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公开(公告)号:JPS5521463A
公开(公告)日:1980-02-15
申请号:JP9478878
申请日:1978-08-03
Applicant: TORAY INDUSTRIES
Inventor: INOUE SHIYUNEI , ISHII SHIGENORI
Abstract: PURPOSE:To prepare a polyester of high whiteness degree and uniform pigment dispersibility with reduced diethylene glycol content, by addition of a pigment after esterification, immediately followed by addition of ethylene glycol and then carrying out polycondensation under vacuum. CONSTITUTION:Bis-beta-hydroxyethylene terephthalate and/or its oligomer are(is) first prepared from terephthalic acid and ethylene glycol. Next, a pigment such as titanium dioxide, etc. is added, and then, within 10 minutes, ethylene glycol is added to the system in an amount of pref. 0.5-3wt% based on the polymer, immediately followed by carrying out polycondensation under vacuum to obtain the objective polyester.