    申请号：YU47589

    申请日：1989-03-07

    Applicant: RHONE POULENC SA

    Inventor： LE ROY P ,  MANDARD-CAZIN B

    IPC: B01J23/46 ,  B01J27/13 ,  C07B61/00 ,  C07D327/10

    Abstract: POSTUPAK ZA DOBIJANJE CIKLIČNIH SULFATA, R2, R3, R4, R5 i R6, identični ili različiti, i označavaju atom vodonika ili halogena ili radikal alkil, aril, alkoksi, ariloksi ili alkoksikarbonil i n je jednako 0 ili 1, pri čemu se podrazumeva da radikal alkil i delovi alkil iz radikala alkoksi ili alkoksikarbonil sadrže 1 do 4 atoma ugljenika i u datom slučaju su supstituisani sa jednim ili više atoma ili radikala, identičnih ili različitih, koji su odabrani izmedju atoma halogena ili radikala alkoksi, ariloksi ili alkoksikarbonil, i da radikali aril i delovi aril iz radikala ariloksi sadrže 6 do 10 atoma ugljenika i u datom slučaju su supstituisani sa jednim ili više atoma radikala, identičnih ili različitih, odabranih izmedju atoma halogena, radikala alkil, alkoksi, ariloksi ili alkoksikarbonil, oksidacijom cikličnog sulfata opte formule: u kojoj R1, R2, R3, R4, R5, R6 i n imaju značenje kao što je gore dato, naznačen time, što se oksidacija realizuje pomoću alkalnog ili zemnoalkalnog hipohalogenita, u prisustvu katalitičke količine derivata rutenijuma i što se radi u vodenoj ili vodeno-organskoj sredini pri temperaturi ispod 10В°C. Prijava sadrži još 7 zavisnih zahteva.

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