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    TEA LEAF COMPONENT-CONTAINING DEODORANT AND PREPARATION THEREOF
    1.
    发明专利
    TEA LEAF COMPONENT-CONTAINING DEODORANT AND PREPARATION THEREOF 失效

    公开(公告)号：JPH0241165A

    公开(公告)日：1990-02-09

    申请号：JP18812588

    申请日：1988-07-29

    Applicant: UBE INDUSTRIES

    Inventor： SATO SANEHIRO ,  TAKESHITA MICHIO ,  KONO TAKASHI ,  YABUTA HIROMI

    IPC: A61L9/01

    Abstract: PURPOSE:To obtain a deodorant containing no caffeine, having excellent deodorizing efficiency and safe from an aspect of health by combining a selective extraction and removal method of caffeine due to a fluid in a supercritical state with an extraction method of an effective component as a deodorant by a solvent. CONSTITUTION:In the presence of water, tea leaves are brought into contact with a solution mixture of a fluid brought to a supercritical state from a gaseous state and at least one kind of an alcoholic org. solvent selected from 1-4C lower aliphatic monohydric alcohols in a supercritical state to selectively extract and remove caffeine from tea leaves. The obtained extraction residue is extracted with a solvent and the raw material residue is removed from the extracted solution by filtering while the filtrate is conc. or conc. to dryness to obtain a raw deodorizing liquid or powder. The deodorant thus prepared contains 5-20wt.% of tannin as a principal deodorizing effective component and the deodorizing rate thereof is 80% or more and the caffeine content thereof is 1wt.% or less.

    BATCH DISTILLATION METHOD
    3.
    发明专利
    BATCH DISTILLATION METHOD 失效

    公开(公告)号：JPS53119274A

    公开(公告)日：1978-10-18

    申请号：JP3395477

    申请日：1977-03-29

    Applicant: UBE INDUSTRIES

    Inventor： INABA YUKIO ,  MIYATAKE TAKASHI ,  TAKESHITA MICHIO

    IPC: B01D3/14

    Abstract: PURPOSE:To increase recovery ratio for each component and to reduce distillation time by installing a flux drum of variable capacity at the top distillate line of a distillation column, by setting the capacity of the drum for the quantity of the component to be separated, and by taking the distillate received in the drum out of the system after total reflux operation.

    DECAFFEINATING PLANT MATERIAL
    4.
    发明专利
    DECAFFEINATING PLANT MATERIAL 失效

    公开(公告)号：JPH01289448A

    公开(公告)日：1989-11-21

    申请号：JP11816588

    申请日：1988-05-17

    Applicant: UBE INDUSTRIES

    Inventor： SATO SANEHIRO ,  TAKESHITA MICHIO ,  KONO TAKASHI ,  IIDA HIROYUKI

    IPC: A23F3/38 ,  A23F5/20

    Abstract: PURPOSE:To raise removal ratio of caffeine without extracting useful substances from a plant material by extracting and removing caffeine from the plant material with a solution prepared by adding a specific organic solvent to a fluid made into a supercritical state from a gas. CONSTITUTION:The bottom of an extractor 1 is charged with water, a plant material is packed into the upper part of the container, a gas such as carbon dioxide is introduced from a storage tank 10 to a heat exchanger 4, liquefied and fed to the bottom of the extractor 1 by a circulating pump 5. An organic solvent of 1-4C lower aliphatic saturated monohydric alcohol base is sent from a storage tank 11 to a delivery piping of the circulating pump 5 by a supply pump 6 and blended with the carbon dioxide. The pressure of the circulating solution in a supercritical state, containing water provided with caffeine is reduced by a pressure-control valve 8 set in a conduit from a separator 2 to a heat exchanger 9, a first component is gasified and separated into gas and liquid by the separator 2. A second component containing caffeine is introduced to a separating system 3 to separate caffeine.

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