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    ADHESIVE FOR METAL
    2.
    发明专利
    ADHESIVE FOR METAL 失效

    公开(公告)号：JPS56103265A

    公开(公告)日：1981-08-18

    申请号：JP621380

    申请日：1980-01-22

    Applicant: TORAY INDUSTRIES

    Inventor： TANAKA CHIAKI ,  NAKASHIMA SHINOBU ,  NAITOU NAGAYOSHI

    IPC: C08G69/00 ,  C08G69/44 ,  C09J177/00

    Abstract: PURPOSE:The titled adhesive capable of being bonded to strongly a metal without primer coating, having improvd water resistance, comprising a polyester amide consisting of an ester made of benzenedicarboxylic acid, etc. as a main ingredient and an amide made of dodecanamide, etc. in a specific ratio. CONSTITUTION:The desired adhesive comprising a polyester amide (preferably relative viscosity 1.25-3.0 and melting point not higher than 210 deg.C) consisting of (A) 5-80wt% ester unit made of benzenedicarboxylic acid (preferably butylene terephthalate and/or butylene isophthalate) and 1,4-butanediol as a main ingredients and (B) 95-20wt% amide unit consisting of dodecanamide and/or undecanamide (preferably 12-aminododecanoic acid and/or 11-aminoundecanoic acid, and their amide forming derivatives shown by the formulas I and II.

    PREPARATION OF POLYESTERRAMIDE
    3.
    发明专利
    PREPARATION OF POLYESTERRAMIDE 失效

    公开(公告)号：JPS56103221A

    公开(公告)日：1981-08-18

    申请号：JP621480

    申请日：1980-01-22

    Applicant: TORAY INDUSTRIES

    Inventor： TANAKA CHIAKI ,  NAKASHIMA SHINOBU ,  NAITOU NAGAYOSHI

    IPC: C08G69/00 ,  C08G69/44 ,  C09J177/00

    Abstract: PURPOSE:To obtain a novel polyester-amide having improved mechanical strength, impact resistance, transparency, softness, oil resistance, water resistance, adhesive property, flexibility, etc., by copolymerizing ester units with amide units each having a specific structure in a specific proportion. CONSTITUTION:A polyester having an average polymerization degree of 3-8 and ester units expressed by formula I and/or II is copolymerized with a nylon salt consisting of formula III (m is an integer 6-12) anf formula IV (n is an integer 6-10) or an aromatic dicarboxylic acid under vacuum at 200-270 deg.C to give the aimed polyester-amide having (A) the ester units expressed by formula I and/or II and (B) amide units expressed by formula V (R is formula VI or monocyclic aromatic nucleus) at a weight ratio between the units (A) and (B) of 20:80-95:/5. USE:Useful for a molded article, e.g. a fiber or film, a hot-melt adhesive for metal, fiber, plastic or wood, a solution adhesive, a coating material, etc.

    POLYESTER AMIDE AND PRODUCTION THEREOF
    4.
    发明专利
    POLYESTER AMIDE AND PRODUCTION THEREOF 失效

    公开(公告)号：JPS5688428A

    公开(公告)日：1981-07-17

    申请号：JP16558879

    申请日：1979-12-21

    Applicant: TORAY INDUSTRIES

    Inventor： TANAKA CHIAKI ,  NAKASHIMA SHINOBU ,  NAITOU NAGAYOSHI

    IPC: C08G69/00 ,  C08G69/44

    Abstract: PURPOSE:To provide a polyester amide having a high degree of polymn. and outstanding performance, consisting of butylene tere (or iso) phthalate unit and dodecanamide unit and/or undecanamide unit. CONSTITUTION:An arom. dicarboxylic acid (A) consisting of terephthalic acid and/or isophthalic acid is reacted with 1,4-butanediol (B) in an amount of 1.05- 2.0-fold moles of the component (A) and 12-aminododecanoic acid and/or 11-aminoundecanoic acid (C) in the presence of an esterification catalyst at a temp. of 150- 260 deg.C. Then the reaction mixt. is subjected to polycondensation at a temp. of 200- 270 deg.C and at a reduced pressure of 10mm.Hg or below to obtain the desired polyester amide consisting of 20-95wt% butylene terephthalate unit and/or butylene isophthalate unit and 80-5wt% dodecanamide unit and/or undecanamide unit, which is transparent when it is molten and whose melting point is several degrees-20 C higher than that of a conventional product.

    HOTTMELT ADHESIVE FOR TEXTILE
    5.
    发明专利
    HOTTMELT ADHESIVE FOR TEXTILE 失效

    公开(公告)号：JPS54153835A

    公开(公告)日：1979-12-04

    申请号：JP6130478

    申请日：1978-05-23

    Applicant: TORAY INDUSTRIES

    Inventor： TANAKA CHIAKI ,  NAKASHIMA SHINOBU ,  NAITOU NAGAYOSHI

    IPC: C08G63/00 ,  C08G63/66

    Abstract: PURPOSE:To provide a hot-melt adhesive for textile use, having excellent dry-cleaning resistance and hot-water washing resistance, giving excellent touch to the bonded part, and composed of a polyether-ester copolymer having a specific intrinsic viscosity. CONSTITUTION:The title adhesive composed of a polyether-ester copolymer having an intrinsic viscosity (25 deg.C) of 0.5-1.5 measured in o-chlorophenol, is prepared by (IX) carrying out the ester exchange reaction of (A) 1 mole of dicarboxylic acids (or their ester-forming derivatives) wherein the acid component is composed of 70-40% of terephtalic acid and 30-60% of isophthalic acid, (B) 1.1-20 moles of 1,4-butanediol, and (C) 1-10 wt% of a poly(alkyleneoxide) glycol having a number average molecular weight of 300-6000, in the presence of an esterification catalyst, at 150-260 deg.C under atmospheric pressure, and then (II) polymerizing the product at 200-270 deg.C under a reduced pressure of

    POLYETHER-ESTER BLOCK COPOLYMER COMPOSITION
    6.
    发明专利
    POLYETHER-ESTER BLOCK COPOLYMER COMPOSITION 失效

    公开(公告)号：JPS5891758A

    公开(公告)日：1983-05-31

    申请号：JP18916681

    申请日：1981-11-27

    Applicant: TORAY INDUSTRIES

    Inventor： FURUTA YOUKO ,  NAITOU NAGAYOSHI ,  TANAKA CHIAKI

    IPC: C08L67/00 ,  C08G59/00 ,  C08G59/40 ,  C08L63/00 ,  C08L67/02

    Abstract: PURPOSE:To provide the titled copolymer compsn. with improved resistance to thermal degradation and hydrolysis, prepared by adding a glycidyl ester compd. to a polyether-ester block copolymer. CONSTITUTION:The compsn. is prepared by adding 0.01-20wt% glycidyl ester compd. of the formula (where R is 1-30C n-valent hydrocarbon group; n is 1-6) to a polyether-ester block copolymer which consists of 15-90wt% polyester hard segment and 85-10wt% polyether soft segment with a number average molecular weight of 200-6,000. The addition of heat stabilizer improves further the resistance to thermal degradation of the compsn. When hindered phenol and thioether compd. and/or thiophosphite compd. are used as heat stabilizer, the compsn. shows excellent resitance to thermal degradation without coloration.

    POLYESTER ELASTOMAER MOLDING
    8.
    发明专利
    POLYESTER ELASTOMAER MOLDING 失效

    公开(公告)号：JPS5650924A

    公开(公告)日：1981-05-08

    申请号：JP12813279

    申请日：1979-10-04

    Applicant: TORAY INDUSTRIES

    Inventor： HIRATSUKA MOTONORI ,  TANAKA CHIAKI ,  NAITOU NAGAYOSHI

    IPC: C08L67/00 ,  C08G63/00 ,  C08G63/46 ,  C08G63/66 ,  C08G63/91 ,  C08L67/02

    Abstract: PURPOSE:To obtain a polyester elastomer molding which is free of fin formation, and also is improved in fluidity, crystallization rate, molding cycle shortening, and releasing property, by adding a specific ester compound to a specific polyether-ester copolymer. CONSTITUTION:One hundred pts.wt. a polyether-ester copolymer (A), containing as requisite components terephthalic acid, 1,4-butanediol, and polyoxyalkylene glycol (5-80wt%), is mixed with 0.1-20pts.wt. a low-molecular ester compound (B), containing as requisite components terephthalic acid and 1,4-butanediol. Thus, a molding which is good in softening property, elastic recovery, and high- temperature characteristics and also is improved in fluidity, crystallization rate, the shortening of molding cycle, and releasing property, as well as free of the formation of fins, can be obtained.

    POLYESTER ELASTOMER MOLDED PRODUCT
    9.
    发明专利
    POLYESTER ELASTOMER MOLDED PRODUCT 失效

    公开(公告)号：JPS55165948A

    公开(公告)日：1980-12-24

    申请号：JP7226679

    申请日：1979-06-11

    Applicant: TORAY INDUSTRIES

    Inventor： HIRATSUKA MOTONORI ,  TANAKA CHIAKI ,  NAITOU NAGAYOSHI

    IPC: C08L67/00 ,  C08L67/02

    Abstract: PURPOSE:Titled molded product having improved appearance, mold release characteristics and transparency, prepared by dispersing in a polyether-ester copolymer, a polyether having a m.p. higher than that of the copolymer, and molding the dispersion. CONSTITUTION:To an injection molding machine or an extruder, is introduced a mixture prepared by dry-blending 100pts.wt. of (A) a polyether ester copolymer having as essential components, terephthalic acid, 1,4-butanediol and a poly(alkylene oxide) glycol having a number-average MW of 300-6,000; 20-95wt% of units of a hard polyester segment and an inherent viscosity of at least 0.35, with 0.1-10pts.wt. of (B) a polyester having a particle diameter

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