Caprolactam purification by oxidn. and distn. - with fast distn. before oxidn. to give higher purity prod. suitable for nylon prodn.

    公开(公告)号:DE3039320A1

    公开(公告)日:1982-05-19

    申请号:DE3039320

    申请日:1980-10-17

    Applicant: SNIA VISCOSA

    Abstract: Raw caprolactam (I), obtd. by extn. from sulphuric soln. with alkylated phenols and re-extn. with water, is purified by oxidn. treatment (pref. with KMnO4), evapn. of the water and successive vacuum distn. The improvement is that a fast distn. in presence of an alkaline cpd. is inserted before the oxidn. treatment. "Fast" distn. means that the evapd. material is not refluxed to the evapn. zone. The purity of the obtd. (I) is further increased by the fast distn. The obtd. (I) may be of sufficient purity to produce polymerisation grade nylon-6 (i.e. nylon suitable for prodn. of industrial prods. such as fibres and plastics). The amt. of oxidising agent reqd. is reduced, which gives ecological and economic advantages, since oxidising agent cost is reduced and less (I) is destroyed by the oxidising agent.

    Caprolactam purificn.
    6.
    发明专利

    公开(公告)号:IT1193210B

    公开(公告)日:1988-06-15

    申请号:IT2465379

    申请日:1979-07-25

    Applicant: SNIA VISCOSA

    Abstract: An information system comprises a computer, storage on the computer for files containing frames of information, a reader for the stored files and a signal transmitter to an output port of the computer. A modulator is connected to the output port of the computer for producing a modulated television carrier signal. A number of television receivers are connected to receive the modulated signal by way of a transmission link. A booster amplifier is provided in the transmission link to increase the strength of the output signal of the modulator. Two or more channels of information are transmitted to the television receivers. The computer storage comprises a magnetic hard disk.

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